常用溶剂碳谱峰溶剂名称化学位移sc(ppm峰数CDOD-d48.87CDC3d76.8~77.13DMSO-d39.67CDCDOD-d(CD3)55.05(CD2)15.97D代吡啶-d5(C3,C5)123.33(C3)135.33(C2,C6)149.03CDCN-d(CD)13.07(CN)118.07(CD)2CO-d(CO)206.47(CD3)29.77THF-ck(C3,C4)25.15(C2,C5)...
溶剂名称化学位移sc(ppm峰数CDOD-d48.87CDC3d76.8~77.13DMSO-d39.67CDCDOD-d(CD3)55.05(CD2)15.97D代吡啶-d5(C3,C5)123.33(C3)135.33(C2,C6)149.03CDCN-d(CD)13.07(CN)118.07(CD)2CO-d(CO)206.47(CD3)29.77THF-ck(C3,C4)25.15(C2,C5)67.45CjDj-d6128.13DCON(GD2-d6(CO)167.53(CD3)35.17CDCOOD-d(CO)178.37(CD3)20.37常见非氘代溶剂的碳谱化学位移及谱峰(CD3)2COCDC3CDODDMSOC6D6CDCNDO甲醇49.750.449.848.649.949.549.4氯仿79.277.379.479.177.879.2—DMSO41.240.740.540.540.041.239.4丙酮(CO)(CH3)205.8207.0209.6206.2204.0207.0216.030.540.030.731.030.131.030.9乙酸(CO)(CH3)172.0176.0175.0172.0176.0173.1177.2J20.520.820.621.020.320.721.0乙腈(CN)(CH3)117.6116.4118.0118.0116.0118.3120.011.218.98.510.320.017.814.6环己烷27.527.028.026.327.327.6—二氯甲烷55.054.055.055.053.555.3—乙醚(CH3)(CH2)15.815.215.515.015.515.614.866.065.966.962.066.066.466.4二甲基甲酰胺(CHO)(CH3)163.0162.5164.7163.0162.0163.2165.536.136.436.935.735.036.637.5(CH3)31.131.431.630.730.731.332.0乙醇(CH3)(CH2)18.918.418.418.518.718.817.557.758.358.356.158.0580.58.0乙酸乙酯(CH3)(CO)20.821.020.921.020.221.221.2170.0171.4173.0170.0170.4172.0175.2(CH2)61.060.561.560.060.261.062.3(CH3)14.514.214.514.414.414.514.0正己(CH3)14.314.114.413.914.314.4—烷(CH2)23.322.723.722.023.023.4—(CH2)32.331.632.731.032.032.4—
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