13C谱最新氘代试剂(核磁试剂)化学位移表

13C谱最新氘代试剂（核磁试剂）化学位移表 2010-7-17 13C氘代试剂（核磁试剂）化学位移表 碳原子 氘代四氢呋喃 氘代二氯甲烷 氘代氯仿 氘代甲苯 氘代苯 氘代氯苯 氘代丙酮 氘代DMSO 氘代乙腈 氘代三氟乙醇 氘代甲醇 氘代水 氘代试剂位移   67.21 53.84 77.16 137.48 128.06 134.19 29.84 39.52 1.32 61.50 49.00 25.31 128.87 129.26 206.26 118.26 126.28 127.96 128.25 125.13 125.96 20.43 乙酸 CO 171.69 175.85 175.99 175.30 175.82 175.67 172.31 171.93 173.21 177.96 175.11 177.21 CH3 20.13 20.91 20.81 20.27 20.37 20.40 20.51 20.95 20.73 20.91 20.56 21.03 丙酮 CO 204.19 206.78 207.07 204.00 204.43 204.83 205.87 206.31 207.43 32.35 209.67 215.94 CH3 30.17 31.00 30.92 30.03 30.14 30.12 30.60 30.56 30.91 214.98 30.67 30.89 乙腈 CN 116.79 116.92 116.43 115.76 116.02 115.93 117.60 117.91 118.26 118.95 118.06 119.68 CH3 0.45 2.03 1.89 0.03 0.20 0.63 1.12 1.03 1.79 1.00 0.85 1.47 苯 CH 128.84 128.68 128.37 128.57 128.62 128.38 129.15 128.30 129.32 129.84 129.34 正丁醇 (CH3)3C 67.50 69.11 69.15 68.12 68.19 68.19 68.13 66.88 68.74 72.35 69.40 70.36 (CH3)3C 30.57 31.46 31.25 30.49 30.47 31.13 30.72 30.38 30.68 31.07 30.91 30.29                             二甘醇二甲醚 CH3 58.72 58.95 59.01 58.62 58.66 58.42 58.77 57.98 58.90 59.40 59.06 58.67 CH2 71.17 70.70 70.51 70.92 70.87 70.56 71.03 69.54 70.99 73.05 71.33 70.05 CH2 72.72 72.25 71.90 72.39 72.35 72.07 72.63 71.25 72.63 71.33 72.92 71.63 二甲基甲酰胺 CH 161.96 162.57 162.62 161.93 162.13 162.01 162.79 162.29 163.31 166.01 164.73 165.53 CH3 35.65 36.56 36.50 35.22 35.25 35.45 36.15 35.73 36.57 37.76 36.89 37.54 CH3 30.70 31.39 31.45 30.64 30.72 30.71 31.03 30.73 31.32 30.96 31.61 32.03 1,4-二恶烷 CH2 67.65 67.47 67.14 67.17 67.16 66.95 67.60 66.36 67.72 68.52 68.11 67.19 DME CH3 58.72 59.02 59.08 58.63 58.68 58.31 58.45 58.03 58.89 59.52 59.06 58.67 CH2 72.58 72.24 71.84 72.25 72.21 71.81 72.47 71.17 72.47 72.87 72.72 71.49 乙烷 CH3 6.79 6.91 6.89 6.94 6.96 6.91 6.88 6.61 6.99 7.01 6.98 乙醇 CH3 18.90 18.69 18.41 18.78 18.72 18.55 18.89 18.51 18.80 18.11 18.40 17.47 CH2 57.60 58.57 58.28 57.81 57.86 57.63 57.72 56.07 57.96 59.68 58.26 58.05                             二氧化碳 CO2 125.69 125.26 124.99 124.86 124.76 126.08 125.81 124.21 125.89 126.92 126.31 二硫化碳 CS2 193.37 192.95 192.83 192.71 192.69 192.49 193.58 192.63 193.60 196.26 193.82 197.25 四氯化碳 CCl4 96.89 96.52 96.34 96.57 96.44 96.38 96.65 95.44 96.68 97.74 97.21 96.73 氯仿 CH 79.24 77.99 77.36 77.89 77.79 77.67 79.19 79.16 79.17 78.83 79.44 18-冠醚-6 CH2 71.34 70.47 70.55 70.86 70.59 70.55 71.25 69.85 71.22 70.80 71.47 70.14 环己胺 CH2 27.58 27.38 26.94 27.31 27.23 26.99 27.51 26.33 27.63 28.34 27.96 二氯乙烷 CH2 44.64 44.35 43.50 43.40 43.59 43.60 45.25 45.02 45.54 45.28 45.11 二氯甲烷 CH2 54.67 54.24 53.52 53.47 53.46 53.54 54.95 54.84 55.32 54.46 54.78 乙醚 CH3 15.49 15.44 15.20 15.47 15.46 15.35 15.78 15.12 15.63 15.33 15.46 14.77 CH2 66.14 66.11 65.91 65.94 65.94 65.79 66.12 62.05 66.32 67.55 66.88 66.42                             乙酸乙酯 CH3CO 20.45 21.15 21.04 20.46 20.56 20.50 20.83 20.68 21.16 21.18 20.88 21.15 CO 170.32 171.24 171.36 170.02 170.44 170.20 170.96 170.31 171.68 175.55 172.89 175.26 CH2 60.30 60.63 60.49 60.08 60.21 60.06 60.56 59.74 60.98 62.70 61.50 62.32 CH3 14.37 14.37 14.19 14.23 14.19 14.07 14.50 14.40 14.54 14.36 14.49 13.92 乙烯 CH2 123.09 123.20 123.13 122.92 122.96 122.95 123.47 123.52 123.69 , 124.08 123.46 乙二醇 CH2 64.35 63.79 64.29 64.34 64.03 64.26 62.76 64.22 64.87 64.30 63.17   H greaseb CH2 30.45 30.14 29.71 30.31 30.22 30.11 六甲基苯 C 131.88 132.09 132.21 131.72 131.79 131.54 132.22 131.10 132.61 134.04 132.53 CH3 16.71 16.93 16.98 16.84 16.95 16.68 16.86 16.60 16.94 17.04 16.90 正己烷 CH3 14.22 14.28 14.14 14.34 14.32 14.18 14.34 13.88 14.43 14.63 14.45 CH2(2,5) 23.33 23.07 22.70 23.12 23.04 22.86 23.28 22.05 23.40 24.06 23.68 CH2(3,4) 32.34 32.01 31.64 32.06 31.96 31.77 32.30 30.95 32.36 33.17 32.73                               吡咯 CH(2,5) 118.03 117.93 117.77 117.61 117.78 117.65 117.98 117.32 118.47 119.61 118.28 119.06 CH(3,4) 107.74 108.02 107.98 108.15 108.21 108.03 108.04 107.07 108.31 108.85 108.11 107.83 吡咯啉 CH2(2,5) 45.82 47.02 46.93 47.12 46.86 46.75 46.51 47.57 47.43 47.23 46.83 CH2(3,4) 26.17 25.83 25.56 25.75 25.65 25.59 25.26 26.34 25.73 26.29 25.86 硅脂 CH3 1.20 1.22 1.19 1.37 1.38 1.09 1.40 2.87 2.10 四氢呋喃 CH2(2,5) 68.03 68.16 67.97 67.75 67.80 67.64 68.07 67.03 68.33 69.53 68.83 68.68 CH2(3,4) 26.19 25.98 25.62 25.79 25.72 25.68 26.15 25.14 26.27 26.69 26.48 25.67 甲苯 CH3 21.29 21.53 21.46 21.37 21.10 21.23 21.46 20.99 21.50 21.62 21.50 C(1) 138.24 138.36 137.89 137.84 137.91 137.65 138.48 137.35 138.90 139.92 138.85 CH(2,6) 129.47 129.35 129.07 129.33 129.33 129.12 129.76 128.88 129.94 130.58 129.91 CH(3,5) 128.71 128.54 128.26 128.51 128.56 128.31 129.03 128.18 129.23 129.79 129.20 CH(4) 125.84 125.62 125.33 125.66 125.68 125.43 126.12 125.29 126.28 126.82 126.29 三乙胺 CH3 12.51 12.12 11.61 12.39 12.35 11.87 12.49 11.74 12.38 9.51 11.09 9.07 CH2 47.18 46.75 46.25 46.82 46.77 46.36 47.07 45.74 47.10 48.45 46.96 47.19                             六甲基二硅醚 CH3 1.83 1.96 1.97 1.99 2.05 1.92 2.01 1.96 2.07 2.09 1.99 2.31 HMPAc CH3 36.89 36.99 36.87 36.80 36.88 36.64 37.04 36.42 37.10 37.21 37.00 36.46 咪唑 CH(2) 135.72 135.76 135.38 135.57 135.76 135.50 135.89 135.15 136.33 136.58 136.31 136.65 CH(4,5) 122.20 122.16 122.00 122.13 122.16 121.96 122.31 121.55 122.78 122.93 122.60 122.43 甲烷 CH4 -4.90 -4.33 -4.63 -4.34 -4.29 -4.33 -5.33 -4.01 -4.61 -5.88 -4.90 甲醇 CH3 49.64 50.45 50.41 49.90 49.97 49.66 49.77 48.59 49.90 50.67 49.86 49.50d 硝基甲烷 CH3 62.49 63.03 62.50 61.14 61.16 61.68 63.21 63.28 63.66 63.17 63.08 63.22 正戊烷 CH3 14.18 14.24 14.08 14.27 14.25 14.10 14.29 13.28 14.37 14.54 14.39 CH2(2,4) 23.00 22.77 22.38 22.79 22.72 22.54 22.98 21.70 23.08 23.75 23.38 CH2(3) 34.87 34.57 34.16 34.54 34.45 34.26 34.83 33.48 34.89 35.76 35.30 丙烷 CH3 16.60 16.63 16.63 16.65 16.66 16.56 16.68 16.34 16.73 16.93 16.80 CH2 16.82 16.63 16.37 16.63 16.60 16.48 16.78 15.67 16.91 17.46 17.19 2-丙醇 CH3 25.70 25.43 25.14 25.24 25.18 25.14 25.67 25.43 25.55 25.21 25.27 24.38 CH 66.14 64.67 64.50 64.12 64.23 64.18 63.85 64.92 64.30 66.69 64.71 64.88 丙烯 CH3 19.27 19.47 19.50 19.32 19.38 19.32 19.42 19.20 19.48 19.63 19.50 CH2 115.74 115.70 115.74 115.89 115.92 115.86 116.03 116.07 116.12 116.38 116.04 CH 134.02 134.21 133.91 133.61 133.69 133.57 134.34 133.55 134.78 136.00 134.61 吡啶 CH(2,6) 150.57 150.27 149.90 150.25 150.27 149.93 150.67 149.58 150.76 149.76 150.07 149.18 CH(3,5) 124.08 124.06 123.75 123.46 123.58 123.49 124.57 123.84 127.76 126.27 125.53 125.12 CH(4) 135.99 136.16 135.96 135.17 135.28 135.32 136.56 136.05 136.89 139.62 138.35 138.2                             以上为核磁共振碳谱中氘代试剂及常用溶剂在相应氘代试剂中的化学位移。