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POTASSIUM HYDROXIDE-氢氧化钾

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POTASSIUM HYDROXIDE-氢氧化钾 POTASSIUM HYDROXIDE Prepared at the 19th JECFA (1975), published in NMRS 55B (1976) and in FNP 52 (1992). Metals and arsenic specifications revised at the 59th JECFA (2002). An ADI not limited' was established at the 9th JECFA (1965) SYNONYMS Caus...

POTASSIUM HYDROXIDE-氢氧化钾
POTASSIUM HYDROXIDE Prepared at the 19th JECFA (1975), published in NMRS 55B (1976) and in FNP 52 (1992). Metals and arsenic specifications revised at the 59th JECFA (2002). An ADI not limited' was established at the 9th JECFA (1965) SYNONYMS Caustic potash, Potassium hydrate; INS No. 525 DEFINITION Chemical names Potassium hydroxide C.A.S. number 1310-58-3 Chemical formula KOH Formula weight 56.11 Assay Not less than 85.0% of total alkali calculated as KOH DESCRIPTION White or nearly white pellets, flakes, sticks, fused masses or other forms FUNCTIONAL USES Alkali CHARACTERISTICS IDENTIFICATION Solubility (Vol. 4) Very soluble in water; freely soluble in ethanol Test for alkali A 1 in 100 solution of the sample is strongly alkaline Test for potassium (Vol. 4) Passes test PURITY Water insoluble substances A 1 in 20 solution of the sample is complete, clear, and colourless Carbonate Not more than 3.5% (as potassium carbonate) Each ml of 1 N sulfuric acid required between the phenolphthalein and methyl orange endpoints in the "METHOD OF ASSAY" is equivalent to 138.2 mg of K2CO3. Lead (Vol. 4) Not more than 2 mg/kg Determine using an atomic absorption technique appropriate to the specified level. The selection of sample size and method of sample preparation may be based on the principles of the method described in Volume 4, “Instrumental Methods.” METHOD OF ASSAY Dissolve about 1.5 g of the sample, accurately weighed, in 40 ml of recently boiled and cooled water, cool to 15o, add phenolphthalein TS and titrate with 1 N sulfuric acid. At the discharge of the pink colour, record the volume of acid required, then add methyl orange TS and continue to titrate to a persistent pink colour. Record the total volume of acid required for the titration. Each ml of 1 N sulfuric acid is equivalent to 56.11 mg of total alkali, calculated as KOH. POTASSIUM HYDROXIDE SYNONYMS DEFINITION Chemical names C.A.S. number Chemical formula Formula weight Assay DESCRIPTION FUNCTIONAL USES CHARACTERISTICS IDENTIFICATION Test for alkali PURITY Water insoluble substances Carbonate METHOD OF ASSAY
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