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封装手册Amperex Technology Limited Handbook for sealing H A N D B O O K Prepared by QM Guo Process department 目录 1. 封装的用途及基本原理………………………………………………… 1.1 封装的用途…………………………………………………………………… 1.2 封装的基...

封装手册
Amperex Technology Limited Handbook for sealing H A N D B O O K Prepared by QM Guo Process department 目录 1. 封装的用途及基本原理………………………………………………… 1.1 封装的用途…………………………………………………………………… 1.2 封装的基本原理……………………………………………………………… 1.2.1 封装材料的结构……………………………………………………… 1.2.2 封装原理……………………………………………………………… 1.3 主要封装工序………………………………………………………………… 2. 封装参数的选择………………………………………………………… 2.1 几种常见的封装材料………………………………………………………… 2.2 设备的工作原理……………………………………………………………… 2.3 设备参数的选择……………………………………………………………… 2.4 工艺参数的选择……………………………………………………………… 2.4.1 温度…………………………………………………………………… 2.4.2 时间…………………………………………………………………… 2.4.3 压力…………………………………………………………………… 2.5 Process Structure… SOP………………………………………………… 3. 封装工艺的控制及效果检查…………………………………………… 4. 常见的封装失效模式…………………………………………………… 4.1 分层 ………………………………………………………………………… 4.2 电阻坏品、腐蚀……………………………………………………………… 4.3 胀气…………………………………………………………………………… 4.4 顶封起皱、鼓泡……………………………………………………………… 5. 封装可靠性评估………………………………………………………… 6. 封装材料的判断………………………………………………………… 7. 封装工序FMEA…………………………………………………………… 8. 附 录…………………………………………………………………….. 1. 封装的用途及基本原理 1.1 封装的用途 电池的使用过程是一个不断充电放电的过程,电芯内部在不断的进行动态的电化学反应,电芯内部存有多用有机溶剂和遇水、氧等能迅速分解产生大量氢氟酸的电解质锂盐,一旦电芯内部HF含量过高,电芯电性能(如容量、循环寿命、放电平台等)会发生损耗,严重影响电芯的使用。 由于内部有机溶剂的存在,必须要求软包装材料能够抵挡有机溶剂的溶胀、溶解、吸收等,同时由于聚合物锂离子电芯的高性能表现,要求其软包装材料对氧、水分的阻隔比普通的铝塑复合膜高上万倍。使用这种高阻隔性的软包装材料将聚合物锂离子电芯极片、电解液与外部环境完全隔绝,使其内部处于真空、无氧、无水的环境,才能保证聚合物锂离子电芯的高性能使用要求,有这层包装的存在,电芯才能正常使用,若包装失效,电芯使用寿命即终止,导致报废。 1.2封装的基本原理介绍 1.2.1 封装材料的结构 我们使用的软包装材料(包装铝箔)结构上主要分为三个部分:Nylon、Al 和 PP, 其示意图如下: 图1 其中,各部分主要作用 Nylon :可以有效阻止空气尤其是氧的渗透,维持电芯内部的环境,同时可以保证包装铝箔具备良好的形变能力。 Al :可以有效阻止空气中水分的渗透,维持电芯内部的环境,具有一定的厚度强度能够防止外部对电芯的损伤。 PP :不会被电芯内有机溶剂溶解、溶胀等,是电芯内部环境的最直接的包装保护,绝缘,有效阻止内部电解质等与Al layer接触,避免Al layer被腐蚀。 1.2.2 封装机理 阴、阳极片等在经过叠片、焊接等工序成裸电芯,需要用包装铝箔进行包装,包装铝箔被冲成所需尺寸形状的单坑或双坑Pocket,坑的正面为包装铝箔内层,即PP层,为进行封装的层面。PP为聚合物包膜层,有一定的熔点,裸电芯放入Pocket内后,包装铝箔折叠,PP面相对,通过给予Nylon层一定的热量,热量经Al layer传递给PP,PP熔化,施加一定的压力使两层熔化的PP混熔,一定时间的相互融合后,冷却,两层包装铝箔通过PP黏结在一起,达到封装的目的。 简单归结为:PP受热熔化,一定的时间、压力冷却后粘合在一起。 1.3 主要封装工序 ATL聚合物锂离子电芯封装工艺共有四道工序,分别为Top sealing、Side sealing、Vacuum sealing和Degassing工序,这四道工序的先后流程如下: 图2 这里简要介绍一下各封装工序的主要功能 Top sealing & Side sealing 电芯在超声波焊接极耳(卷绕电芯例外)后,装入Pocket loading在夹具上,使用顶封封装机进行Top sealing和Side sealing。裸电芯正负极Tab上各有Sealant(Sealant为类似于包装铝箔PP的材料,性质与PP相似,可以与PP混熔),所以在Top sealing时在极耳处Tab通过Sealant与PP从而被密封在Pocket中,顶部其他区域和Side sealing 一样,通过PP的粘合达到密封的效果。 Vacuum sealing 电芯在经过Top sealing 和Side sealing 后,已经将两个敞开的Pocket口密封,剩下的一个口在气袋边。电芯在干燥房灌注完电解液并经过真空静置后,为保证电芯在此后化成等工序中电芯内部与外界隔绝,需要在干燥房对最后的开口边进行抽真空密封。此工序即称为Vacuum sealing. Degassing 电芯在经过化成、Baking等工序,由于SEI膜的形成等会产生一定量的气体,气体会导致电芯在以后正常充放电使用的过程中性能下降,所以必须要将内部产生的气体抽出,并在真空条件下,对电芯主体旁的Pocket Die进行最终的密封。此称为Degassing工序。 各封装工序封装位置示意如下图3所示: 图3 ATL 包装铝箔采用的是冲坑模式,将裸电芯放入Pocket中,将Pocket对折,进行三口封装,Top sealing和Side sealing使用的是顶封封装机;Vacuum sealing使用的是比较简易的封装机器,此工序难度较小;Degassing机器比较复杂,工序难度较大。 2. 封装参数的选择 2.1 几种常见的封装材料 目前国产的软包装材料在密封性、黏结性、拉伸变形强度等各种性能方面还比较欠缺。ATL使用的包装铝箔来源于国外,主要有DNP的PFR-001-04, SHOWA公司的PFR-001-05、PFR-002-05等,及Toppan公司产品。其中,MP经常使用的两种包装铝箔为PFR-001-05和PFR-002-05。现在主要介绍一下这两种包装铝箔的结构性能。 表1 Type Nylon Thickness (μm) Al layer Thickness (μm) PP Thickness (μm) PP Melting Point (ºC) PFR-001-05 20 40 40 158~160 PFR-002-05 20 40 80 158~160 其余两层胶水的厚度为10μm PFR-001-05的单层厚度为110μm,PFR-002-05的单层厚度为150μm, 熔点可通过DSC分析仪测得(如图4和图5所示),从表1可以看出两者的区别只是PP层厚度的差异,这也就决定了在进行封装时两种包装铝箔所用的封头的差异。 2.2 设备的工作原理 顶封封装机和Degassing机器采用的都是上下双封头热压的方式,Vacuum sealing采用的是单封头热压的方式,此种为简易封装机器,构造比较简单,这里主要介绍顶封机器和Degassing机器的主体构造及其功能。 2.2.1顶封封装机 安装:a.设备的安装:参考说明书 b.把机器放置在承重能力大于200kg的工作台上,并用水平规调整水平 c.把机器的电源与220V单相电源连接,机器的气源管线与0.4~0.7mpa的压缩气源连接。 调试:a.将设备与压缩气管路连接,调节机器的总压力到0.4Mpa b.将机器接通电源启动,首先切换到手动状态下进行顺序动作,调整气缸上的传感器到合适位置 c.将转盘在手动状态下进回原点操作,待转盘回到原点后放上夹具校正封头的位置 d.将温控器的设定温度调到要求值,对机器进行升温 e.待温度升到设定值后,将机器切换到自动状态进行运作 f.调整夹具首先用MRB电池进行试做,检查上下封头的平行度和是否有错位情况 g.如有错位或是平行度不良则调节上下封头的可调行程气缸调节高度或移动封头底座的位置进行对位 h.在移动上下封头的过程中注意要先把封头的温度降下来,确保安全 j.将机器连续运行2个小时以上试其各仪表和传动部件的稳定性 维护:日常维护事项, a.清洁台面,使之光洁而不凌乱,每班一次 b. 检查各气管是否漏气,如有漏气及时更换,每班一次 c. 检查校对面板各仪表显示与WI文件要求相符,每班一次 d. 检查校对封装压力与WI文件要求相符,每班一次 f. 检查校对封装压力与WI文件要求相符,每班一次 g. 检查更换封头铁氟龙,使封头平整且无任何胶粒及脏物,每2小时一次 定期维护事项 a.给各轴承加润滑脂,每月一次 b.检查、更换开裂的封头隔热块,每月一次 c.检查、更换破损的封头的感温线及加热管,每月一次 d.检查、紧固松动的传动装置,每周一次 e.检查、校正封头及各连接体,使之连接可靠,性能良好,每周一次 目视控制: 安全操作: a. 严禁将手伸入热封头下及其它运动部件等危险处 b. 严禁触摸加热部件及其它带电部件 c. 设备发生异常情况时,立即反馈给相关设备 工程 路基工程安全技术交底工程项目施工成本控制工程量增项单年度零星工程技术标正投影法基本原理 师 d. 严禁两人同时操作机器 e. 严禁违反相关文件操作机器 仪表检查: a.温度检查:每班开拉前用测温仪测量加热部分的实际温度与温控器的显示温度是否相符,要求偏差不得超出WI允许范围,并且适当增减温度的设定值,相求表的显示及实际值要有相应趋势的变化。 b.压力检查:每班前要检查表的外观有无损坏,并通过调压阀相应增减压力,看表指针有无相应的变化,要求变化要灵敏,并且当无压缩气供给时,表的显示为零。 c.记 录:将结果写入关键设备参数跟踪 记录 混凝土 养护记录下载土方回填监理旁站记录免费下载集备记录下载集备记录下载集备记录下载 表(参照QSP-016附表),如有异常要及时通知相关人员解决 常见设备异常及解决方法: 故障1:机器运行不连贯有中途停止的现象 产生原因:(1)起传递动作信号的传感器位置不对或传感器坏掉导致各动作之间 衔接不上而中途停止 (2)封头的温度超标导致温控器报警而终止运行 (3)温控器失灵导致温度失控而报警终止动行 (4)感温线接触不好,在运动过程中传递的信号跳动过大导致的报警 而终止运行 (5)STAR按键触点接触不良导致的信号传递不及时而产生的不动作 或误动作 解决方法:(1)把机器切换到手动状态,按照机器自动状态运作的动作顺序分步 动作对好每一个气缸上动作传感器的位置 (2)检查温控器的温度控制偏差是否过小或继电器是否有损坏,如有 异常及`时校正或更换配件 (3)如温控器坏掉则在关闭电源后可把温控器从面板中抽出换上新的 温控器(注意不需要拆接任何电线接头) (4)切断电源后把相对应的封头腔体拆下,拿出封头,拆下感温线确 认更换 (5)切断电源后把操作板拆下更换按键 故障2:温控器显示出现错误 产生原因:这一般是感温线损坏的表征信号,有时感温线是没有完全断掉,可能在 运动的过程中断点会分离,在不动的过程中断点又接触所以显示器上会 跳动或异常显示 解决方法:切断电源后把相对应的封头腔体拆下,拿出封头,拆下感温线确认更换 故障3:温度不上升 产生原因:(1)温控器的设置错误导致加热功能被关闭 (2)中间继电器损坏,导致加热管没有电流通过 (3)加热管损坏无法加热 解决方法:(1)重新校正温控器 (2)更换继电器 (3)切断电源后把相对应的封头腔体拆下,拿出封头,拆下加热管确认更换。 故障4:转盘机的转盘定位不准 产生原因:(1)转盘皮带松动导致转盘转动时晃动或滑动而定位不准 (2)步进电机的脉冲设置错误 (3)步进电机的轴销松动或脱落 解决方法:(1)重新调整皮带的松紧,以刚好张紧用手轻推而没有松驰为宜 (2)重新校正脉冲 (3)拆下电机检查,确认重新装配 故障5:转盘机的转盘转动不灵活,或偶有偏离定位孔的现象,或响声过大 产生原因:(1)转盘皮带过紧 (2)转盘皮带与转轮间的配合不相吻合有咬牙现象 (3)步进电机的转动轴转动不灵活 解决方法:(1)重新调整皮带松紧,以刚好张紧用手轻推而没有松驰为宜 (2)重新装配皮带,使之相吻合 (3)拆下电机检查,确认重新修理 2.2.2 Degassing机器 安装:a. 每台设备的占地面积约2平方米 b.设备应安置于水平的地面且四脚要平稳。 c.设备的电源插头应与220V,50Hz,单相电源连接。 e.设备的压缩空气管与0.5~0.7Mpa的厂房气源连接,真空管与〈=L-90kpa的 真空源连接。 调试: a.将设备与真空管路、压缩气管路连接,调节机器的总压力到0.6Mpa,真空-90kpa. b.机器电源启动,首先切换到手动状态下进行顺序动作,调整气缸上的传感器到合适位置 c.将温控器的设定温度调到要求值,对机器进行升温。 d.待温度升到设定值后,将机器切换到自动状态进行运作。 e.将垫板调整到合适位置首先用MRB电池进行试做,检查上下封头的平行度和是否有错位情况 f.如有错位或是平行度不良则调节上封腔的位置以移动封头进行对位。 g.在移动上封腔的过程中注意不要使刺刀受到损伤,要保证刺刀的对位准确、运作顺畅和刺穿效果良好。 h.将机器连续运行2个小时以上试其各仪表和传动部件的稳定性。 维护:日常维护: a. 每天清洁整理台面,使其光洁而不凌乱。 b. 每天检查各气管是否漏气,如果漏气要及时更换。 c. 每天检查校对压力显示与PI文件要求相符。 d. 每天检查校对控制面板各仪表显示值及实际值与PI文件要求相符。 e. 每天检查机器运行是否正常,如有异常及时反馈相关人员检修。 f. 检查更换封头铁氟龙,每2小时必须更换一次。 定期维护 a. 清洁机器腔体、整理各管线,每月一次。 b. 给各轴承及导轨加润滑油或润滑脂,每月一次。 c. 检查、更换机器加热系统,每月一次 。 d. 清洁及检查更换真空电磁阀,每月一次。 e. 检查及更换各气缸的换向阀,每月一次。 f. 检查校正封头的平行度,每周一次。 目视控制:同顶封机器 标准 excel标准偏差excel标准偏差函数exl标准差函数国标检验抽样标准表免费下载红头文件格式标准下载 安全操作:a. 严禁将手伸入热封头下及其它运动部件等危险处。 b. 严禁触摸加热部件及其它带电部件。 c. 设备发出异常情况时,立即反馈给相关设备工程师。 d. 严禁两人同时操作机器。 e. 严禁违反相关文件操作机器。 仪表检查:同顶封机器标准 常见设备故障及解决: 故障1:机器运行不连贯有中途停止的现象,参考顶封机器 故障2:温控器显示出现错误,参考顶封机器 故障3:温度不上升,参考顶封机器 故障4:转盘机的转盘定位不准,参考顶封机器 故障5:转盘机的转盘转动不灵活,或偶有偏离定位孔的现象,或响声过大,参考顶封机器。 故障6:真空度不够 产生原因:(1)总的真空管路系统真空度不够 (2)拆装封腔过程中没有装配好或是密封硅胶损坏而导致密封不良 (3)真空电磁阀损坏或电磁阀内部电解液过多导致堵塞 解决方法:(1)检查管路系统的真空度,确认系统问题后及时找厂房维修 (2)重新装配封腔,更换密封硅胶 (3)更换新的电磁阀或拆下电磁阀后清洗电磁阀内腔 故障7:不抽真空 产生原因:(1)真空电磁阀的电感线圈损坏导致电磁阀没有动作 (2)上压腔的气缸动作传感器损坏或没有感应到而导致电磁阀没有 指令信号 (3)真空表的设置错误导致信号终止 解决方法:(1)更换电磁阀的电感线圈 (2)更换传感器或重新调整传感器的位置 (3)重新校正真空表的设置 2.3 设备参数的选择 封头的选择 封头有两种,一种是用于Top sealing的顶封封头,一种是用于Side sealing和Degassing封装的侧封封头。 顶封封头主体示意图(侧视图) 图4 顶封封头俯视示意图 图5 各标示点注释: a为顶封封头封头凹槽宽度,由电芯Tab宽度决定,可参考《封头履历表》 b宽度由电芯Tab 设计 领导形象设计圆作业设计ao工艺污水处理厂设计附属工程施工组织设计清扫机器人结构设计 中心矩决定,可参考《封头履历表》 2c为封头凹槽深度,由Tab厚度决定,常见对应数据如下表2所示,在本节后面附计算方法 Tab thickness (mm) 0.1 0.08 0.05 Groove depth (mm) 0.23±0.01 0.22±0.01 0.18±0.01 d为顶封封头的辅助加热块,由于Tab和Sealant的存在,顶封热量容易损失,所以在上、下封头各有一与封头联结的加热块,用于在封装过程中压住Tab给予Tab一定的热量,从而达到好的密封效果。 结构:下封头辅助加热块与封头一体固定,其平面与封头凹槽持平;上封头辅助加热块由弹簧控制,要求其必须高出封头约 1mm,才能保证在封头下压后它能够压紧Tab。 Al转Ni tab后厚度发生变化,在辅助加热块上此位置处有大约0.02mm的凹槽。 要点:上封头与弹簧配套的两根小铜棒必须为光滑状,否则弹簧易被卡助,达不到辅助加热Tab的目的。 侧封封头示意图(侧视)如图6 图6 图6中,封头尺寸由电芯尺寸决定(可参考《封头履历表》),上封头封装截面为平面 下封头封装截面有两个凹槽: a称为避胶槽,其尺寸参考《封头履历表》 b称为Stopper,其高度由电芯所使用的包装铝箔类型、厚度决定,表3给出了常用的Thickness ~ Stopper对照数值,其原理算法将附在本章节后面。 表3 Foil Types Foil Thickness (mm) Stopper Depth (mm) PFR-001-05 / PFR-001-04 0.15 0.25±0.01 PFR-002-05 0.11 0.18±0.01 Stopper作用是可以有效控制Packing foil PP的变形率,达到比较好的封装性能,同时 可保证电芯有比较好的电阻性能。 备注: 在侧封封头内侧有一个倒角。 附:侧封头Stopper高度和顶封头凹槽深度的原理计算 附1:侧封头Stopper高度与Packing foil厚度关系计算方法 设PP厚度为a;PP变形率为b;Nylon、Al等厚度为c;Stopper高度为h,则计算公式为: h=2a(1-b)+2c 附2:顶封头凹槽深度与Tab厚度关系计算方法 设PP厚度为a;PP变形率为b;Nylon、Al等厚度为c;Sealant厚度为d;Tab;厚度为e;顶封Tab位变形率为f;凹槽深度为h,则计算公式为: e+2(a+d)(1-f)+2c=h+2c+2a(1-b) 即 h=e+2(ab-af+d-df) 如:以PFR-002-05及0.1mm厚度Tab为例 Stopper h=2*0.08*(1-0.3)+2*0.07=0.252mm 凹槽h=0.1+2*(0.08*0.3-0.08*0.2+0.075-0.075*0.2)=0.236mm 封头的检查 封头在使用一段时间后,由于上下封头不断的碰撞磨损,封头的Stopper和凹槽可能会有一定程度局部磨损,尤其是侧封封头,其Stopper一般较长,下封头长时间受上封头的力后极易发生磨损。为保证封头的精确性,一般每周对封头Stopper和凹槽进行一次平行度检查,在使用25~30万次后进行一次返修。另在调整或使用新封头,也需要根据尺寸要求对封头进行检查。 ATL目前通常采用一下两种方法对Stopper 和凹槽进行检查确认: 塞尺法 侧封头检查:选择合适尺度的塞尺放入侧封封头Stopper之间,将上封头手动下压后,左右拉动塞尺检查Stopper间隙是否合格。判断标准如下: 表4 Stopper 高度 塞尺厚度(mm) 检查要求 0.25mm 0.24 塞尺可通过Stopper 间的每一个区域 0.26 Stopper 被抬起,且两端Stopper 间隙相当 0.18mm 0.16 塞尺可通过Stopper 间的每一个区域 0.19 Stopper 被抬起,且两端Stopper 间隙相当 顶封头检查:选择0.02mm的塞尺,放在封头无槽位置,要求在整个封头上能够受力均匀。 复写纸法 侧封头检查:按照目前两种Stopper高度的封头,对复写纸和打印纸有不同的要求。 Stopper为0.25mm,将封头温度调整到70±10℃左右,在三层打印纸中夹两张复写纸,放在下封头上,手动将上封头打下压在复写纸上约1s,将封头抬起,检查封头留在打印纸上的印痕。 Stopper为0.18mm,将封头温度调整到70±10℃左右,在两层打印纸中夹一张复写纸,放在下封头上,手动将上封头打下压在复写纸上约1s,将封头抬起,检查封头留在打印纸上的印痕。 顶封头检查:将封头温度调整到70±10℃左右,在两层打印纸中夹一张复写纸,放在下封头上,手动将上封头打下压在复写纸上约1s,将封头抬起,检查封头留在打印纸上的印痕。 附:打印纸封头印痕判断方法,主要不良如下: 印痕太黑。原因是温度过高或者压下时间长,不能发现问题,需要重新制作样品; 印记一边深一边浅。原因是封头两不平行,需要调整平行后再验证; 印记一边清晰整齐一边模糊。原因是一边有倒角模糊或者沿宽度方向倾斜。要求调机再验证; 印记两边整齐清晰,中间模糊。原因是封头变形。要求将封头卸下进行返修打磨; 印记清晰,均匀,中间有些花纹但是也均匀,没有过黑现象,封头平行度OK。 封头平行度印痕不良图示举例 夹具的选择 顶封夹具:a. 是用于 Loading裸电芯和Pocket进行封装,需要根据电芯的尺寸选择调整夹具的限位,调整夹具Tab中心矩时,必须合适,保证Loading电芯时两Tab能够刚好在夹具对应位置,电芯tab且不可发生扭曲,否则在顶封极易导致Ni tab与包装铝箔Al 发生短路,造成电芯腐蚀 。 b. 目前ATL顶封夹具Tab槽位处都配有Sealant胶挡位块,目的是在顶封 控制Sealant外露长度,避免电芯最终长度超出Spec. c. 夹具压板,对于M6S卷绕电芯一般使用size较大,可防止顶部错位,封边起皱等。 平板调节:平板位置必须要与夹具、封头等匹配,否则易发生起皱,注意螺丝的调节 度。 平衡垫块的选择:Degassing机器转盘区域必须加有一定高度的垫块,防止在封装时机 盖板过度挤压电芯,或电芯受力不均匀,导致电芯出现外观问题或其他性能问题。垫块高度与所生产的电芯高度相同,一般要高出电芯1~2mm。 刺刀选择:按经验来说,进行Degassing封装时,刺刀加密和刺刀位置的选择对电芯 封装有一定的好处,在抽真空过程中,电芯内部残留电解液杂质会随气体 均匀抽走,不易在封边处发生堆积,降低封边分层的可能性。 气缸选择:按经验规则是,长度100mm及以上的电芯一般选择大缸径的气缸,直径大概在40mm以上;长度较小的电芯选择比较小缸径的气缸,一般选择直径为32mm 或20mm直径的气缸,若电芯封边起皱,也可尝试换成大缸径气缸进行试验。 2.4工艺参数的选择 我们知道包装铝箔为铝塑复合膜,是给其一定的温度、时间和压力使它内层的PP熔化黏结在一起达到密封的目的。在保证封头各结构性能尺寸参数都复合条件的情况下,还必须要达到一定的温度才能使PP熔化,一定的压力和时间才能进行融合凝结,本章节主要介绍了制定温度、时间和压力参数的依据,一些试验原理及参数对封装性能的影响。 这里先列出ATL常用的包装铝箔的封装参数(Top & Side sealing、Degassing),供参考: 表5. Top sealing顶封、侧封封装参数表 Foil类型 封头要求 Tab类型 热封时间 顶、侧气压 设定温度 顶封 侧封 顶封 侧封 顶封 侧封 PFR-001-05 PFR-002-05 PFR-001-04 Tab加热 ALL 3S 3S 0.3MPa 0.4MPa 185°C 180°C 表6. Degassing封装参数表 Foil 类型 封头Stopper 封头Teflon 封头气缸压力 封装真空度 真空保持时间 封装时间 封头设定温度 PFR-001-05 PFR-002-05 PFR-001-04 No Yes 0.6Mpa ≤-90.0KPa 4s 6s 200℃(上/下) Yes Yes 0.6Mpa ≤-90.0KPa 4s 6s 200℃(上/下) Yes No 0.6MPa ≤-90.0KPa 4s 6s 180℃(上/下) 备注:PFR-001-05、PFR-002-05和PFR-001-04这三种包装铝箔PP的熔点经DSC测试,基本一样,都分布在160ºC左右,因此使用相同的温度参数。在早期,ATL使用无Stopper的侧封封头,需要在封头表面贴有Teflon胶布防止封边受过度挤压。 温度、时间参数的选择 我们已经知道封装PP的熔点,必须要保证封装温度超过其熔点,才能使其熔化达到好的封装效果,我们设定的是封头的温度,而热量需要经过Nylon和Al才能传递到PP,还需要排除其他散热损失的影响,即必须使封装过程中PP所收到的实际温度超过其熔点一定的范围,才会保证PP受热熔化处于稳定的温度状态。 为测量PP在受热熔化过程中的实际温度,我们使用Tracker (HIOKI 8420-51 MEMOERY HiLOGGER)进行封装实际温度的测量,为准确地测量,使用的测量探头为两种专用细金属丝,先介绍一下测量原理: 图7 测量示意图 测量记录设备可以每0.01s自动记录一次温度数据,测量导线被完全封装在两层PP中间,因此得到的温度~时间数据曲线为PP的封装实际熔化温度曲线。 从以上数据关系图可以看出,封头温度为175ºC,仪器所测量的PP实际受热温度温度由室温上升到160ºC(PP熔化温度)大概需要0.8s,在160ºC~165ºC 间维持1.2s;封头温度为180ºC,PP受热实际温度由室温上升到160ºC大概需要0.4s,维持在此温度上1.6s,最高温度在170ºC,热量由封头传递到PP,温度损失了将近10ºC. 考虑到机器设计的偏差,给予封头温度±5ºC的偏差,所以若封头温度为175ºC,就会PP受热温度不够的可能性,导致封装不良。为保证顶封PP、Sealant与Tab的良好黏结及Tab的散热损失,将顶封的温度选定为185°C且需要对封头进行辅助加热。经试验证明封头温度过高会造成PP破损加剧,电阻坏品增加。另温度在195ºC以上时,Nylon会老化发黄,影响到其性能。 从温度曲线可以看出,随着封装时间的延长,PP受热温度维持在最高水平的时间越长,PP熔化黏结的效果越好,但PP的变形也越大,如下四副侧封边横截面剖视图(在X700显微镜下观察) 180ºC/3s/0.4Mpa Remark: PP黏结时受损严重,两层PP间有明显的分口。 180ºC/2s/0.4Mpa Remark: PP黏结时融合较好,封边处有良好的PP堆积保证有好的电阻 但从下面顶封的温度(185ºC)曲线来看,,封装时间为2s ,Sealant封装部位温度在140ºC(DSC测量ATL所用Sealant熔点为140ºC左右)以上的时间明显非常短,对比3s的封装时间曲线,可以看出它有比较好的时间进行融合 Top sealing 2s Top sealing 3s 由于Degassing在后工序Forming进行,Degassing边的包装铝箔PP已经经过了长时间 的电解液浸泡,在Formation及Baking等工序可能产生凝胶等,PP的融合黏结性能会变差。经大量的试验证明,在上下封头上贴Teflon,下封头Teflon在Stopper上,电芯的封装效果会很好。 下面图示为上下封头贴Teflon,温度均为200ºC,封装时间为6s的温度变化曲线。Vacuum阶段,机器真空腔会闭合,同时下封头带动刺刀上来刺传Pocket,由于下封头的热传导,PP温度会稍有上升,在Sealing阶段,上封头下来与下封头闭合进行热压,6s时间内需要大概1.3s达到PP的熔化温度,其余时间用于进行封装。 Teflon会导致热量的损失,所以温度由180 ºC调整到200ºC。 压力参数 封边所受到的压力F与气缸直径d、压强参数m的关系为: F=π*(d/2)*(d/2)*m*N N为固定系数。气缸直径越大,电芯封边所受的压力越大,一般来说,32mm缸径选择0.6Mpa的压强,50mm缸径选择0.4Mpa的压强。 真空度的选择 在ATL早期生产过程中,需要进行真空抽出电芯内部气体的共有3道工序,即: Injection Vacuum sealing Standby Formation I Pre-degassing Formation II Baking Degassing Vacuum sealing、Pre-degassing和Degassing需要进行抽真空,由于工艺及产品性能的改 进,目前只有Vacuum sealing和Degassing两道工序,已经取消了Pre-degassing,Formation 只进行一次。Vacuum sealing为在Dry room进行灌液真空静置后,进行封口前抽掉内部空气 防止影响到电芯的化成,进而影响到电芯的性能。当然此工序真空度也不可过高,以避免电 解液被抽出。-60Kpa ~ -40Kpa已经能够很好满足要求。 Degassing工序,电芯已经彻底完成活化,以后的充放电不会再产生气体,所以为保证 电芯的使用性能,在此工序必须要抽出内部所有气体,采用<-90Kpa的真空度,进行4s钟 抽气过程。做完Degassing的电芯内部真空度达到-40Kpa一下,一般对P1及M6S工艺电 电芯,真空度可以达到-60Kpa一下,可以在抽真空测量系统测得。 备注:经大量实验证明,Degassing机器真空度在-85Kpa以下、4s钟抽气或-90Kpa 以下,2s钟抽气,基本不会影响电芯内部的真空度和使用性能。 2.5 Process structure….SOP Top sealing process Top sealing工序由三个小工序组成:电芯Loading工序,Sealing工序,电芯Unloading 工序,每道小工序由一个员工操作,共三个作业人员,机器为感应器感应进行封装操作,有转盘机和普通机两种,转盘机可同时进行两次顶封,两次侧封。普通机有两种机型,一种是顶、侧封同时操作,一种是顶、侧封可以分开操作。 Loading工序:将裸电芯Bi-cell和空Pocket分别使用操作台面的吸尘器进行吸尘处理,将Bi-cell放置在Pocket坑内,再loading在顶封夹具并进行调整对位,注意Tab要准确放入槽位,不能发生扭曲,Sealant外露要合乎规格要求,顶部Pocket不能错位。 Sealing工序:先进行顶封操作,再进行侧封操作,注意封装过程中不可使感应器感应,否则会造成假封装; Unloading工序:将作好顶封、侧封的电芯从夹具上取下,并进行目视检查。检查项目有:侧封未封区,顶封未封区,Sealant外露,顶边错位,封印尺寸。 Top sealing 工序操作流程 第一步:清洁并开机检查 · 打开电源,打开压缩空气阀,设定封头气缸压力,封头温度以及封装时间; · 检查机器手动、自动状态下封头和平板动作是否正常; · 手动:正常状态平板不动或没有下降到位情况下,按上封头不能动作; · 自动:正常状态平板下降到位后上封头才能自动打下,反之属异常; · 每班生产前检查顶封夹具(侧边挡条,压把等)、挡胶块是否弯曲受损变形或断裂,若有变形或受损现象,立即更换; · 每班生产前需用Master校验顶封夹具,观察Master是否可松紧适当地放入夹具定位区域及挡胶块Tab定位槽内,夹具顶边与挡胶块的距离是否符合Master sealant 位置尺寸; · 测量封头热封面温度并作好记录(此项由生产部专人负责以确保测量的一致性); · 检查顶封Teflon胶布表面是否有起皱、破损、粘结不牢、严重变色现象,发现以上情况需及时更换Teflon胶布;(封头贴Teflon进行本操作) 第二步:首件制作 · Loading电芯,将铝箔袋对折,使上下边对齐,放入夹具定位,Tab 保持平行并放入定位槽中; · 调节Sealant高度,使Sealant露出包装袋上边缘约0.2~0.5mm; · 将夹具置于热封机工作台上定位,启动封装机,对电池进行封装; · 取出电池,检查封装平行度,槽位印,未封区,封装外观,Tab距电芯主体边距离等,数据记录在首件评估表; 第三步:正常生产 · 首件填写完毕,经技术员及技术员以上工程人员确认OK后开始量产; · 量产时,发现封装异常,停止生产并立即汇报当班技术员和工程师,调试OK后,重新制作首件,确认OK后,再进行生产(调机时生产的货MRB). · 封装完成后从夹具上取下电芯,检查Sealant外露,封印尺寸外观等是否符合要求,并根据好坏品分开放置。 质量控制要求 · 顶封和侧封靠外靠内的未封区区域是否符合要求; · PP胶是否粘封头,金属tab上是否有PP胶溢出; · 实测温度需在设定温度±5℃范围内,顶封辅助加热块设定温度和顶封封头温度相同,夹具放整齐; · 封头热封面的温度为封头实测温度(热封头和温度感应头均不贴Teflon); · 调节温度控制器的补偿值之前必须严格测试封头温度,并记录在调机记录表中; · 拉力测试不可斜拉,须将测试样放正才可固定进行测试,拉力测试频次: 每台机每班1次; · 如连续三次拉力测试不OK,需知会相关工程师进行及时的处理; · 新品种开拉要测拉力,所有拉力测试结果须技术员及技术员以上工程人员确认后方可开始量产,所有拉力测试的拉速选择中速; · Tab拉力测试样品,必须保证Tab侧面无sealant此时测出的拉力值即为tab与sealant的真实拉力; · 封装机上下封头的重合度偏离不能超过0.2mm,夹具凹槽与封头凹槽应该处于同一水平位置; · 异常质量处理:因停电停气压停机,恢复正常后,需重新测温,确认相关参数,并重做平行度测试; · 顶封的载料盘子底部必须要垫一层1mm厚和白色硅胶防止电池打滑产生不良。 Top sealing辅料及工夹具 物料(含辅料)清单 工夹具清单 序号 名称 数量 序号 名称 数量 1 pocket 1 剪刀 1把 2 裸电芯 --- 2 钢尺 1卷 3 Teflon --- 3 测温仪 1套 4 复写纸 --- 4 塞尺 1把 5 5 游标卡尺 1把 6 6 封装手柄 4把 7 7 拉力器 1台 安全操作要求 · 封头在工作时,在高温条件下,不可触摸,以免烫伤; · 操作时手不能轻易放在封头下,以避免手被压; · 严禁两人同时操作一台机器; Vacuum sealing 一机一人,机器为Single bar机,采用手动双按钮控制操作。需要注意的是封印的清晰度和封印的重合情况。 Degassing 一机一人,为圆盘转动机器,根据电芯长短和封头长度决定所放置电芯的数量,小电芯可以放置两个,大电芯放置一个。采用双按钮控制操作。机器的运转过程如下:上下腔体合 并 开始真空抽气 下封头上来,刺刀刺破Pocket 保持4s真空抽气 上封头下压,进行6s封装 腔体充气,封头分离,完成封装操作。Visual电芯的封印和未封区等情况。 Degassing标准操作过程 第一步:清洁 · 每半小时清洁真空腔、上压板、刺刀压板一次。 · 每2小时更换抹布1次,确保每次用无污物的抹布对机器进行清洁,避免交叉污染。 · 每半小时清洁剪刀一次。(如有刺刀的机器则无需做此项工作)。 · 每班必须关闭电源对设备进行全面清洁一次,确保当班产生的污物不残留在机器上。 第二步:开关机 · 通压缩空气和真空阀、开控制箱背部的电源开关,系统通电。 · 开机:按Power ON 键,机器参数表显示各参数,在运行画面(主菜单)按“自动”键。 · 关机:按Power OFF,紧急关机:按E-Stop,暂停时须按Stop。 第三步:设定参数 参照包装铝箔的P/N设定封头温度,选择合适的De-gassing封头, 设定封头气缸压力 第四步:首件制作 待封头显示温度达到设定值后,适用温度表测量封头温度,并进行记录,温度符合要求进行下首件制作,否则需进行检查。根据首件制作要求(可参考首件制作表)电芯各尺寸符合要求后方可进行正常生产。 第五步:放置电芯 用手拿电芯主体的中部,放入到Degassing机的真空槽位内,电池凸起的肩部紧靠真空槽的内壁,电池位置符合定位标记,双手按下控制面板上的绿色START按钮。操作时,双手避免触摸气袋。 取电芯 用手拿电芯主体的中部,从Degassing机的真空槽位中取出,良品放入流拉盒(蓝色); 不良品放入不良盒(红色)。操作时,双手避免触摸气袋。 过程进行             放置电芯          启动封装          封装完毕       Degassing完毕        OK电芯           NG电芯 质量控制要求: · 真空腔内需用Teflon于电芯绝缘 底腔垫板垫到合适厚度,使电池在封装时可以被盖板压紧以防Foil 起皱;同时针对不同厚度的电芯选用相对应厚度的平衡垫块以平衡上弹簧压板运作平稳。即保证Degassing 时上下压板能平稳地压住电芯表面;对于电芯表面有涨液现象的品种,要求电池定位槽内及上弹簧压板相对于电池的位置要贴专用海绵; · 操作时,只能手拿电芯的主体,不能触摸气袋;同时,需轻拿轻放,避免野蛮操作; · 外观平整无污染:电芯主体不能有电解液污物,封印上不能有皱褶,未封区要保证,另外,对于该工序F024(凹点)的控制,要求每两小时每台机抽检100ea电池确认F024是否达到要求,其标准参考QA提供的样本,如没有达到要求,则停拉整顿直到合格,如参照样本还难以判断则要求通过测量显微镜进行定量检测再和QA的样本进行对比区分(针对外观有特殊要求的品种)。 · 封印明显平整,尺寸正确;未封区宽度;切边后封印的宽度≥1.5mm,封印边缘距离电芯0.5~1.5mm。 · 检查Degassing封装后,有无Pocket角位破损。 安全控制: 高温,严禁手触摸高温区;严禁两人同时操作,换胶布要将一个垫块放在机器真空腔旁平台上的保护手。 应急处理办法: ● 在紧急情况下或在Degassing 机出现异常时,按下设备控制面板上的紧急开关。 ● 在生产过程中系统出现异常(如:厂房系统压力突然降低,设备在封装过程中温度超出 控制限,设备突然停电等)时,设备中的电池不可翻修,做报废处理,且当系统恢复正常 后要重新做首签方可正常生产。 工夹具及辅料: 物料(含辅料)清单 工夹具清单 序号 名称 数量 序号 名称 数量 1 化成后电芯 --- 1 剪刀 1把 2 Teflon --- 2 钢尺 1卷 3 复写纸 --- 3 测温仪 1套 4 白纸 4 塞尺 1把 5 5 游标卡尺 一把 6 6 拉力器 1台 7 7 六角扳子 1套 3. 封装工艺的控制及效果检查 这里主要介绍在整个封装工艺过程中的控制细节,比较凌乱,并附有三个封装工序的 PFMEA。 封装尺寸的控制 下面表格详细介绍了电芯Pocket上的封装尺寸(Top sealing & Degassing ) 检查项目 描述 规格要求 目的 Dim A 顶部未封区域宽度 电芯主体部分≥ 0.1mm,气袋部分允许没有未封区。 减少溢胶;去掉Teflon减少封装不良 Dim B 侧封与顶封交叉的距离 重叠区域大于1mm 边封时顶部不溢胶; 且部分与顶封重叠避免漏气 Dim C, G 顶封超出电芯主体的距离 ≥3.5mm 确保封装宽度, 减少顶封漏气机会 Dim D 侧封封印到电芯距离 0.5~1.5mm,测量标准以深坑为准 避免隔离膜烫伤,减少腐蚀机会 大电芯以封印两头到电芯距离为准;中小电芯以封印中部到电芯距离为准。 Dim F 气袋边封印位置 0<F≤3mm 顶封时封头两边不溢胶, 去掉Teflon,减少封装不良 Dim H 侧封封印宽度 ≥2.5mm 确保封装宽度 Dim J 顶封封印宽度 ≥(封头宽-0.5mm) 确保封装宽度, 确保漏气和抗水性 Dim K 顶封槽印与Tab 的距离 ≥0.5mm(大中电池) 避免Tab 和 Foil 短路 ≥0明显距离(小电池) 检查项目 描述 规格要求 目的 Dim A 边封与电池顶边的距离 0.5~1.5mm 边封时顶部不溢胶; 且部分与顶封重叠避免漏气 Dim B 边封封印宽度 ≥3.0mm 确保封装宽度 Dim C 封印到电芯距离 (从电芯深坑边测量) 0.5~1.5mm 避免隔离膜烫伤 控制重点:1.顶封封印的位置:若太接近顶部,会造成顶部PP胶溢出污染封头,存在 压Tab的可能性,导致Ni tab与包装铝箔Al layer短路,发生腐蚀。若过于接近Pocket,会造成Pocket坑与顶边衔接处Nylon受高温与Al layer分离,发生鼓泡影响到密封性。 2.封边与电芯的距离:封边与电芯Pocket的距离越大,热封时封边处PP受损伤的机率越小,电芯的电阻性能越好,综合考虑电芯的切边宽度与实体宽度,未封区控制在1.0~1.5是比较优化的条件。 测量以电芯深坑边为基准,可以使用CCD电子测量显微镜进行精确测量也可以钢尺抵住Pocket进行测量。 3.封装宽度:电芯在切边成型必须控制切边后的有效封装宽度,经封装可靠性实验证明,1.0mm的有效封装宽度可以保证电芯密封性,由于控制的精确性, 规定 关于下班后关闭电源的规定党章中关于入党时间的规定公务员考核规定下载规定办法文件下载宁波关于闷顶的规定 至少在1.5mm,ATL目前一般在2.5mm左右。 (附:有效封边宽度实验研究报告) 4.顶封封头宽度:为有效控制顶封封印及控制电芯长度提高容量,我们对顶封封头宽度进行了评估,结果证明使用PFR-001-05包装铝箔,1.7mm封头可以满足ATL电芯密封性能的要求。 (附:Top sealing 1.7mm封装评估报告) 5.侧封封印必须要与顶封封印重合,要求在Top sealing调试夹具与Degassing定位必须在制作首件时调整OK。 6.封头定位:ATL采用上下封头热压的方式进行封装,必须要求上下封头合在一起能够对齐,否则会导致封边处内部PP被没有重合的封头烫伤,造成电阻坏品,目前控制标准是前后左右错位不超过0.2mm,每周进行一次检查。   7.外观控制:为防止电芯在成型后内部有异物(如Film、Separator、Packing foil 等)造成凸点凸痕,裸电芯在Loading前,需要和Pocket一起进行吸尘处理;为防止在后工序造成表面损伤,顶封后电芯表面需要包装Mylar;另电芯在后工序避免人为或机器操作作用力集中在Pocket气袋上,导致角位破损。ATL大电芯采用在角位加热熔胶减少必要损失。  8.Teflon胶布:由于Degassing边PP经受长时间电解液的浸泡和电解液杂质等的影响,给封装带来一定的困难,所以我们在Degassing封头Stopper位加贴一层Teflon,以增加柔韧性,可以获得较好的封装效果。但需控制Teflon的粘贴方式,不能贴在Stopper外封头上,否则会造成封装不良;并且Teflon 一定要平整,生产过程中不能超过2个小时更换一次胶布,防止Teflon起皱、破损导致封装不良。 封装效果的检查 首件测试,包括拉力测试、未封区检查、Sealant外露检查、封装尺寸检查、电阻测试、封装平行度检查、分层检查等 拉力测试:Top sealing和Degassing都要进行真实样品的制作,并用拉力测试机进行拉力测量。Top sealing需要检查侧封边和顶封边,方法:侧封边剪切8mm宽测试样2条,进行拉力测试;顶封边两tab拉力测试样品是沿Tab的侧面剪开,然后用刀片刮去Tab两个侧面的Sealant 和Foil确保TAB的两侧金属外露,并进行拉力测试.;顶封边tab之间和气袋部分取测试样三个进行拉力测试;Degassing边方法与侧封边一样(拉力参考值,Foil拉力大于15N;Tab拉力大于5N,可计算工序能力) Tab加热块检查:Top sealing工序,先将下封头打上来,将Al、 Ni tab分别搭在封头槽位,再将上封头压下来,然后用手拉动tab,观察tab加热条是否能压住tab(正常情况下Tab 加热块比顶封封头高出约1mm)。 未封区检查:首件制作要检查电芯的未封区以确认机器夹具等已经调节到位,并在生产过程中Unloading电芯时对未封区宽度进行Visual。 Sealant外露检查:Sealant有两个作用,一是用于进行封装连接Tab与Foil;一是具有绝缘作用,Tab上的Sealant外露可以防止焊接PTC,Ni tab由于折叠与Foil Al 短路造成腐蚀,所以Ni tab上Sealant必须露出至少0.2mm。若受电芯长度限制,可在顶封夹具上使用挡胶快控制Sealant外露过长。Al tab与Al短路不存在风险,所以可不必考虑其上 Sealant没有外露。 封装尺寸检查:根据前面表格所述尺寸检查,确保各规格符合要求。特别注意的是顶封封印不可压到Tab,顶封槽位不能压在Tab上,否则造成顶封Ni tab短路引起腐蚀。 电阻测试:Top sealing在封装后可使用万用表测量Ni tab与包装铝箔Al间的电阻,一般必须保证为无穷大,可以保证顶封机器夹具已经调试OK,避免短路腐蚀。在后工序Final Visual工序,需要100%测量Ni tab与包装铝箔Al的电阻,挑出不合格品,在Degassing工序需要进行控制,因此要进行抽检,优率低于报警线需要Troubleshooting。 封装平行度检查:Top sealing工序,检查正常封装的电芯,撕开封装面包括顶封和侧封,观察PP黏结状况,要求无Foil本色,乳白色为良好状态,重点检查Tab有无缝状黏结不良处,如有异常需工程师判断是否来料异常或设备异常等并进行解决。本文后面章节对平行度判定进行了总结。Top sealing工序平行度需每2小时检查一次。 分层检查:Degassing工序,电芯成型切边后用刀片轻刮检查Degassing边横切面,反复2~3次看是否有部位有轻微裂口出现,重点检查Degassing与Top sealing重合部位附近及封边上较软的部位,两封边没有分开判断为OK,若分开判断为分层。 封边内PP检查:控制未封区的目的就是防止电芯隔离膜或所包绿较在封装时划破隔离膜导致电解液渗透造成电阻坏品。在检查封装平行度后,要观察是否封边压到隔离膜或绿较,封边处PP是否破损,如有,需进行调整。 4. 常见的封装失效模式 4.1 封装不良(分层) ATL电芯共进行四次封装,分别是Top sealing、Side sealing、Vacuum sealing和Degassing,任何一道工艺的封装不良都可能导致电芯漏液、胀气、性能下降等。封装不良指包装铝箔PP(或与Sealant)没有黏结完好导致两层包装铝箔局部分开,使电芯内部与外界空气等接触。下面介绍常见导致封装不良的主要原因及各工序失效经验的总结。 我们知道温度、时间、压力是影响封装的关键工艺参数,前面我们已经介绍了PP的熔点和封装时温度变化曲线,一旦由于机器或设置原因导致封头实际温度低于设置温度范围,PP的实际受热温度可能达不到它的熔点,会造成它的熔化粘接不良,所以会进行定期的温度测试已保证封头温度;封头温度发生异常偏低时,必须要准确确认封头实际温度,检查是否感温线、加热管等老化或断裂,切不可调整超出范围的温度补偿。时间和压力比较稳定,可以有效的保证封装所需的条件。 Top sealing & Side sealing 引起顶封封装不良漏液的原因主要有两种:一是温度不够,顶封有Tab和Sealant的存在需要较高的温度;一是封装面处有杂质;顶封有两种粘接情况,PP与PP粘接;PP与Sealant粘接;PP与Sealant部位经常发生封装不良,导致电芯在后工序Baking时发生漏液。此处发生封装不良漏液的情况有: 1.封头温度过低导致PP与Sealant受热温度不够(可参考升温曲线); 2.Tab辅助加热块没有压住Tab起到辅助作用(可参考前面辅助加热块控制方法);例:603028曾发生大量漏液; 3.封装区域有杂质或其它辅助液体溶剂,例:P2 Model 463450曾在极耳处加AT2绝缘胶水防止内部短路,由于操作及控制方法不当导致胶水残留在Sealant上,造成封装不良; 4.单面Sealant;Sealant制作时 Tab没有在两片Sealant中间,封装时Tab与PP直接接触,时有发生; 5.Tab-lead Sealant有气泡或污物;应该检查改善Tab-lead制作工序,是否Teflon破损、起皱、脏等,环境是否清洁,机器Rubber是否受损等,例:604396曾经因Sealant污物而漏液; 6.Tab表面污物或处理不均匀;ATL所使用的Al tab在制作Sealant前是经过溶剂处理的,否则在制作成Sealant后经受电解液浸泡的能力非常弱(85ºC 低于10分钟Sealant就会脱落),导致电芯灌注电解液短时间内就发生漏液。目前Al tab,采用C4或C5处理,清洗掉表面的油渍、污渍,在其表面形成络合层,(在X700显微镜下表面无明显条纹)处理后的Tab-lead 85ºC下经受电解液浸泡24小时以上Sealant不会脱落;Ni tab制作成Sealant前需经过丙酮清洗处理,85ºC下经受电解液浸泡40分钟左右(C6处理抗电解液时间会更加长些);处理后的Tab-lead制作成电芯后就不存在灌注电解液后发生泄漏的可能性。若清洗或处理的不完全,Tab-lead Sealant部位Tab上有污物,那么在灌注电解液后极有可能发生漏液情况。此种现象多有发生,604396情况最为严重。 7.假封装,电芯在封装过程中,封头压在封边部位后,误操作导致感应器感应,尚未完成封装操作,封头就离开封边,Pocket只被压在了一起,PP 没有完好融合在一起; 8.夹具定位不准,夹具与封装对位没有调整好,侧封封边与顶封封边没有重合。 Vacuum sealing 目前ATL采用的是简易的Single bar 机进行Vacuum sealing。下封头愈腔体一体,下封头单独加热,采用的温度比较高,并加了几层的Teflon胶布。Vacuum sealing 封装不良会导致电芯内部与外界水分、氧气等接触,电解液会发生变质变性影响到电芯的化成(激活)、容量、循环性能等。影响到封装性能的主要有: 1. 下封头温度,由于采用的是单封头加热,热量比较容易损失,所以必须保证封头的 温度; 2. 封头平行度,下封头粘贴了几层Teflon,必须保证封头的平行度符合要求,注意 Teflon的使用寿命、破损、老化、褶皱等;05年55A5130曾经由于封头长期使用导致平行度失控造成大批量电芯漏液,性能下降; 3. 操作问题,个别员工为提高效率,放置在腔体内的电芯过多,封装部位超出封头长度范围或在封装边缘,会导致部分区域没有封装或封装不良(温度不够),这种情况在拉上经常出现。现在已经对电芯与封头的放置位置作了规定。 4. 假封装,电芯在封装过程中,封头压在封边部位后,误操作导致感应器感应,尚未完成封装操作,封头就离开封边,Pocket只被压在了一起,PP 没有完好融合在一起。 Degassing Degassing是电芯的最后一道封装工序,电芯已基本成型,后面主要是性能测试工序,若发生封装不良导致电芯胀气、漏液等性能失效,基本都在加工商或最终客户反应出来,严重影响信誉。它不像Top sealing、Side sealing和Vacuum sealing 等可以在Baking工序或流拉过程中能够表现出来。它是异常重要的一道工序,也是问题经常发生的工序,电芯PP在Degassing前已经过了长时间的电解液浸泡,激活过程电解液的变质,并且需要进行高真空的抽气后才进行封装,所以比较难以进行封装,任何的异常都可能导致封装不良,造成密封缺陷。事实上,电芯发生封装不良(分层)基本都分布在Degassing边,这里介绍以往关于分层经验的总结。 1.温度,Degassing采用上下封头同时加热进行封装,由于机器本身原因或调试原因封头温度过低会导致封装实际温度达不到PP熔化温度(可参考升温曲线);目前封头均贴有Teflon,更要注意温度的控制; 2.封头平行度,不同厚度Packing foil,需使用不同高度Stopper的封头,若PFR-002-05使用的是0.18mm的封头必然会导致封装不良。另封头长期使用会造成磨损,导致Stopper间隙局部或整体变大,导致PP变形率不够。封头封装部位有凹点(破损)或凸点(杂质)也可能造成封装不良;封头上有粘胶,污物,杂质等。 3.Teflon,若Teflon发生脱落、褶皱等,都会造成封边不良,正常生产情况下Teflon的使用寿命不能超过2小时,否则易发生变形,在实际生产过程中必须随时监控Teflon处于正常状态,一旦异常及时更换,更换新的Teflon要保证平伏的贴在封头表面; 4.电芯定位,调试机器制作首件时要保证电芯Degassing封边与顶封封印重合至少0.5mm,才不会发生封边不良; 5.电解液凝胶,电芯化成进行激活是一个消耗电解质形成SEI膜的反应过程,之后的85ºC 4hrs Baking工序可促进相界面的形成稳定,得到比较好的C-rate、Cycle life特性。为控制电芯厚度,许多Model采取夹具Baking方式,夹具Baking后电解液会形成大量凝胶(无色透明)聚集在电芯的顶部和尾部,真空抽气会把凝胶聚集在Degassing封边部位,即使极少量的凝胶在两层PP间也会造成此部位封装不良,发生整体或局部分层。由于凝胶导致的分层多分布在顶封和Degassing交叉部位附近,这是因为尾部有教多隔离膜外露,凝胶被隔离膜所阻挡,抽气时不易聚集在封边部位,而顶部空间较大(极耳的存在)凝胶可以无障碍地被抽吸到此位置导致封装不良。 电解液凝胶导致的分层经常出现,一般采用以下几种方法解决问题:a.取消夹具,直接进行Baking;b.必须夹住baking,可在Degassing后进行(目前基本采用这种方法,已进行过性能评估);c.对于P2Model,必须在Degassing前夹住Baking,需在干燥房剪掉气袋(保证干燥房的控制条件)使用棉签和无尘纸采用规定方法清洁掉凝胶,再进行Degassing封装,并且需要加封一次才能保证封装OK。但电芯在干燥房敞口时间不能过长,防止性能受影响;d.采取预封装方法,电芯化成前静置时采用特殊封头对Degassing边(交叉部位)进行1/3预封装,最终再进行Degassing封装。e.尝试研究一次封装;对于进行两次封装的情况,需要控制第二次封边的位置、封装时间,以保证电芯电阻。 6.凝胶电解质,ATL部分Model采用凝胶电解质以提高电芯的高温性能,要求在化成前电解质先进行胶化,此电解质严重影响电芯的Degassing封装性能。此电解质进行Baking就可以胶化,若封边处在注液后残留有电解液经Baking会在此处产生胶状物质,影响封装。可以在真空静置后剪开气袋清洁掉封边位置的电解液再进行一次热压走完后面工序。或在胶化前进行预封装。若具有可行性,通过添加剂实现一次封装。 7.电芯内部杂质的影响,若电芯脱炭掉粉在封边处或被吸到封边处也会影响封装;经验证明电芯极耳所包黄胶,经不同电解液浸泡后产生的胶状物或电解液被污染,流到交叉部位也会导致两PP产生界面隔膜不能很好的粘合,表现为PP没有软化。黄胶为CE认证,不能取消(如有其它胶纸可代替最好),可以控制黄胶纸在Degassing边极耳外露的尺寸。 8.电芯定位不准,定位调整或操作放置不到位会导致Degassing封边与顶边不重合,引起封装不良。 4.2 电阻坏品、腐蚀 ATL电芯从开始到结束共有三次阻抗测试,包括:极片Hi-pot测试、Foil电阻测试和内阻(IMP)测试。Hi-pot影响电芯的化成,内阻(IMP)影响电芯的自放电,它们只反应到电芯的电压、容量性能,可以通过现有的高精度设备将坏品挑出。但Foil电阻坏品有发生腐蚀的可能性,一般需要一段时间最终在客户出表现出来,它的失效表现为外观Al被腐蚀破烂,变黑,电芯胀气,无法使用,可以说是最严重的坏品表现,是一件非常恐怖的事情! Foil电阻坏品指的是电芯Ni tab(阳极)与包装铝箔Al layer短路,目前ATL定义Ni tab 与Al layer 电阻低于1.0×200Mohm(非OEM产品)和OEM产品为低于2.0×200Mohm的为电阻坏品,使用万用表测量挑出以避免电芯在客户处发生腐蚀。当然,电阻越大甚至无穷大,发生腐蚀的概率越低。对于这两个标准的选择是基于对电芯进行On-hold模拟测试而定,大概客户反应的腐蚀坏品为4ppm,个别案例除外(指由于特殊原因导致电芯必然会发生腐蚀)。 我们知道控制这种电阻坏品的目的是防止包装铝箔的铝层发生腐蚀,下面就从腐蚀发生原因、腐蚀防止、电阻坏品防止几个方面入手介绍。 腐蚀原因 引起电芯腐蚀必须具备两个短路的通道:一,离子短路通道,即包装铝箔铝层与阳极发生离子短路;二,电子短路通道,即包装铝箔铝层与阳极发生电子短路。这样包装铝箔的铝层就与阳极形成一个短路的回路,阳极即为电芯负极,处于低电势的部分,一旦与铝接触会通过电导率较高的电解液引起电化学反应,化学反应,导致铝层的不断被消耗。空气中水分会进入电芯内部导致进一步反应产生大量气体。这两种短路是电芯发生腐蚀的必要条件,两者缺一不可。 腐蚀防止 我们知道离子短路和电子短路是发生腐蚀的必要条件,要防止腐蚀就必须弄清楚两种短路形成的原因。我们已经知道了包装铝箔的结构,内部为绝缘PP,PP的一个作用就是绝缘,将电解液环境与铝层隔离,保护铝层,发生离子短路是由于PP发生破损致使电解液渗透将铝层与阳极导通,因此腐蚀均发生在PP破损部位。电子短路必须是有导体在阳极和铝层(PP破损处)间能够导通电子或阳极通过Ni tab直接与铝层短路导通电子。要防止腐蚀的发生就必须杜绝两种短路的存在。在电芯的封装过程中,封边部位的PP受到热压后PP比较容易发生破损,所以会产生比较多的电阻坏品,因此只要发生电子短路,腐蚀必然发生,防止腐蚀,必须先从防止电子短路开始。 阳极通过Ni tab与包装铝箔铝层在顶封部位发生短路,PP绝缘胶失去保护作用,Ni tab与铝层接触,这种情况必然会发生腐蚀。目前Ni tab与包装铝层发生短路主要有两种情况: 第1, 在顶封过程中两者直接短接: a. 顶封封头槽位与包装铝箔厚度不匹配或封头变形损坏等导致Ni tab顶封时PP变形率过大,被挤压到严电芯长度方向,Ni tab与铝层导通; b. 顶封夹具、Loading操作失误或顶边宽度设计不够,顶封时封头压偏在Ni tab上,使Tab顶部PP被挤压流走,发生短路; c. 顶封封头槽位压在Ni tab上或过度压偏导致两者短路; d. 顶封夹具调整不合理或Tab中心矩不合格(尤其焊接返修产品),在loading电芯时为Ni tab发生扭曲,导致两者在封装过程中短路; e. Tab 上有毛刺或杂质刺穿Sealant和PP导致两者短路。 第2, 在焊接PTC或Fuse过程中,折叠Ni tab两者直接发生短路: a. 顶封后Ni tab上Sealant没有外露或外露长度不够,导致在折叠后Ni tab直接与包装铝箔截面铝层发生短路; b. 如2×0.5mm Ni tab 比较柔软,由于折叠方法问题导致Ni tab与截面铝层导通(即使有外露Sealant保护);451730曾经由于此种原因在客户处发生大量腐蚀,缘由是由于加工商没有考虑到折叠后对截面的绝缘保护。 以上所列到的原因为实际过程中对腐蚀样品失效分析经验的总结,Ni tab一旦与包装铝箔铝层发生直接短路,电子直接导通,必然会发生腐蚀,毋庸置疑!在生产过程中必须注意对以上所列举的方面的控制,同时在进行腐蚀失效时也需要先从这几个方面入手。其实除阳极通过Ni tab与铝层在顶封部位直接发生短路外,还有另外一种情况就是在电芯内部阳极通过电子导电物质与PP破损处裸露铝层短路。电子导电物质一般为金属Partical、碳粉或导电剂物质,多发生P1工艺的Model上,因为它的阳极几乎直接暴露在PP破损的两个侧封边部位。P2工艺电芯由于表面有隔离膜包裹住电芯,封边部位阳极没有与铝层接触的可能性,目前位置尚未发现因为电子导电物质引起腐蚀的案例。M6S卷绕工艺电芯由阴极收尾,外面一层为阴极铝箔,隔离膜和阴极铝箔会阻止阳极与铝层接触,但M6S采用的是Overhung的设计方式,阳极要超出阴极1mm,当发生严重错位阳极膜片会在电芯底部或顶部伸出隔离膜而暴露,阳极膜片比较脆碳粉等导电物质易脱落引起短路,383450目前位置有一个电芯为此种短路案例。 刚才介绍了引起电阻坏品及发生腐蚀的诸多原因,引起电芯发生腐蚀最常见的直接因素便是顶封部位Ni tab与包装铝箔铝层发生短接,由于前面所指各种原因导致该部位绝缘胶变薄,不能完全隔断Ni tab与包装铝箔铝层。可以参考下面的示意图: 以上为短接情况的示意图,我们在分析时需要进行切边观察,沿Tab方向切刮掉包装铝箔和Sealant胶,在高倍率放大镜下观察切边Ni tab和包装铝箔铝层的位置情况,下图a为切面观察无短路情况,图b为切面观察发生短路的情况。可作为参考。              图a 图b   以上的是引起腐蚀的第一种情况,下面为引起腐蚀的第二种情况,Ni tab弯折后与顶部截面铝层发生短接。图c所示Ni tab在铝箔上有明显的印痕,图d将Ni tab弯折后测量发生为短路。                   图c 图d 电子短路一旦形成必然会发生腐蚀,因此必须在各过程中控制严防电子短路的发生,工艺、夹具、操作方法规范可避免直接短路的发生,还需要控制电子导电物质的存在,注意顶封前的各工序对隔离膜、阴、阳极、Pocket、Tray、操作台面等partical的预防控制,目前在顶封loading电芯前采用吸尘方式裸电芯和Pocket进行控制。注意卷绕工艺的膜片错位和膜片脱膜掉碳的控制检查。 电阻坏品防止 任何电阻坏品都有发生腐蚀的潜在可能性,对电阻坏品规格的定义是经验上的总结,被Reject的电芯需要进行On-hold(待潜在的腐蚀发生),不能正常出货,增加了成本控制和影响到产品的总体优率。我们知道PP破损导致包装铝箔铝层发生裸露才会导致阳极通过电解液与其发生短路。提高电阻优率可降低发生潜在腐蚀的可能性,也能极大地节约成本(ATL目前日产量近300K),因此必须控制电芯在Top sealing、Side sealing和Degassing三个工艺控制PP的意外受损,也可能需要从设计上进行改善。 目前使用的包装铝箔主要有两种:PFR-001-05和 PFR-002-05,两种厚度不同的包装铝箔是因为PP厚度的不同,PFR-001-05 PP的厚度为40um,PFR-005-05的PP厚度为80um,PP越薄越容易发生破损产生电阻坏品,所以普遍来说使用薄Showa的Model电阻优率一般比厚Showa的要低些。PP破损的原因主要归结以下几个方面(包括控制检查方法): 1.温度过高,封装温度过高,封边Pocket内PP受热辐射影响易被烫伤,产生鼓泡,折边后发生破损。目前对机器温度采用首件测量和On-line monitor的方式进行控制。 2.PP变形率过大,用错Stopper高度的封头或封头磨损、杂质等原因导致封装PP受过度挤压,变形率过大,PP胶堆积在电芯封边内部折边易发生破损。目前采用平行度检查、监控的方式保证封头处于良好状态。 3.封头错位,封头沿宽度方向错位,封装热压时未重合部位直接烫伤PP。目前定期检查封头错位情况。 4.隔离膜划伤,主要表现在P1 Model,该种工艺为叠片方式,隔离膜裸露在电芯两侧,热压封边周围PP受热辐射影响比较软,隔离膜伸到PP将其划伤,由以CD隔离膜和大电芯最最为严重,CD隔离膜萃取后变硬,大电芯Pocket中间部位易发生形变。目前一些Model采用在裸电芯两侧贴短条或长条绿较(根据电芯实际情况和电解液渗透)阻止隔离膜外伸,灵活调整Bi-cell折叠方式,隔离膜比较长的一端放入深坑内,同时控制侧封的未封区宽度,避免隔离膜在封装过程中划伤pocket PP层。 5. 绿胶划伤,为防止P1Model隔离膜两侧外露划伤PP,在Bi-cell两端加贴了绿胶,但经常发生由于绿胶的松动而引起绿胶被封装在封边区域或绿胶边缘划伤PP,因此在贴绿胶工序必须贴紧绿胶,同时灵活地变更方式,绿胶端缘(收尾)不能在Bi-cell侧面,尽量上到电芯实体上。 6. Bi-cell错位,对于叠片工艺的P1Model。Bi-cell一旦发生错位,不仅隔离膜可能损伤PP。甚至集流体会严重地划破PP,因此必须在叠片工序控制Bi-cell的错位情况,尽量使用夹具限位。 7.未封区过小,不考虑切边后实际封装宽度的情况下,未封区(封装区域到电芯主体的距离)越大,PP受隔离膜、绿胶等损伤的机率越小。根据切边宽度和有效封装宽度,将P1Model未封区宽度定义在1.0mm比较合适。虽然M6S工艺和P2工艺的电芯两侧没有隔离膜外露,但也应有适当的未封区域,否侧会受到电芯实体的挤压而造成PP拉伸变薄,电阻会明显降低。 8.电解液影响,电解液是作为导体连接阳极和铝层造成电阻坏品,电解液越少,造成电阻坏品的机率和比例也会越低,电解液越多,电阻坏品也会相应的增加,曾经M6S 383450和P1 451730 等曾经出现过。所以需要对各Model电解液的使用系数进行优化。目前所用的系数不是最优化的条件,由以M6S Model最为严重。 9.Forming 折烫边的影响,在Forming工序共有两种折边方式:单折和双折,电芯厚度比较薄一般低于3.2mm,为保证折边不超厚和有效封装宽度,一般采用双折边方式,其余情况下单折就可以满足正常要求。单折边机器有切、折、烫功能,必须调整好机器加热块的距离,不可过度挤压电芯实体,以免造成封边部位PP的破损,需要对距离进行优化调节;采用双折边工艺的电芯采用的都是薄的包装铝箔,PP厚度只有40um,更加容易破损,所以必须优化调节好滚论的间隙和高度,防止实体封边受到过度挤压造成电阻坏品,对于双折边由于调节不宕,这种情况经常出现并且电阻优率非常低。 产生电阻坏品必是由于某处PP受损导致铝层裸露,众多原因可以归结为两种情况,一是PP被划伤,一是封边内堆积PP发生断裂破损。两种情况可参考下面图片:    这里介绍一种检查PP绝缘不良部位即破损部位的方法,采用电镀的方法。具体操作方法为:① 成型品或做成袋子形状,里面灌入硫酸铜20%水的液体; ② 6V的电源,阳极放入液体中,阴极与包装膜的铝层接触; ③ 通电20分钟-60分钟; ④ 根据铜的表面析出,可找到绝缘不良处。 实施方法可以参考下面模拟图: 成品电芯模拟图 Pocket模拟图 通电反应到一定时间后,会发现在包装铝箔的某些部位有金属铜析出,该部位即为绝缘不良部位,亦PP破损的部位。金属铜析出的情况如图所示:        原始图                放大图 这里介绍一下电阻和腐蚀失效样品的分析方法: 对于电阻坏品,可以采用分别将每一个折边摊平测量Ni tab与铝层电阻的方法,假设单独摊平Degassing边电阻数据没有变化,而单独摊平Side sealing边电阻数据变大,说明电阻坏品是由于Side sealing边PP的破损造成,需要拆开电芯检查Side sealing 边是何种原因造成,再加以改正预防。若摊平两边电阻都没有增大,可以检查顶封封边和切面,同时必须要检查两侧封边是否已经发生严重破损,必要的话检查一下Pocket各部位PP的情况。具体可参考附件的电阻坏品改进分析报告。 对于腐蚀样品,需要先测量Ni tab与包装铝箔铝层间的电阻,在调整万用表档位情况下,电阻若只有几Mohm甚至几Ohm,所明阳极与包装铝箔发生了直接的短路,可观察顶封Ni tab位的封装外观,是否发生压Tab或压槽位或Tab折叠位置等发生异常,并且可以对Ni tab封装部位作横切面分析,在×700显微镜下观察Ni tab与铝层的情况,电阻很低时,一般这两者必定发生了短接,在某点或某个部位PP、Sealant绝缘胶失去保护作用,在这里形成了电子短路;然后再拆开电芯找出腐蚀部位PP的破损证据,即离子短路的证据,找到了离子短路和电阻短路的证据,分析产生的原因加以控制。也可以采用测量Al tab和包装铝箔铝层的电压反应Ni tab与铝层短路的情况,若两Tab间电压为3.8V,而Al tab和铝层的电压在3.0V以上则说明阳极必定与铝层发生了直接短路。还有另外一种情况就是电阻测试没有显示数据很小或显示负数(说明Pocket已经带电),这种情况一般是没有发生硬性的短路,需要拆开电芯先找到腐蚀区域PP破损部位及形成原因(离子通道),同时观察是否有电子导电物质形成电子通道,如阳极是否暴、是否错位严重、是否有碳粉等杂质,也可以对顶封Ni tab部位有无发生轻微短接。不论哪种情况,进行腐蚀分析必须找到离子通道和电子通道。在附属报告里面会附上一份腐蚀分析报告的范本。 4.3 胀气 聚合物锂离子电芯采用的是铝塑复合膜的软包装技术,当电芯内部由于异常化学反应的发生而产生气体时,Pocket会被充起,电芯鼓胀(有轻微鼓胀和严重鼓胀两种情况),且不论外观如何,电芯的使用性能(Capacity、Cycle life、C-rate等)会发生严重的下降,电芯不能使用。胀气会发生在生产过程中也会在客户甚至最终用户手中。当然,电芯在化成激活或Baking过程中会正常的产生一定量(一般很少)的气体,这根据所使用的原材料而异,这种气体在Degassing工序会被抽掉。目前部分Model(一次封装成型电芯)通过添加V18溶剂来消除这种SEI层形成、相界面稳定所产生的气体。 但是由于工序异常所产生的气体在Degassing前表面非常明显或者Degassing后产生不能再消掉或者V18也不能消除。这里简要介绍工序异常产生气体的原因: 1.封装不良,由封装不良所引起胀气电芯的比例已经大大地降低。前面已经介绍了引起Top sealing、Side sealing和Degassing三边封装不良的原因,任何一边封装不良都会导致电芯,表现以Top sealing 和Degassing居多,Top sealing主要是Tab位密封不良,Degassing主要是分层(包括P2 Model受电解液和凝胶影响导致PP与Al脱离)。封装不良引起空气中水分进入电芯内部,引起电解液分解产生气体。 2.Pocket表面破损,电芯在流拉过程中,受到异常损坏或人为破环导致Pocket破损(如针孔)而使水分进入电芯内部。 3.角位破损,由于折边角位铝的特殊变形,气袋晃动会扭曲角位导致Al破损(电芯越大,气袋越大,越易破损),失去对水的阻隔作用。可以在角位加皱纹胶或热熔胶缓解。并且在顶封后的各工序禁止拿气袋移动电芯,更要注意操作方式防止老化板上电芯的摆动。 4.电芯内部水含量超标,前面我们已经介绍过对电芯内水含量有一定的要求,一旦水含量超标,电解液会失效在化成或Degassing后产生气体。造成电池内部水含量超标的原因主要有:电解液水含量超标,Baking后裸电芯水含量超标,干燥房湿度超标。若经FA怀疑水含量超标导致胀气,可进行工序的追溯检查。 5.化成流程异常,错误的化成流程会导致电芯发生胀气。 6.SEI膜不稳定,电芯在容量测试充放电过程中发射功能轻微胀气。 6.过充、过放,由于流程或HK机器或保护板的异常,使电芯被过充至4.5V或过度放电,电芯会发生严重鼓气。 7.短路,由于操作失误导致带电电芯两Tab接触发生短路,电芯会发生鼓气同时电压迅速下降,Tab会被烧黑。 8.内部短路,电芯内部阴阳极短路导致电芯迅速放电发热同时严重鼓气。内部短路的原因有很多种:设计问题;隔离膜收缩、卷曲、破损(ATL隔膜最为严重);Bi-cell错位;毛刺刺穿隔离膜;夹具压力过大;烫边机过度挤压等。例如502030曾经由于宽度紧张,烫边机过度挤压电芯实体导致阴阳极短路胀气。422339早期由于马甲的存在,夹具Baking工序导致隔离膜压破阴阳极短路胀气。 9.腐蚀,电芯发生腐蚀,铝层被反应消耗,失去对水的阻隔作用,发生胀气。 10.真空抽气异常,系统或机器的原因导致真空度异常Degassing抽气不彻底;Vacuum Sealing的热辐射区过大(一般它的热辐射宽度为8mm),导致Degassing抽气刺刀不能有效地刺破Pocket袋而导致抽气不干净。 这里介绍一下胀气电芯的通用分析方法,并附有一些电芯胀气后的气体成分的Database: 1.根就电芯的Barcode了解电芯的日期,是否有生产时期的异常记录(比如干燥房湿度超标、停电等),从DTS查阅电芯出货的基本信息,包括电压、内阻、容量等。 2.测量电压的开路电压、内阻数据,并与出货数据比较,测量它的充放电曲线。 3.检查电芯的外观,是否有Pocket破损、角位破损、封装不良等 4.对电芯内气体进行气相色谱分析,判断气体成分及比重 5.若H2含量过多,可以判断为电芯内水含量超标导致,为包装铝箔失效导致电芯内部 与外界接触或工序过程中电芯水含量超标。                 气相色谱结果分析图   对各种不同条件下电芯内部气体的成分分析统计,通过气相色谱方法分析获得: ① 模拟实验产生气体结果分析 实验电芯:3945135-010D;MI-410;P1工艺 电芯组成:阳极:FAM-03301;阴极:FCM-01540;电解液:E4;隔离膜:FSM-02140; 试验条件: 第1组: 充电至4.33V左右,然后60℃baking至电芯严重鼓胀,然后取出即时做气体分析(在常温停留时间不超过3小时); 第2组: 充电至4.33V左右,然后60℃baking至电芯严重鼓胀,然后取出在常温摆放3天后做气体分析; 第3组: 恒压充电5.0V至电芯鼓胀,然后取出在常温摆放3天后做气体分析; 第4组: 恒压充电5.0V至电芯鼓胀,然后取出在常温摆放7天后做气体分析; 第5组: 取半充满电电芯(3.810V左右)向电芯内注入约0.05g水,密封好后,待电芯鼓胀后做气体分析; 第6组:60ºC&30cycle产生气体的电芯 分析结果: Group H2 CO CH4 CO2 C2H4 C2H6 C3H6 C3H8 C2H2 1 0.07% 14.79% 23.59% 36.53% 0.62% 11.84% 0.72% 11.84% 0.00% 2 0.04% 10.66% 18.48% 48.59% 0.81% 8.29% 0.89% 11.54% 0.19% 3 0.00% 2.76% 8.87% 77.43% 0.12% 6.97% 0.17% 3.58% 0.10% 4 0.00% 1.04% 5.58% 76.35% 0.06% 15.16% 0.82% 0.89% 0.11% 5 10.53% 49.78% 10.53% 1.89% 0.00% 12.77% 14.50% 0.00% 0.00% 6 0.00% 44.62% 24.72% 15.35% 0.129% 15.088% 0.00% 0.00% 0.095% ② 不同模拟条件产生气体 Over discharge Electrolyte Status H2% CO% CH4% CO2% C2H4% C2H2% C2H6% E4 discharge to 0v at RT,E3 7.2 13.0 27.4 49.6 0.1 2.7 0.0 Baking Model Electrolyte Process Status H2% CO% CH4% CO2% C2H4% C2H2% C2H6% C3H6+C3H8% 383450 E6 P3 85°C/4h 0.0 14.3 2.8 79.6 0.46 0.0 2.8 0.0 383450 E2 P3 80C/5days 0.0 42.0 14.4 34.5 1.2 0.1 5.7 2.2 Formation Model E Process Gas H2% CO% CH4% CO2% C2H4% C2H2% C2H6% C3H6% 8235138 E2 P1 Mean 14.8 18.3 6.9 8.3 50.9 0.8     383562(A1) E3 P1 Mean 22.1 14.4 5.8 14.1 43.1 0.5     383450 E4 P1 Mean 39.0 20.2 4.3 1.4 28.7 2.6   4.0 Overcharge E Swelling status H2% CO% CH4% CO2% C2H4% C2H2% C2H6% C3H6% E3 1C charge to 4.8v 0.0 1.5 7.5 88.1 0.5 2.1 0.3 0.0 E3 1C charge to 6v 0.0 4.0 4.9 76.8 1.9 12.0 0.4 0.0 E3 1C charge to 6v 0.0 5.0 5.0 77.2 1.7 10.9 0.2 0.0 ATL-11 1C charge to 5.04V 5.2 4.9 1.4 83.4 2.4 0.3 1.5 1.1 ATL-11 1C charge to 5.04V 3.3 1.6 2.0 83.6 3.1 0.3 4.1 1.9 ATL-11 1C charge to 5.04V 3.2 1.5 1.5 85.4 4.1 0.0 2.2 1.5 ATL-11 1C charge to 5.04V 3.5 5.2 1.5 84.1 2.5 0.3 1.6 1.2 Mean   3.4 3.4 82.7 1.5 E3 60°C baking 36hrs at 4.35v 0.0 5.4 12.0 79.9 0.6 1.8 0.3 0.0 E3 4.35v cycling at 60°C 1.5 6.5 16.4 73.0 0.2 2.2 0.2 0.0 E3 4.35v cycling 224 times at 45°C 6.1 2.9 20.3 66.7 0.1 3.8 0.2 0.0 E3 4.20v@60°C 25cycles 6.0 9.5 36.3 43.5 0.3 4.2 0.1 0.0 E2 4.6v cycling 180 times at RT 1.5 2.5 28.4 62.4 0.3 4.8 0.0 0.0 E2 4.20v@60°C 122cycles 0.0 11.1 23.2 55.9 0.5 9.4 0.0 0.0 Mean   6.33 22.76 63.56 0.14 Storage Model E Status H2% CO% CH4% CO2% C2H4% C2H2% C2H6% C3H6+C3H8% 383562 E4 Storage gas 210days 43.0 1.8 6.8 45.1 0.0 0.0 3.0 0.0 3945135 E4 4.3V baking 15.4 12.6 20.0 31.0 0.5 0.0 10.1 10.7 3945135 E4 4.3V storage 3days at RT 6.1 10.0 17.4 46.0 0.8 0.2 7.8 11.7 3945135 E4 5V storage 3day at RT 0.0 2.8 8.9 77.4 0.1 0.1 7.0 3.7 3945135 E4 5V storage 7day at RT 0.0 1.0 5.6 76.3 0.1 0.1 15.2 1.7 501235 E2 3.8V storage gas 56.0 24.9 1.5 17.2         5080122 E3 Storage gas 0.0 0.4 7.9 89.2 0.2   2.2   413055 E3 FC&RT and half year 0.0 20.0 9.3 68.9 0.2 1.7     413055 E3 DC&RT and half year 0.0 6.0 3.3 89.2 0.1 1.4         0v storage 5days 21.2 4.8 25.8 45.4 0.1 0.0 2.3 0.2 451730 E4 4.2v storage 30days at 60°C 0.0 20.5 13.3 57.9 0.2 0.0 7.8 0.2   E4+V18 4.2v storage 30days at 60°C 0 15.8 8.9 62.8 0.1 0.0 10.6 1.7 Cycle (At room temperature) Model Electrolyte Status H2% CO% CH4% CO2% C2H4% C2H2% C2H6% C3H6+C3H8% 463050 E2 130 cycle gas 0.0 7.6 37.5 39.6 0.4 0.0 9.2 4.6 463050 E2+0.1%V18 130 cycle gas 57.2 2.7 7.2 28.8 0.8 0.1 1.7 1.3 463050 E2+0.2%V18 130 cycle gas 0.0 5.2 13.8 73.0 0.7 0.1 4.1 3.1 463050 E2+1.5%V18 130 cycle gas 0.0 7.9 19.0 63.7 0.6 0.1 6.3 2.4 463050 E2+0.2%V16+0.3%V18 130 cycle gas 0.0 1.7 8.6 82.5 0.6 0.1 3.4 3.1 383555 E4 160 cycle gas 49.6 5.6 29.4 0.0 0.9 0.0 14.0 1.2 463050 E4 130 cycle gas 0.0 4.1 56.6 13.2 0.4 0.0 24.1 1.6 463050 E4+V18-02 130 cycle gas 32.1 1.9 25.5 29.1 0.7 0.0 10.1 0.6 463050 E4+0.5V18 130 cycle gas 0.0 10.4 64.6 0.1 0.6 0.0 23.4 0.8 463050 E4+1.5%V16+0.3%V18 130 cycle gas 0.0 3.8 33.3 51.3 0.3 0.0 10.8 0.6 463050 E4+0.85%V16+1.9%V18 130 cycle gas 1.5 2.9 24.4 59.6 0.0 0.0 10.8 0.8   DMC+salt 30cycles 9.5 86.0 0.0 0.0 0.0 4.4   EMC+salt 30cycles 5.1 78.6 0.0 0.1 0.0 16.0   PC+salt   4.3 0.1 95.9 Cycle (At High temperature 60ºC) Group Electrolyte Additive H2% CO% CH4% CO2% C2H4% C2H2% C2H6% C3H6+C3H8% HP01 E2 0 7.60 37.49 39.58 0.41 9.20 4.608 HP02 E2+V18-01 0.10% 57.23 2.73 7.35 29.49 0.81 0.08 1.69 1.28 HP03 E2+V18-02 0.20% 0.0 5.2 13.8 73.0 0.7 0.1 4.1 3.1 HP06 E2+V18-15 1.50% 0.0 7.9 19.0 63.7 0.6 0.1 6.3 2.4 HP18 E2+V16+V18 0.2%+0.3% 0.0 1.7 8.5 82.5 0.6 0.1 3.4 3.1 HP07 E4 0.0 4.1 56.6 13.2 0.4 0.0 24.1 1.6 HP09 E4+V18-02 0.20% 32.1 1.9 25.5 29.1 0.7 0.0 10.1 0.6 HP10 E4+V18-05 0.50% 0.0 10.4 64.6 0.1 0.6 0.0 23.4 0.8 HP14 E4+V16+V18 1.5%+0.3% 0.0 3.8 33.3 51.3 0.3 0.0 10.8 0.6 HP17 E4+V16+V18 0.85%+1.9% 1.5 2.9 24.4 59.6 0.0 0.0 10.8 0.8 463050 E4(FC130+LiPF6) 120cycles 0.0 23.1 62.0 0.2 0.2 14.6 0.0 5432100 E2 200cycles 0.0 4.2 18.0 49.3 0.3 0.0 15.9 12.3 3945135 E4 65°C/30cycles 0.0 23.4 33.7 20.9 0.2 0.1 20.5 1.1 Mean   7.6 31.1 39.4 11.9 Gas component for corrosion Swelling condition H2% CO% CH4% CO2% C2H4% C2H6% corrosion at edge 93.9 4.2 1.2 0.1 0.015 0.3 corrosion at edge 90.6 5.8 2.2 0.4 0.001 0.9 Gas component for battery with moisture Injecting 0.015g~0.050g H2O into battery Battery E Status H2% CO% CH4% CO2% C2H4% Others 3945135 E4 2.76V 70.7 0.6 18.3 5.7 0.1 4.6 3945135 E4 3.0v 65.0 0.7 16.5 14.0 0.0 3.8 3945135 E4 3.8v 94.6 2.9 0.7 0.2 0.0 1.5 383562 E4 4.1v 71.7 7.5 7.3 6.4 0.04 7.1 Gas component for battery with impurity (HF) Battery No. HF (ppm) H2 (%) CO (%) CH4 (%) CO2 (%) C2H4 (%) C2H6 (%) Others (%) Normal 15 11.1 13.3 13.7 42.5 18.1 1.1 0.2 383562 157 12.2 12.7 13.9 41.0 18.9 1.2 0.2 383562 205 15.7 13.2 13.9 37.6 18.3 1.1 0.0 383562 1224 22.9 12.3 10.2 36.0 17.3 1.1 0.1 ③ 其它参考数据 Gas source Main gas components Name Range storage gas CO2 70~90% FC storage CO2/ CO 70%/20% Overcharge (long time) CO2/ CH4 60~85%/5~15% C2H6 7~12% Overcharge cycling &60°C CO2/ CH4 40~80%/10~40% Over discharge CO2/ CH4/ CO 54%/30%/14% H2O H2/ CO 50~75%/20~40% 4.4顶封起皱、鼓泡   Pocket起皱 顶封工序通常会发现在电芯顶封边或侧封边发生包装铝箔起皱现象,起皱会引起封装PP层间粘结性变差,不能很好的熔合,有封装不良隐患,同时也表现出不良的外观。这里介绍引起顶封边或侧封边产生皱痕的几种原因,并提供行之有效的解决方法。 ①  Pocket成型不良,Pocket冲压成型后电池主体两端出现变形,Pocket深坑和浅坑之间不能完好的重合;或Pocket冲压成型后的深度太浅与电芯的厚度不符,需要对冲模及配件等进行检修,使Pocket符合规格要求。 ② 切边成型后的Pocket搁置时间过长没有进行顶封,可能导致成型后的Pocket发生回弹变形。因此要求必须对Pocket做到及时使用,主要表现在大电池及深坑电池Pocket上。 ③ 顶边Pocket切边宽度过窄,设计尺寸或切刀尺寸有问题。 ④ Pocket坑深度过浅,检查并加深Pocket坑深度到合理尺寸。 ⑤ 顶封Loading电芯时,电芯不平整或顶边Pocket错位,需要纠正操作手势。 ⑥ 顶封夹具的底面与封头的高度相差大,封头过高或着过低都会有产生起皱的问题,需要重新调整该尺寸,通常封头表面和电池的封装表面完全对齐。 ⑦ 顶封夹具压电池压块压在电池表面的力度不均,需要调整或重新设计压块以保证完全压住电池。 ⑧ 上下封头的运动速度不协调也是导致起皱的原因之一。 ⑨ 一些其它原因:TAB折叠位过高;Tab-lead sealant肩宽过宽;隔离膜宽度超宽(非标设计);顶封封头越宽越容易起皱 顶封Pocket鼓泡 顶封封装后出现的靠近电池主体产生的气泡原因分析: 通常顶封封装出现的气泡主要表现为Pocket表面的Nylon层开裂或者产生的气孔,主要原因如下: ① 定位夹具与封头侧面完全接触或着间隙过小,使封头的热量辐射到电池主体边缘,顶封或者侧封离电芯主体的距离太近,或者说电池封装后的未封区尺寸偏小(0.5mm)以下,需要调整封头和顶封夹具间的距离在正常的>0.2mm范围内。 ② Pocket冲压成型中模具的凹模板的所有圆角和平面表面粗糙度差,使得拉伸过程中Nylon层受损,在经过顶封或者侧封高温时Nylon层受到自身的内应力作用而出现开裂。需要对模版重新修整。 ③ Pocket冲压成型中模具的凹模板的所有圆角偏小成型中Nylon层被拉伸严重,需要重新修磨加大凹模板的圆角。 ④ Packing foil受潮或环境湿度过高,冲压成型后对片料进行85℃Baking ⑤ 调整冲压拉伸速度和冲压压力,减缓Nylon层受损。 ⑥ 其它原因:顶封封头调整的高度不合适;调整好高度。 Pocket成型切边不利索(部分扯掉),更换好刀模和盖板报。 5.封装可靠性评估 我们知道包装铝箔的作用是隔绝电芯内部与外部的环境,保证电芯的正常使用性能。由于电芯的使用过程是一个不断的充放电的过程,电芯内部的不断变化和外部的使用环境都会对包装铝箔产生较大的影响。目前正常工艺过程中的包装铝箔可以充分保证电芯使用过程中的密封要求。一旦工序或材料发生异常或变更,根据需要应该对包装铝箔的使用密封性能进行评估,可以有选择地设计模拟实验进行间接的评估。本章节介绍的是变异情况下的实验设计,可供参考。 关于Tab 、Sealant、Tab-lead 材料发生变化,工序发生异常或工艺参数发生变化,可进行以下的实验设计: 1.制作成Tab-lead进行浸泡电解液的测试,方法:尽量使用与电芯相同电解液浸泡,也可使用E2或E4,将Tab-lead浸泡在密闭塑料瓶的电解液中,最好是悬空使用电解液蒸气侵蚀,在85ºC条件下Baking(炉子温度达到设定值后再放入测试物);抗电解液能力即Tab与Sealant分离情况,Ni tab至少在25min以上,Al tab须在24h以上。 2.Tab 封装平行度检查;Sealant与Tab拉力测试;Tab与Packing foil拉力测试。 3. 电解液冲击测试; a. Tab lead 与空Pocket进行顶、侧封后,灌注一定量的电解液,再递加一滴水,最后封口进行85ºC 、4h Baking,检查鼓气后是否发生泄漏,若泄漏是由于内部气体压力冲开还是封装失效。 b. Tab lead与Pocket加电芯进行封装,灌注电解液封口后进行85ºC、4h 夹具Baking,看是否Tab位会发生漏液。 关于包装铝箔出现异常或封装条件、工艺更改,进行以下的实验设计: 1.封装平行度检查,顶封、侧封、Degassing拉力测试。 2.制作成成品电芯,在顶封、Degassing分别留样,同时进行以下几项测试: 3.成品电芯,Degassing工序分层比例、Ni tab与包装铝箔电阻分布情况; 4.成品电芯,满充4.2V,70ºC & 95% RH Storage 48h测试,UL测试标准,检查样品是否泄漏及失效原因; 5.成品电芯,满充4.2V,130ºC & 30min Baking 测试,UL 测试标准,检查样品是否泄漏及失效原因; 6.成品电芯,满充4.2V,45ºC & 7days浸泡测试,剪掉Al tab,清除周边杂质,使用 3M A/B胶水将Al tab完全封住,干燥后放置在水中,检查样品是否泄漏及失效原因; 目前制作成品电芯,主要采用上面所述几种方法进行密封可靠性评估,有必要的话,Tab lead评估也可以采用成品电芯评估的方法。但需要提醒的是作评估必须要有对比,可取正常状态下的产品作为参照样品。附有平行度不良包装铝箔可靠性评估报告。 6.封装平行度判断 包装铝箔的封装平行度是指封装后两层包装铝箔PP的黏结情况,在撕开封装的包装铝箔时不可过快,否则会影响判断效果。包装铝箔平行度最好的情况是撕开封装截面都呈现乳白色,但目前很多的来料封装截面表现非常差,出现大量的点状包装铝箔原色,程度表现不同。现在根据两种包装铝箔平行度的情况进行分级,并对各级别的包装铝箔进行可靠性评估,得到是否可用的结论。 PFR-001-05 判断 Grade A Grade B Comment: Normal PP appearance, Comment: Abnormal situation, some ivory-white PP exist on the two parts of each side PP was taken sides of packing foil fully. to another, also much PP silk appear Grade C Grade D Comment: PP are all on one side, Comment: PP distribution similar None on the other, it is the color as grade C, but it is more rough Of Al layer, PP color is not clear an much points seems has no PP at And it is rough. all. 这四种不同程度的包装铝箔在经过一系列的验证和可靠性测试后(附有评估报告),可以证明Grade D的包装铝箔不能保证密封可靠性,不能用于生产,Grade A为正常材料,Grade B和C可以使用,可以以上面图示情况对包装铝箔来料进行判断。建议是只使用Grade A和Grade B两种情况的材料。 PFR-002-05来料判断 Grade A Grade B Comment: Normal PP appearance, Comment: Abnormal situation, PP ivory-white PP exist on the two appearance has stria. sides of packing foil fully. Grade C Grade D Comment: PP are all on one side Comment: PP distribution similar and none on the other, it is the as grade C, but PP is more rough and color of Al layer PP color is nor much points seems has no PP at all. clear and its surface is rough. 可靠性实验评估证明,Grade B、C 和D可以保证电芯的密封要求并能够用于正常生产,但建议尽量不采用物料D。 7.封装工序FMEA Top sealing Process Vacuum Sealing Process Degassing Process 8. 附 录 附录一 封装厚度与热封强度及绝缘性能的关系(DNP~ND405 VS SHOWA~PFR-001-05),资料由DNP公司提供。 DNP公司测量ATL样品封边各标示位置处的厚度数据及拉力强度 DNP公司对ATL样品和其公司样品进行封装厚度和拉力强度关系分析,方法是采取两封边每片15mm Packing foil的拉力强度。ATL样品封边厚度在下面图示所标示范围内。蓝色线为DNP材料在不同封装厚度情况下的拉力强度和绝缘性能变化趋势;红线为SHOWA材料在不同封装厚度情况下的拉力强度和绝缘性能变化趋势; DNP对于PP绝缘不良位置的分析图示和不良部位PP的断面照片,可以看到PP堆积后有明显的破损,导致电解液的渗透造成电阻坏品。主要表现在Degassing边,可参考下面报告。 ATL样品测分析报告 以下是DNP公司测试ATL提供的样品分析结果及解决对策的总结。 1.结论 · 因过于要求强热封效果,CPP层及周遍挤压过狠。 因D-EL40H与昭和的材料不同,它的CPP层的MFR(树脂的流动性能较好)参数较大。 认为现在的贵司热封条件过强。 · 过于挤压热封时,大量流出来的树脂凝聚在电芯内恻。 · 大量流出来得树脂A的部位里面含有气泡。 · 电芯最后两边折起来的时候,A的部位受力而产生龟裂的概率高。 · 特别是贵司热封时,填充恻(电解液残留的部位的那一侧),因过于挤压热封 导致此部位的绝缘性能明显下降。 测定贵司样品的厚度如下。 样品# ① ② ③ ④ ⑤ ⑥ ⑦ ⑧ ⑨ ⑩ ⑪ #1  174 178 184 181 429 195 434 172 174 174 175 #2 180 182 186 186 401 196 430 160 163 167 169 #3 171 174 178 177 460 209 430 160 163 167 169 · 有可能使用昭和的材料时,因填充部位(⑧-⑪)的热封强度不稳定而需要进行强力的 挤压热封。但D-EL40H则不许要太强的热封条件来进行热封。 2.对策 · 不少的电芯厂家对热封方面有个误解,认为热封时加强力度热封的话,提高热封效果,防止龟裂漏夜现象。 · 但是热封时过于加大压力的话,会导致热封部位变得过薄,流出大量的树脂。 · 过大的热封压力对热封效果产生不好的效果。 · 这也会导致绝缘性能下降。 · 做为对策,建议把热封条件调整弱一点,热封后的厚度尽量贴进上述的理论植。 · 如果使用金属的热封头的话,可尝试调整热封头之间的间隙来控制热封后的厚度。 · 另外DNP公司测定热封后的厚度时,使用的是2㎜φ平面头的千分尺。 因使用的千分尺的头太大或球形的的话,测试厚度不太精确。 DNP公司的热封条件 侧封 0.5Mpa(面压)、190℃、3秒 机耳部位 1.0Mpa(面压)、190℃、3~5秒 面压={ P×(D/2)×(D/2)}÷S P;供给汽缸的气压(Mpa) D;汽缸的缸孔的直径 S;热封的表面面积 (注意)因各公司的热封头的热容量不同,故上述条件仅供参考。 附录二  PFR-001-05使用1.7mm顶封封头可靠性评估报告 附录三 有效封装宽度评估试验 附录四 腐蚀电芯分析报告 附录五 平行度异常包装铝箔评估流程报告 附录六 电阻坏品F030分析报告 附录七 胀气电芯失效分析报告 附录八 Degassing工序能力分析 附录九 Degassing机器真空腔体密封性研究 附录十 Heating loss when sealing research 附录十一 Special Sealing in latter process to eliminate delamination 附录十二 Sealing DOE Nylon Al layer PP Nylon Al layer PP � EMBED Excel.Chart.8 \s ��� � EMBED Excel.Chart.8 \s ��� Dim F Dim K Dim B Dim A Dim C Dim H Dim J Dim G 封印宽度 Dim D DIM:A DIM:B DIM:C 8mm foil 拉力方向 夹具 夹具 � EMBED Excel.Chart.8 \s ��� 控制对象:螺丝松动。 控制要点:在螺丝上面画线或者作标示,此线称为骑缝线,和周围不运动的部件连到一起。只要骑缝线不重合,就是螺丝松动了。 控制对象:仪表正常。 控制要点:液位在绿色区域为正常,落在红色区域为过高或过低。 一般D-EL40H的热封厚度 侧面①~④、⑧~⑪的热封后的厚度为 210~220μm。 机耳部位的⑤、⑦热封后的厚度为 480~500μm。 机耳的总厚度视为300μm。 机耳胶带100μm×2+金属带100μm ⑪ ⑩ ⑨ ⑧ ⑦ ⑥ ⑤ ④ ③ ② ① 适当热封端面 过于挤压热封端面 A ① ② ③ ④ ⑤ ⑥ ⑦ ⑧ ⑨ ⑩ ⑪ ⑫ Lamination strength A B C PAGE 55 ATL Confidential _1208780199.bin _1213777206.xls 图表1 3.3793351857 6.3293141667 1 7.6116088462 1 1 3.3981234714 22.76423 CH4% 31.0863719231 CH4% CH4% 82.6650725429 63.5642891667 CO2% 39.3746138462 CO2% CO2% 1.4786399714 0.1433333333 C2H6% 11.9294546154 C2H6% C2H6% overcharge overcharge+cycle RTcycling 60°C cycling RT storage 60°C storage Gas component vol.% mainly Gas Distribution Summary Background Package model 604396 swelling because of Ni tab leakage after 60º storgae for 60 days.we try to design experiment to improve and satisfy customers Designing Ni tab lead manufacture( Ultrasonic shaking ) information A : Cleanout it with acetone (15mins) for three times ,each using fresh acetone and then baked in the glove box for 90mins. B : Cleanout it with actone for 30mins once, then baked in the glove box for two hours C: Teated Ni tab Evaluation design 1.For three kinds of Ni tab lead , Dipped in the electrolyte steam and 85ºC baking. 2.For A and C , sealing with bare pocket (two Ni tab) and injecting electrolyte(E2+V20)10g,then 85ºC 35hrs baking 3.For current 604396, 85ºC 35hrs baking test. 4.Assembling battery with A and C tab lead (604396),Doing the 85ºC baking test 5.For assembled battery ,Doing the 60ºC&60days test Result & analysis 1. Tab lead dipped in the electrolyte steam (85ºC baking) We observe the sealant separate with Ni tab Tab lead Type Sample size 40mins 1hrs 3hrs 10hrs 24hrs A Three times clean 20 Yes B Twice clean 20 Yes C Treated 20 None None 1(20) None None Remark : For treated Ni tab ,when time past 3hrs, one side of one tab, sealant separate with Ni tab slightly. The failure is because of Ni tab is not treated perfectly Ni tab surface under the X350 microscope Normal Treated 1 Good surface Treated 2 poor surface Summary : From the Group A and B ,A should be cleaned better than B ,they have same anti-electrolyte performace. Treated Ni tab has good anti-electrolyte performance far than A and B ,If treated is not adequately enough , it can not last 24hrs 2. Sealed with bare pocket and injecting electrolyte (E2+V20) Baked under the temperature of 85ºC ,electrolyte weight :10g Electrolyte leakage statistic distribution with baking time Tab lead Type Sample size 14hrs 19hrs 36hrs 82hrs 106hrs 156hrs 296 A Three times clean 18 None 1(18) 4(17) 4(13) 7(9) C Treated 14 None None None None None None None Summary : Sealing Tab with bare pocket(electrolyte),Treated Tab show good performance than normal on anti-electrolyte corrosion 3. 604396 cell with Normal Ni tab baking test(temperature :85ºC) Sample size Primary status Result 14hrs 35hrs 70hrs 82hrs 106hrs 156hrs 11 Fully charge Leakage None None None None None None Swelling None 9(11) All All All takeout one to do the gas analysis bacorde CO,% CH4,% CO2,% C2H4,% C2H2,% C2H6,% C3H6+C3H8,% 25080182472 2.03 2.51 86.45 0.93 0.03 2.01 2.01 record Background Package model 604396 swelling because of Ni tab leakage after 60º storgae for 60 days.we try to design experiment to improve and satisfy customers Designing Ni tab lead manufacture information A : Cleanout it with acetone (15mins) for three times ,each using fresh acetone and then baked in the glove box for 90mins. Our normal Ni tab (On line) cleanout procedure : B : Cleanout it with actone30mins once C: Teated Ni tab Evaluation design 1.For three kinds of Ni tab lead , electrolyte steam 85ºC baking. 2.For A and C , sealing with bare pocket (two ni tab) and injecting electrolyte(E2+V20)10g,then 85ºC 35hrs baking 3.For current 604396, 85ºC 35hrs baking test. 4.Assembling battery with three kinds of tab lead (604396),Doing the 85ºC 35 baking test 5.For assembled battery ,Doing the 60ºC&60days test Result Record 1. For Tab A 40min sealant separate with Tab completelyd start from 11:00 on 28-Oct For Tab B 35min sealant separate with Tab completely For Tab C ,40min no problem, 1hrs no problem ,4hrs no problem, 7hrs no problem 9hrs no problem; 10hrs no problem, 23hrs ,Only 1 piece ,pull strength between sealant and tab become poor ,we can separate them , Other (total 20 pieces no problem , the failure one should has symmetrical treated layer) 2. Start from 20:00 on 28-Oct ,14hrs None leakage ,19hrs Group A one, 35hrs, GroupA has 5 pieces leakage 82 hrs OK 106hrs group A has 9pieces leakage ,C OK 3. Start from 20:00 on 28-Oct,14 hrs 9 pieces of 11 battery swelling and none leakage 35 hrs and 70hrs none electrolyte leaking ,82 hrs OK none leaking 106hrs none leakage but swelling seriously gas analysis Material Amperex Technology Limited RD-Lab Report No: GAS11042 Tel; 86-769-2405338, Ext:1365 Gas Analysis Report Sample name: Battery gas Client : Guo Qingming Submit date: 11/4/05 Vendor No.: Sample Qty: 1 Measured by: Chen YR Background: Battery swelling after formation and baking at 85 °C. Test method: Injected 1ml sample into GC, and split ratio is 50:1. Inlet temperature : 220°C, oven temperature: 29~220°C at 20 °C/min, 220~240°C at 10 °C/min, end. Using TCD detector. Analysis results: 604396Battery bacorde CO,% CH4,% CO2,% C2H4,% C2H2,% C2H6,% C3H6+C3H8,% 25080182472 2.03 2.51 86.45 0.93 0.03 2.01 2.01 Tested by: Chen YiRong Approved by: 11/5/05 Date: 11/4/05 Date: JL _1209299049.xls 图表1 30.9 28 28.8 31 28 28.9 31 28 29.2 31 28 73.5 31.1 28 117.9 31.2 28.1 135 31.3 28.2 145.2 31.5 28.2 151.2 31.6 28.2 154.9 31.8 28.3 157.2 31.9 28.3 158.8 32 28.4 159.9 32.1 28.3 160.6 32.3 28.4 161.1 32.4 28.4 161.7 32.5 28.5 162.1 32.5 28.5 162.4 32.6 28.5 162.6 32.7 28.5 162.8 32.7 29.6 163 32.7 28.9 163.1 32.8 97.4 163.1 33.1 126 163.2 33.8 143 163.3 35.1 153 161.4 36.7 159 152 38.4 162 143.3 40.3 164 135.5 42.2 166 128.7 51.7 167 122.6 116 168 116.6 141.5 168 111.5 155.6 169 106.7 162.1 169 102.2 165.6 169 97.9 167.7 170 93.8 169 170 90.1 169.9 170 86.6 170.4 170 83.3 170.8 170 80.4 171.2 170 77.7 171.4 170 75.2 171.6 162 73.1 171.7 154 71.3 171.8 147 69.6 171.9 141 68 172 135 66.5 172 129 65 172 124 63.5 172.1 119 61.9 172.1 114 60.3 172.1 110 58.8 172.1 106 57.4 172.1 102 56.1 172.1 97.7 54.9 172.1 94.2 53.7 172.1 90.8 52.5 172.1 87.6 51.5 172.1 84.6 50.4 172.1 81.8 49.5 172.1 79.2 48.6 172.1 76.8 47.8 172.1 74.7 47.1 172.1 72.9 46.3 172.1 71.2 45.7 172.1 69.6 45.1 172 68.1 44.4 172 66.6 43.8 172 65.1 43.2 172 63.6 42.7 172 62 42.2 172 60.4 41.6 172 58.9 41.2 172 57.5 40.8 172 56.1 40.3 172 54.9 39.9 172 53.8 39.5 172 52.6 39.1 172 51.6 38.7 171.9 50.7 38.4 172 49.8 38 171.9 49 37.7 171.9 48.2 37.3 171.9 47.4 37 171.9 46.6 36.8 171.9 46 36.6 171.9 45.3 36.3 171.9 44.7 36.1 171.9 44 35.8 171.9 43.4 35.7 171.9 43 35.5 171.9 42.4 35.3 171.9 41.9 35.2 171.8 41.5 35 171.9 41 34.9 171.9 40.7 34.8 171.8 40.4 34.6 171.8 40.2 34.5 171.9 39.9 34.4 171.8 39.5 34.3 171.8 39.2 34.2 171.8 38.9 34 171.8 38.7 33.9 171.8 38.4 33.8 171.8 38.2 33.7 171.8 38 33.6 171.8 37.8 33.5 171.8 37.7 33.5 171.8 12.6 33.4 171.8 12.7 33.3 171.7 12.8 33.2 171.8 12.9 33.2 171.8 13 33.1 171.8 13.1 33 171.8 13.2 32.9 171.7 13.3 32.9 171.7 13.4 32.8 171.8 13.5 32.7 171.7 13.6 32.7 171.8 13.7 32.6 171.8 13.8 32.6 171.8 13.9 32.5 172.9 14 32.5 163.8 14.1 32.4 157.4 14.2 14.2 151.8 14.3 14.3 146.4 14.4 14.4 141.2 14.5 14.5 136.2 14.6 14.6 131.5 14.7 14.7 127.1 14.8 14.8 122.9 14.9 14.9 119 15 15 115.3 15.1 15.1 111.8 15.2 15.2 108.5 15.3 15.3 105.4 15.4 15.4 102.4 15.5 15.5 99.6 15.6 15.6 96.9 15.7 15.7 94.5 15.8 15.8 92.2 15.9 15.9 90 16 16 87.8 16.1 16.1 85.9 16.2 16.2 84 16.3 16.3 82.3 16.4 16.4 80.7 16.5 16.5 79.3 16.6 16.6 78.1 16.7 16.7 77 16.8 16.8 75.9 16.9 16.9 74.9 17 17 73.9 17.1 17.1 72.8 17.2 17.2 71.7 17.3 17.3 70.5 17.4 17.4 69.3 17.5 17.5 68.2 17.6 17.6 67.1 17.7 17.7 180-3 180 2s 175 2s Sheet1 180-1 180-2 180-3 175-1 175-2 180 2s 175 2s 1.8 32.60 32.6 30.9 29 29.5 28 28.8 1.9 32.60 32.6 31 29.2 29.6 28 28.9 2 32.50 32.5 31 29.4 29.7 28 29.2 2.1 32.30 32.3 31 29.5 29.9 28 73.5 2.2 32.00 32 31.1 29.6 29.9 28 117.9 2.3 31.80 31.8 31.2 29.8 30 28.1 135 2.4 31.50 31.5 31.3 29.8 30.1 28.2 145.2 2.5 31.30 31.3 31.5 29.9 30.1 28.2 151.2 2.6 31.30 31.3 31.6 30 30.1 28.2 154.9 2.7 31.10 31.1 31.8 30 30.2 28.3 157.2 2.8 31.00 31 31.9 30.1 30.2 28.3 158.8 2.9 30.90 30.9 32 30.2 30.2 28.4 159.9 3 30.90 30.9 32.1 30.3 30.6 28.3 160.6 3.1 30.90 30.9 32.3 30.4 31.2 28.4 161.1 3.2 30.80 30.8 32.4 30.5 32 28.4 161.7 3.3 30.80 30.8 32.5 30.6 32.9 28.5 162.1 3.4 30.90 30.9 32.5 30.7 33.9 28.5 162.4 3.5 31.00 31 32.6 30.7 34.9 28.5 162.6 3.6 31.00 31 32.7 31.2 35.9 28.5 162.8 3.7 31.10 31.1 32.7 32.1 37 29.6 163 3.8 31.10 31.1 32.7 33.3 103.6 28.9 163.1 3.9 31.00 31 32.8 34.5 132.4 97.4 163.1 4 31.00 31 33.1 35.8 147 126 163.2 4.1 30.90 30.9 33.8 37.1 155.8 143 163.3 4.2 30.90 30.9 35.1 38.4 160.8 153 161.4 4.3 30.90 30.9 36.7 39.6 163.8 159 152 4.4 30.80 30.8 38.4 41 165.7 162 143.3 4.5 30.70 30.7 40.3 42.1 166.9 164 135.5 4.6 30.70 30.7 42.2 43.2 167.8 166 128.7 4.7 30.70 30.7 51.7 44.2 168.3 167 122.6 4.8 30.80 30.8 116 46 168.7 168 116.6 4.9 33.00 33 141.5 109.1 169.1 168 111.5 5 34.60 34.6 155.6 133.7 169.3 169 106.7 5.1 38.00 38 162.1 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131.5 14.7 14.7 127.1 14.8 14.8 122.9 14.9 14.9 119 15 15 115.3 15.1 15.1 111.8 15.2 15.2 108.5 15.3 15.3 105.4 15.4 15.4 102.4 15.5 15.5 99.6 15.6 15.6 96.9 15.7 15.7 94.5 15.8 15.8 92.2 15.9 15.9 90 16 16 87.8 16.1 16.1 85.9 16.2 16.2 84 16.3 16.3 82.3 16.4 16.4 80.7 16.5 16.5 79.3 16.6 16.6 78.1 16.7 16.7 77 16.8 16.8 75.9 16.9 16.9 74.9 17 17 73.9 17.1 17.1 72.8 17.2 17.2 71.7 17.3 17.3 70.5 17.4 17.4 69.3 17.5 17.5 68.2 17.6 17.6 67.1 17.7 17.7 180-3 180 2s 175 2s _1209376374.xls 图表2 34.7 40.6 46.8 52.6 57.3 62.4 66.2 69.7 72.7 75.4 77.3 79.3 81.2 82.9 84.4 85.9 87.3 88.6 89.8 90.9 91.9 92.7 93.6 94.4 95.2 95.8 96.5 97.2 97.7 98.3 98.8 99.2 99.7 100.1 100.5 100.8 101 101.3 101.6 101.9 102 102.3 102.5 102.6 102.7 102.9 103 103.1 103.3 103.4 114.5 125.8 132.5 137.8 142.9 147.1 150.5 153.2 155.3 157.2 158.8 160.1 161 162.2 163.3 164.2 165.3 165.9 166.1 166.4 166.6 166.8 167.3 167.4 167.4 167.5 167.6 167.8 167.8 167.9 167.9 167.9 167.9 167.9 167.9 168 168 168 168.1 168 168 168 168 168 167.9 167.9 167.9 168 168 168 168 168 167.9 167.9 167.8 167.8 167.8 167.8 167.8 167.8 162.5 154.9 150.3 146.6 143.8 140.4 137.2 134.8 132.9 131.2 125 119.1 113.4 108.7 104.9 Sealing stage Vacuum stage CH3 Degassing temperature trend Sheet4 1 2 3 501235 Sheet1 With teflon 200ºC time CH1 CH2 CH3 CH4 time CH1 CH2 CH3 CH4 0.1 34.7 33.6 34.7 28.4 0.1 37.6 38.0 39.7 27.8 0.2 37.3 37.6 40.6 28.4 0.2 55.8 46.8 69.3 27.8 0.3 40.3 42.3 46.8 28.4 0.3 67.0 60.3 79.1 27.9 0.4 43.8 46.7 52.6 28.3 0.4 73.8 67.9 84.2 27.8 0.5 46.7 50.4 57.3 28.3 0.5 78.6 72.5 88.7 27.8 0.6 49.7 53.5 62.4 28.4 0.6 82.1 76.8 92.7 27.8 0.7 51.9 56.3 66.2 28.4 0.7 84.8 80.2 95.8 27.8 0.8 54.2 58.9 69.7 28.4 0.8 87.2 83.0 98.6 27.8 0.9 56.1 61.2 72.7 28.3 0.9 89.3 85.1 100.8 27.8 1.0 57.9 63.3 75.4 28.4 1.0 91.2 87.2 102.7 27.8 1.1 60.1 65.3 77.3 28.3 1.1 93.0 87.2 104.6 27.9 1.2 61.5 66.8 79.3 28.3 1.2 94.4 88.8 106.3 27.9 1.3 62.8 68.1 81.2 28.3 1.3 95.7 90.5 107.7 27.9 1.4 64.1 69.5 82.9 28.2 1.4 96.9 91.8 109.1 27.9 1.5 65.3 70.8 84.4 28.2 1.5 98.0 93.2 110.2 27.9 1.6 66.3 72.0 85.9 28.2 1.6 99.0 94.4 111.2 27.9 1.7 67.2 73.2 87.3 28.2 1.7 99.9 95.4 112.2 27.9 1.8 68.2 74.3 88.6 28.2 1.8 100.8 96.1 113.0 27.9 1.9 69.0 75.3 89.8 28.2 1.9 101.5 96.9 113.7 27.9 2.0 69.9 76.3 90.9 28.2 2.0 102.1 97.5 114.5 27.9 2.1 70.6 77.2 91.9 28.1 2.1 102.7 98.2 115.0 27.9 2.2 71.2 78.0 92.7 28.1 2.2 103.1 99.0 115.6 27.9 2.3 71.9 78.7 93.6 28.1 2.3 103.6 99.3 116.2 27.9 2.4 72.6 79.5 94.4 28.1 2.4 104.0 99.7 116.6 27.9 2.5 73.1 80.1 95.2 28.1 2.5 104.5 99.9 117.1 27.9 2.6 73.7 80.7 95.8 28.2 2.6 104.9 100.5 117.5 27.9 2.7 74.1 81.3 96.5 28.2 2.7 105.3 100.8 118.0 27.9 2.8 74.6 81.8 97.2 28.3 2.8 105.6 101.4 118.5 27.9 2.9 75.0 82.3 97.7 28.3 2.9 105.9 101.7 118.8 27.9 3.0 75.4 82.7 98.3 28.3 3.0 106.2 102.0 119.2 27.9 3.1 75.9 83.1 98.8 28.3 3.1 106.5 102.2 119.5 28.0 3.2 76.2 83.6 99.2 28.3 3.2 106.7 102.5 119.8 27.9 3.3 76.6 83.9 99.7 28.3 3.3 107.0 102.8 120.0 27.9 3.4 76.9 84.2 100.1 28.2 3.4 107.2 103.1 120.2 27.9 3.5 77.3 84.5 100.5 28.2 3.5 107.3 103.3 120.4 27.9 3.6 77.6 84.8 100.8 28.2 3.6 107.5 103.5 120.5 27.9 3.7 77.9 85.1 101.0 28.2 3.7 107.6 103.6 120.6 27.9 3.8 78.1 85.4 101.3 28.2 3.8 107.7 103.7 120.7 27.9 3.9 78.4 85.6 101.6 28.2 3.9 107.8 103.9 120.8 27.9 4.0 78.6 85.8 101.9 28.1 4.0 107.9 104.0 120.9 27.9 4.1 78.8 86.0 102.0 28.1 4.1 108.0 104.0 121.0 27.9 4.2 79.1 86.2 102.3 28.0 4.2 108.1 104.2 121.1 27.9 4.3 79.3 86.4 102.5 28.0 4.3 108.1 104.2 121.2 27.9 4.4 79.4 86.6 102.6 28.0 4.4 108.2 104.3 121.2 27.9 4.5 79.5 86.7 102.7 28.0 4.5 108.3 104.4 121.3 27.9 4.6 79.7 86.9 102.9 28.0 4.6 108.3 104.4 121.3 27.9 4.7 79.9 87.0 103.0 28.0 4.7 108.3 104.5 121.3 27.9 4.8 80.1 87.2 103.1 28.1 4.8 108.5 104.5 121.4 27.9 4.9 80.2 87.3 103.3 28.2 4.9 108.5 104.6 121.5 27.8 5.0 80.3 87.4 103.4 28.2 5.0 108.5 104.7 121.6 27.9 5.1 90.1 89.1 114.5 28.2 5.1 121.0 119.7 137.8 27.8 5.2 102.4 96.2 125.8 28.2 5.2 131.3 129.6 146.1 27.8 5.3 110.4 101.8 132.5 28.2 5.3 136.4 133.7 150.4 27.8 5.4 117.2 106.0 137.8 28.3 5.4 139.0 138.2 153.6 27.8 5.5 122.3 110.3 142.9 28.3 5.5 141.1 141.9 156.0 27.8 5.6 126.2 113.9 147.1 28.3 5.6 143.1 145.3 157.8 27.9 5.7 128.4 118.6 150.5 28.3 5.7 144.9 149.9 159.2 27.9 5.8 130.9 122.6 153.2 28.4 5.8 145.9 153.3 160.3 27.9 5.9 133.1 126.2 155.3 28.4 5.9 146.7 161.8 161.3 27.9 6.0 135.0 129.3 157.2 28.3 6.0 147.7 162.0 162.0 27.8 6.1 136.9 131.9 158.8 28.4 6.1 148.8 162.0 162.6 27.9 6.2 138.4 134.2 160.1 28.5 6.2 149.6 162.1 163.2 27.8 6.3 139.7 137.0 161.0 28.5 6.3 150.5 162.3 163.7 27.8 6.4 141.4 139.4 162.2 28.5 6.4 151.3 162.5 164.0 27.8 6.5 143.0 140.9 163.3 28.4 6.5 151.8 162.6 164.3 27.8 6.6 144.8 142.1 164.2 28.3 6.6 152.2 162.6 164.6 27.8 6.7 146.2 143.3 165.3 28.3 6.7 152.5 162.6 164.9 27.8 6.8 147.4 144.4 165.9 28.3 6.8 152.8 162.6 165.1 27.9 6.9 148.1 145.0 166.1 28.4 6.9 153.1 162.6 165.4 27.9 7.0 148.7 145.5 166.4 28.3 7.0 153.3 162.6 165.6 27.9 7.1 149.2 145.8 166.6 28.3 7.1 153.4 162.6 165.7 27.9 7.2 149.8 146.1 166.8 28.4 7.2 153.6 162.7 165.9 27.8 7.3 150.2 146.3 167.3 28.3 7.3 153.8 162.8 166.0 27.9 7.4 150.8 146.7 167.4 28.2 7.4 153.9 162.8 166.1 27.8 7.5 151.3 147.0 167.4 28.4 7.5 154.0 162.9 166.3 27.8 7.6 151.4 147.5 167.5 28.3 7.6 154.0 163.0 166.4 27.9 7.7 151.6 148.0 167.6 28.3 7.7 154.0 163.0 166.4 27.9 7.8 151.8 148.4 167.8 28.3 7.8 154.0 163.1 166.6 27.9 7.9 151.9 148.7 167.8 28.5 7.9 154.0 163.0 166.6 27.9 8.0 152.1 148.9 167.9 28.5 8.0 154.1 163.1 166.7 27.9 8.1 152.2 149.1 167.9 28.5 8.1 154.1 163.1 166.8 27.9 8.2 152.2 149.2 167.9 28.5 8.2 154.2 163.1 166.8 27.9 8.3 152.3 149.3 167.9 28.6 8.3 154.3 163.2 166.9 27.8 8.4 152.3 149.5 167.9 28.7 8.4 154.3 163.1 166.9 27.9 8.5 152.4 149.6 167.9 28.7 8.5 154.3 163.1 166.9 27.8 8.6 152.4 149.8 168.0 28.7 8.6 154.5 163.2 167.0 27.8 8.7 152.5 149.8 168.0 28.7 8.7 154.5 163.2 167.1 27.8 8.8 152.6 149.9 168.0 28.7 8.8 154.6 163.3 167.1 27.9 8.9 152.6 150.0 168.1 28.7 8.9 154.6 163.3 167.1 27.9 9.0 152.6 150.0 168.0 28.7 9.0 154.7 163.3 167.1 27.9 9.1 152.6 150.1 168.0 28.7 9.1 154.7 163.5 167.1 27.8 9.2 152.7 150.1 168.0 28.6 9.2 154.7 163.5 167.1 27.9 9.3 152.6 150.2 168.0 28.6 9.3 154.8 163.5 167.2 27.9 9.4 152.7 150.2 168.0 28.6 9.4 154.9 163.5 167.2 27.9 9.5 152.7 150.2 167.9 28.7 9.5 154.9 163.5 167.2 27.9 9.6 152.7 150.2 167.9 28.7 9.6 154.9 163.5 167.2 27.9 9.7 152.7 150.3 167.9 28.7 9.7 155.0 163.5 167.2 27.9 9.8 152.7 150.3 168.0 28.7 9.8 155.0 163.5 167.2 27.9 9.9 152.7 150.3 168.0 28.6 9.9 155.1 163.5 167.2 27.9 10.0 152.7 150.3 168.0 28.6 10.0 155.0 163.5 167.2 27.8 10.1 152.8 150.3 168.0 28.5 10.1 155.1 163.5 167.2 27.8 10.2 152.8 150.3 168.0 28.5 10.2 155.1 163.5 167.2 27.8 10.3 152.8 150.3 167.9 28.5 10.3 155.1 163.5 167.2 27.7 10.4 152.8 150.4 167.9 28.5 10.4 155.2 163.5 167.3 27.8 10.5 152.8 150.4 167.8 28.5 10.5 155.2 163.6 167.3 27.8 10.6 152.8 150.4 167.8 28.5 10.6 155.2 163.6 167.3 27.8 10.7 152.8 150.4 167.8 28.5 10.7 155.3 163.6 167.3 27.8 10.8 152.8 150.3 167.8 28.4 10.8 155.3 163.6 167.3 27.8 10.9 152.8 150.4 167.8 28.4 10.9 155.3 163.5 167.3 27.7 11.0 152.8 150.4 167.8 28.4 11.0 155.3 163.5 167.3 27.7 11.1 151.8 145.8 162.5 28.4 11.1 151.2 149.5 161.4 27.8 11.2 145.8 141.6 154.9 28.4 11.2 144.8 145.7 154.8 27.7 11.3 141.5 137.7 150.3 28.4 11.3 140.4 142.0 150.2 27.7 11.4 138.1 134.3 146.6 28.4 11.4 136.8 138.5 146.8 27.7 11.5 135.0 131.4 143.8 28.3 11.5 133.9 135.4 143.6 27.7 11.6 132.2 128.6 140.4 28.4 11.6 131.0 131.4 140.0 27.7 11.7 129.7 126.1 137.2 28.4 11.7 128.4 128.7 137.2 27.7 11.8 127.6 123.9 134.8 28.5 11.8 126.3 126.5 134.7 27.7 11.9 125.7 121.9 132.9 28.5 11.9 124.4 124.5 132.8 27.7 12.0 124.1 120.1 131.2 28.6 12.0 122.7 122.9 131.0 27.7 12.1 119.8 117.9 125.0 28.6 12.1 118.5 119.5 125.2 27.6 12.2 114.5 114.2 119.1 28.6 12.2 113.8 114.1 119.2 27.6 12.3 109.7 109.7 113.4 28.5 12.3 109.2 109.5 113.7 27.6 12.4 105.8 105.8 108.7 28.5 12.4 105.5 105.7 109.3 27.6 12.5 102.3 102.4 104.9 28.6 12.5 102.3 102.4 105.9 27.6 12.6 99.5 99.3 102.9 27.6 12.7 97.2 96.6 100.4 27.6 Sheet1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Sealing stage CH3 Degassing temperature trend Sheet2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 CH1 CH2 CH3 Sheet3 With teflon 200ºC TIME "CH1" "CH2" "CH3" "CH4" 333.4 47.6 42.7 39.5 28.0 333.5 56.0 51.2 45.0 28.0 333.6 61.9 58.5 50.8 28.0 333.7 66.7 64.7 55.9 28.1 333.8 68.8 68.2 60.0 28.0 333.9 71.7 72.4 63.5 28.1 334.0 75.1 75.9 66.8 28.0 334.1 77.9 79.1 69.9 28.0 334.2 80.4 82.2 72.9 28.0 334.3 77.4 83.9 76.0 28.1 334.4 77.9 86.1 78.4 28.1 334.5 79.3 88.1 80.8 28.0 334.6 81.1 90.0 83.1 28.1 334.7 82.2 91.7 85.2 28.0 334.8 84.3 93.4 87.1 28.0 334.9 86.3 94.8 88.9 28.0 335.0 88.3 96.2 90.6 28.0 335.1 90.1 97.5 92.1 28.0 335.2 91.3 98.7 93.6 28.0 335.3 91.9 99.7 94.8 28.0 335.4 92.5 100.7 95.9 28.0 335.5 93.5 101.6 97.1 28.1 335.6 94.4 102.4 98.1 28.0 335.7 95.2 103.2 99.1 28.1 335.8 95.7 103.8 100.0 28.1 335.9 96.3 104.5 100.8 28.1 336.0 96.7 105.0 101.5 28.1 336.1 97.2 105.5 102.2 28.1 336.2 97.5 106.0 102.8 28.1 336.3 98.0 106.5 103.4 28.1 336.4 98.4 106.9 104.0 28.1 336.5 98.8 107.2 104.5 28.1 336.6 99.0 107.5 105.0 28.1 336.7 99.4 107.8 105.4 28.1 336.8 99.6 108.0 105.8 28.1 336.9 100.0 108.3 106.2 28.1 337.0 100.2 108.6 106.5 28.1 337.1 100.6 108.8 106.8 28.1 337.2 100.8 109.0 107.2 28.2 337.3 101.0 109.2 107.4 28.2 337.4 101.3 109.4 107.7 28.1 337.5 101.5 109.5 107.9 28.2 337.6 101.7 109.7 108.1 28.2 337.7 102.1 109.9 108.3 28.2 337.8 102.4 110.0 108.5 28.1 337.9 102.7 110.2 108.7 28.1 338.0 102.9 110.3 108.8 28.1 338.1 103.0 110.4 109.0 28.2 338.2 103.2 110.5 109.2 28.2 338.3 107.4 108.3 113.8 28.1 338.4 118.6 115.0 130.3 28.1 338.5 125.0 119.6 139.2 28.1 338.6 129.8 123.7 144.6 28.1 338.7 134.3 127.7 149.6 28.1 338.8 139.1 131.0 153.7 28.1 338.9 144.0 133.8 158.5 28.1 339.0 148.3 136.7 160.9 28.1 339.1 151.7 139.5 162.5 28.1 339.2 154.4 143.0 163.6 28.0 339.3 156.4 145.5 164.7 28.0 339.4 158.6 147.1 165.6 28.0 339.5 160.5 148.3 166.3 28.0 339.6 161.6 149.3 167.0 28.0 339.7 162.7 150.2 167.4 28.0 339.8 163.2 151.0 167.7 28.0 339.9 163.7 151.5 168.0 28.0 340.0 164.2 151.9 168.0 28.0 340.1 164.5 152.1 168.1 28.0 340.2 165.0 152.4 168.1 28.1 340.3 165.3 152.6 168.1 28.0 340.4 165.6 152.8 168.1 28.0 340.5 165.9 153.0 168.1 28.1 340.6 166.1 153.1 168.1 28.1 340.7 166.4 153.3 168.3 28.0 340.8 166.5 153.4 168.3 28.0 340.9 166.7 153.5 168.5 28.0 341.0 166.9 153.6 168.6 28.0 341.1 167.0 153.6 168.5 28.0 341.2 167.1 153.6 168.5 28.0 341.3 167.2 153.6 168.5 28.0 341.4 167.2 153.6 168.6 28.0 341.5 167.3 153.7 168.6 28.0 341.6 167.4 153.8 168.6 28.0 341.7 167.5 153.8 168.6 28.0 341.8 167.5 153.9 168.6 28.0 341.9 167.6 154.0 168.6 28.0 342.0 167.6 154.0 168.7 28.0 342.1 167.7 154.1 168.7 28.0 342.2 167.7 154.1 168.7 28.0 342.3 167.8 154.1 168.7 28.0 342.4 167.9 154.1 168.7 28.0 342.5 168.0 154.2 168.8 28.0 342.6 168.0 154.2 168.8 28.0 342.7 168.1 154.3 168.8 28.0 342.8 168.1 154.3 168.8 28.0 342.9 168.1 154.3 168.8 28.0 343.0 168.1 154.3 168.8 28.0 343.1 168.1 154.3 168.8 28.0 343.2 168.2 154.3 168.9 28.0 343.3 168.2 154.3 168.9 28.0 343.4 168.2 154.4 168.8 28.0 343.5 168.2 154.3 168.9 28.0 343.6 168.3 154.4 168.8 28.0 343.7 168.2 154.4 168.9 28.0 343.8 168.3 154.4 168.9 28.0 343.9 168.3 154.4 168.9 28.0 344.0 168.3 154.4 168.9 28.0 344.1 168.3 154.4 168.9 28.0 344.2 168.3 154.4 168.9 28.0 344.3 166.2 154.5 164.2 28.1 344.4 156.4 147.8 155.8 28.0 344.5 150.8 142.8 151.0 28.1 344.6 146.8 139.3 147.9 28.1 344.7 143.3 136.8 144.9 28.1 344.8 140.0 134.1 142.3 28.1 344.9 136.9 132.0 139.2 28.1 345.0 134.4 130.0 137.1 28.0 345.1 132.1 128.2 135.2 28.0 345.2 130.4 126.7 133.6 28.1 345.3 127.1 123.2 128.3 28.1 345.4 120.0 116.1 121.2 28.1 345.5 114.4 110.0 113.3 28.1 345.6 109.9 105.7 108.4 28.1 345.7 106.0 102.0 104.4 28.1 345.8 102.8 98.8 101.1 28.1 345.9 100.2 96.1 98.3 28.1 346.0 97.9 93.8 95.8 28.1 346.1 96.0 91.7 93.7 28.1 346.2 94.2 89.9 91.8 28.1 346.3 92.7 88.3 90.2 28.1 346.4 91.3 86.9 88.7 28.0 346.5 89.9 85.6 87.3 28.1 346.6 88.7 84.5 86.1 28.1 346.7 87.8 83.4 85.1 28.1 346.8 86.9 82.6 84.2 28.1 346.9 86.2 81.7 83.4 28.1 347.0 85.4 80.8 82.4 28.1 347.1 84.6 80.0 81.6 28.1 347.2 83.9 79.1 80.7 28.1 347.3 83.1 78.2 79.9 28.1 347.4 82.3 77.4 79.1 28.1 347.5 81.5 76.7 78.4 28.1 347.6 80.7 75.9 77.6 28.1 Vacuum stage Sheet3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 "CH1" "CH2" "CH3" No teflon 180ºC TIME "CH1" "CH2" "CH3" "CH4" TIME "CH1" "CH2" "CH3" "CH4" 0.1 37.5 39.9 36.8 28.8 0.1 41.6 41.6 41.1 29.2 0.2 42.5 45.2 41.2 28.8 0.2 41.8 41.9 41.4 29.3 0.3 47.8 50.4 46.2 28.6 0.3 42.0 42.1 41.6 29.2 0.4 52.4 54.9 50.8 28.7 0.4 42.6 43.1 42.6 29.2 0.5 55.5 58.5 55.0 28.8 0.5 65.2 72.3 58.9 29.1 0.6 58.7 63.1 59.0 28.9 0.6 84.4 88.6 29.3 0.7 61.3 67.4 62.4 28.8 0.7 95.0 96.3 29.4 0.8 63.6 71.1 65.4 28.8 0.8 100.9 102.0 29.3 0.9 65.9 74.5 68.1 28.9 0.9 104.1 107.4 29.4 1.0 67.9 77.5 70.7 28.9 1.0 104.5 109.7 29.3 1.1 71.8 79.7 72.8 29.0 1.1 106.3 111.6 29.3 1.2 73.3 82.1 74.8 29.1 1.2 107.9 112.8 29.3 1.3 74.6 84.2 76.5 29.1 1.3 109.3 114.1 29.3 1.4 75.9 86.3 78.4 29.0 1.4 110.6 115.3 29.3 1.5 77.4 88.1 80.0 29.2 1.5 111.0 116.6 29.3 1.6 78.8 89.8 81.5 29.1 1.6 112.0 117.8 29.3 1.7 80.1 91.4 82.8 29.2 1.7 113.0 118.9 29.3 1.8 81.8 92.8 83.9 29.1 1.8 113.7 120.0 29.3 1.9 82.7 94.1 85.1 29.0 1.9 114.5 121.1 29.3 2.0 83.5 95.3 86.0 28.9 2.0 115.1 121.5 29.3 2.1 84.5 96.4 86.9 28.9 2.1 115.7 122.3 29.4 2.2 85.5 97.3 87.9 28.9 2.2 116.2 122.8 29.4 2.3 86.2 98.3 88.8 28.8 2.3 116.6 123.2 29.3 2.4 87.0 99.1 89.6 28.8 2.4 117.0 123.7 29.3 2.5 87.6 99.9 90.4 28.8 2.5 117.4 124.0 29.3 2.6 88.3 100.5 91.0 28.8 2.6 117.7 124.3 29.3 2.7 88.9 101.2 91.6 28.8 2.7 118.0 124.5 29.4 2.8 89.6 101.8 92.2 28.7 2.8 118.2 124.7 29.4 2.9 90.3 102.4 92.7 28.8 2.9 118.5 124.9 29.4 3.0 90.9 102.8 93.2 28.7 3.0 118.6 125.0 29.4 3.1 91.4 103.3 93.6 28.7 3.1 118.8 125.2 29.5 3.2 92.0 103.7 94.1 28.7 3.2 119.1 125.3 29.5 3.3 92.3 104.1 94.5 28.7 3.3 119.2 125.3 29.5 3.4 92.7 104.5 94.8 28.7 3.4 119.3 125.4 29.5 3.5 92.9 104.8 95.1 28.6 3.5 119.4 125.4 29.5 3.6 93.2 105.2 95.4 28.7 3.6 119.5 125.5 29.5 3.7 93.6 105.5 95.7 28.7 3.7 119.6 125.5 29.5 3.8 93.8 105.8 95.9 28.6 3.8 119.7 125.5 29.5 3.9 94.1 106.0 96.2 28.6 3.9 119.8 125.6 29.5 4.0 94.3 106.2 96.3 28.6 4.0 119.8 125.6 29.5 4.1 94.4 106.4 96.4 28.5 4.1 119.9 125.6 29.5 4.2 94.6 106.6 96.5 28.6 4.2 120.0 125.6 29.5 4.3 94.6 106.9 96.7 28.5 4.3 120.1 125.7 29.5 4.4 94.7 107.1 96.9 28.5 4.4 120.1 125.6 29.5 4.5 94.9 107.2 97.0 28.5 4.5 120.1 125.7 29.5 4.6 95.0 107.4 97.2 28.5 4.6 120.2 125.7 29.5 4.7 95.1 107.5 97.3 28.4 4.7 120.2 125.7 29.6 4.8 95.3 107.6 97.5 28.5 4.8 120.2 125.7 29.6 4.9 95.4 107.7 97.6 28.4 4.9 120.3 125.7 29.6 5.0 95.6 107.9 97.7 28.4 5.0 120.2 125.7 29.6 5.1 113.4 121.9 109.6 28.4 5.1 120.3 125.7 29.6 5.2 134.4 139.3 126.8 28.4 5.2 120.3 125.6 29.6 5.3 150.2 158.3 137.9 28.4 5.3 120.3 125.7 29.6 5.4 160.4 165.0 145.6 28.5 5.4 120.3 125.6 29.6 5.5 167.1 165.5 152.1 28.5 5.5 126.4 137.7 29.6 5.6 167.2 168.0 159.7 28.5 5.6 135.5 146.8 29.6 5.7 166.0 169.1 159.4 28.5 5.7 141.0 153.2 29.6 5.8 170.9 169.8 159.8 28.5 5.8 145.2 156.8 29.6 5.9 170.2 170.1 160.2 28.6 5.9 148.1 158.9 29.6 6.0 170.1 170.2 160.5 28.5 6.0 150.2 160.3 29.6 6.1 169.9 170.3 160.8 28.6 6.1 151.9 161.2 29.6 6.2 169.8 170.4 160.9 28.6 6.2 153.1 161.8 29.6 6.3 169.7 170.4 161.0 28.5 6.3 154.0 162.4 29.6 6.4 169.6 170.3 161.1 28.6 6.4 154.7 162.7 29.7 6.5 169.5 170.2 161.1 28.6 6.5 155.3 163.0 29.7 6.6 169.3 170.2 161.2 28.6 6.6 155.8 163.2 29.7 6.7 169.4 170.1 161.2 28.5 6.7 156.2 163.3 29.7 6.8 169.2 170.1 161.1 28.5 6.8 156.7 163.5 29.8 6.9 169.1 170.0 161.1 28.5 6.9 157.1 163.5 29.8 7.0 169.0 170.0 161.0 28.5 7.0 157.5 163.7 29.8 7.1 168.8 169.9 161.0 28.5 7.1 158.0 163.7 29.9 7.2 168.6 169.9 161.0 28.5 7.2 158.5 163.7 29.9 7.3 168.5 169.7 160.8 28.5 7.3 159.0 163.7 30.0 7.4 168.4 169.7 160.8 28.5 7.4 159.5 163.7 30.0 7.5 168.4 169.7 160.7 28.5 7.5 159.9 163.7 30.0 7.6 168.3 169.6 160.6 28.4 7.6 160.0 163.8 30.0 7.7 168.3 169.6 160.5 28.3 7.7 160.1 163.7 30.0 7.8 168.2 169.5 160.5 28.3 7.8 160.2 163.8 30.1 7.9 168.2 169.3 160.4 28.2 7.9 160.3 163.8 30.1 8.0 168.1 169.3 160.3 28.2 8.0 160.3 163.7 30.0 8.1 168.0 169.3 160.2 28.2 8.1 160.3 163.7 30.1 8.2 168.0 169.2 160.2 28.1 8.2 160.4 163.7 30.0 8.3 167.9 169.2 160.1 28.1 8.3 160.3 163.7 30.0 8.4 167.9 169.1 160.1 28.1 8.4 160.4 163.6 30.1 8.5 167.8 169.0 159.9 28.1 8.5 160.4 163.7 30.0 8.6 167.7 168.9 159.8 28.0 8.6 160.3 163.6 30.1 8.7 167.7 168.9 159.8 28.0 8.7 160.3 163.5 30.1 8.8 167.6 168.8 159.7 27.9 8.8 160.3 163.5 30.0 8.9 167.6 168.7 159.7 27.9 8.9 160.3 163.5 30.0 9.0 167.6 168.6 159.6 27.9 9.0 160.3 163.5 30.0 9.1 167.5 168.5 159.5 27.9 9.1 160.2 163.4 30.0 9.2 167.5 168.5 27.9 9.2 160.2 163.4 30.0 9.3 167.5 168.4 28.0 9.3 160.2 163.4 30.0 9.4 167.5 168.3 28.0 9.4 160.2 163.3 30.0 9.5 167.5 168.3 28.1 9.5 160.2 163.3 29.9 9.6 167.5 168.2 28.1 9.6 160.3 163.3 29.9 9.7 167.4 168.1 28.1 9.7 160.2 163.2 29.9 9.8 167.4 168.1 28.2 9.8 160.3 163.2 29.9 9.9 167.4 168.0 28.2 9.9 160.3 163.1 29.9 10.0 167.4 167.9 28.1 10.0 160.3 163.2 29.9 10.1 167.4 167.8 28.1 10.1 160.2 163.1 29.9 10.2 167.4 167.8 28.2 10.2 160.3 163.1 29.9 10.3 167.4 167.7 28.2 10.3 160.2 163.0 29.9 10.4 167.3 167.6 28.2 10.4 160.2 163.1 29.9 10.5 167.3 167.6 28.2 10.5 160.2 163.0 29.9 10.6 167.3 167.6 28.2 10.6 160.2 163.0 29.9 10.7 167.2 167.5 28.2 10.7 160.2 163.0 29.8 10.8 167.1 167.5 28.2 10.8 160.2 163.0 29.8 10.9 167.1 167.4 28.2 10.9 160.1 162.9 29.8 11.0 167.1 167.1 28.2 11.0 160.1 162.9 29.9 11.1 162.1 165.1 28.2 11.1 160.1 162.9 29.9 11.2 157.9 161.7 28.2 11.2 160.1 162.8 30.0 11.3 154.6 158.7 154.5 28.2 11.3 160.1 162.8 30.0 11.4 152.0 155.7 153.1 28.2 11.4 160.1 162.8 30.1 11.5 149.2 153.2 151.8 28.2 11.5 156.9 163.3 30.1 11.6 145.3 155.3 148.1 28.2 11.6 152.6 159.0 30.1 11.7 141.6 152.4 144.5 28.3 11.7 149.1 155.9 30.1 11.8 138.6 149.5 141.7 28.2 11.8 146.4 153.8 30.1 11.9 136.3 147.1 139.5 28.3 11.9 144.6 151.3 30.1 12.0 134.6 144.9 138.5 28.3 12.0 141.0 148.0 30.1 12.1 126.9 133.5 129.6 28.2 12.1 137.7 145.9 30.1 12.2 120.5 125.5 121.2 28.3 12.2 135.0 143.6 30.1 12.3 115.5 118.8 115.8 28.3 12.3 132.7 141.5 30.1 12.4 111.5 113.8 111.1 28.3 12.4 130.9 140.4 30.0 12.5 108.0 109.7 107.3 28.3 12.5 123.6 130.4 30.0 12.6 105.0 106.1 104.1 28.2 12.6 117.8 121.8 30.1 12.7 102.5 103.1 101.4 28.2 12.7 113.4 116.0 30.1 12.8 100.1 100.4 99.0 28.2 12.8 109.8 111.5 30.1 12.9 98.0 98.1 96.8 28.2 12.9 106.6 107.7 30.1 13.0 96.1 95.9 94.7 28.2 13.0 103.8 104.5 30.0 13.1 94.3 94.1 93.0 28.1 13.1 101.4 101.6 30.0 13.2 92.7 92.3 91.3 28.1 13.2 99.3 99.2 30.0 13.3 91.3 90.7 89.7 28.0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 "CH1" "CH2" "CH3" 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 "CH1" "CH2" "CH3" _1211103675.xls 图表2 43.9 31.1 43.5 31.1 43.6 31.1 43.2 31.1 43 31.2 43 31.2 42.7 31.3 42.2 31.3 41.8 31.4 40.9 31.4 40.1 31.4 39.7 31.5 39 31.5 38.2 31.5 37.9 31.5 37.6 31.5 37.3 31.5 37.1 31.6 37.2 31.6 37.8 31.6 37.8 31.6 38.7 31.7 40.2 35.4 63.3 52.3 87.7 71.3 104.6 84.7 116 94.5 125.1 102.7 135 111.1 142 118.8 146.3 124.5 149.6 128.5 152.5 131.4 155.2 133.7 157.6 135.4 159.5 136.8 161 138 162.3 138.9 163.2 139.6 163.9 140.2 164.5 140.8 165 141.2 165.4 141.6 165.7 141.9 165.9 142.2 166 142.5 166.2 142.7 166.3 142.9 166.4 143.1 166.5 143.3 166.7 143.4 166.7 143.6 166.8 143.8 166.8 143.9 164.7 141.4 155 134 144.7 128.1 135.7 122.9 128 118.2 121.2 113.9 115.3 109.9 110 106.2 105.3 102.8 101 99.7 97 96.7 93.5 94 90.2 91.4 87.2 88.9 84.5 86.6 81.9 84.5 79.5 82.4 77.6 80.5 75.8 78.6 74.2 76.9 72.7 75.2 71.3 73.7 70 72.3 68.5 70.9 67 69.7 65.4 68.5 64 67.3 62.8 66.2 61.6 65.2 60.5 64.1 59.4 63.2 58.5 62.2 57.6 61.3 56.7 60.4 55.9 59.6 55 58.7 54.3 57.9 53.6 57.2 52.9 56.4 52.3 55.8 51.6 55.2 51.1 54.5 50.4 53.9 51 53.5 57.5 53.5 67.4 58.9 90.5 71.5 116 84.4 131.1 96.1 142.5 106.6 150.7 114.9 156 121.7 159.2 127 161.4 130.9 162.8 133.7 163.8 135.8 164.6 137.5 165.2 138.8 165.7 139.8 166.1 140.7 166.4 141.4 166.6 142 166.8 142.4 167 142.8 167.2 143.2 167.3 143.5 167.4 143.8 167.5 144 167.6 144.3 167.6 144.4 167.7 144.6 167.8 144.7 167.8 144.8 167.8 145 167.9 145.1 167.9 145.2 167.7 145.2 163.4 141 152.3 134.4 142.9 129 134.7 124.2 127.7 119.8 121.6 115.7 116.1 112 111.2 108.5 106.9 105.2 102.9 102.3 99.3 99.5 96.1 97 93.1 94.5 90.3 92.2 87.7 90 85.3 88 83.1 86.1 81.1 84.4 79.4 82.7 77.8 81.1 76.4 79.6 75.1 78.1 73.9 76.7 72.8 75.4 71.6 74.2 70.4 73 69.1 71.9 67.9 70.9 66.7 69.9 65.5 68.9 64.5 68 63.6 67.1 62.7 66.3 61.8 65.4 60.9 64.7 60 63.9 59.2 63.1 58.5 62.4 57.8 61.7 57.2 61 56.5 60.3 55.8 59.7 55.2 59 54.8 58.5 54.3 58 53.9 57.5 53.5 57 53 56.5 52.5 56 52.2 55.5 51.9 55.1 51.5 54.7 51.1 54.3 50.7 54 50.4 53.6 51.8 53.3 58.8 53.8 68.6 59.3 88 71 109.9 83.1 125 92.8 138.4 102.5 148.8 111.6 155.3 118.7 159.1 124.3 161.4 128.6 162.9 132 163.9 134.4 164.8 136.4 165.3 137.9 165.8 139.1 166.2 140.1 166.5 140.9 166.8 141.6 167 142.2 167.2 142.7 167.3 143 167.4 143.4 167.6 143.8 167.6 144.1 167.7 144.3 167.8 144.6 167.9 144.7 167.9 145 168 145.1 168 145.3 168 145.4 168.1 145.5 167.9 145.4 162.8 140.8 150.7 134.6 141.7 129.2 133.9 124.5 127.2 120.1 121.3 116.2 116.1 112.5 111.4 109.1 107.2 106.1 103.4 103.2 100 100.6 96.8 98 93.9 95.7 91.2 93.5 88.6 91.4 86.4 89.4 84.3 87.5 82.5 85.8 80.7 84.2 79.2 82.7 77.8 81.3 76.5 79.9 75.4 78.5 74.3 77.3 73.2 76.1 72 75 70.9 73.9 69.8 72.9 68.6 71.9 67.6 70.9 66.6 70 65.7 69.2 64.8 68.3 64 67.5 63.2 66.7 62.4 66 61.6 65.3 60.8 64.5 60 63.8 59.2 63 58.4 62.3 57.8 61.6 57.3 60.9 56.7 60.2 56.3 59.7 55.8 59.1 55.1 58.4 54.6 57.9 54.1 57.3 53.7 56.8 53.3 56.2 52.9 55.7 52.5 55.3 52.1 54.8 51.7 54.4 51.3 54 PP&PP at top side PP&Sealant at AL tab Time/s Temp/ºC Temp rise curve Sum Top sealing temp trend for 604396 at SSL factory Top sealing time interval 2s Top sealing time interval 3s Conclusion: For PP&Sealant,the temperature reach 140ºC from RT need 1.5s,the highest is 145ºC. For PP&PP,need0.8~1.0s,the temperature over160ºC and the hightest is 168ºC. Top sealing time interval 3s Sum 31.5 30.8 31.5 30.9 31.3 31 31.2 31 31.4 31.1 31.9 31.3 35.8 31.6 40.6 32.6 51.8 47.6 81 69.4 101.3 84.5 113.4 95.5 121.9 103.8 129.5 110 134.9 114.7 139.1 118.7 141.7 122.1 144.1 125 145.8 127.5 147.3 129.4 148.4 131.1 149.2 132.4 150.2 133.6 150.8 134.6 151.4 135.4 151.8 136.1 152.2 136.7 152.7 137.2 153 137.7 153.2 138.1 153.5 138.4 153.7 138.7 153.8 139 153.8 139.2 154 139.4 154.1 139.7 154.3 139.9 154.4 140 154.5 140.2 175.1 137.8 145.6 131 134.9 125.2 126.5 120 119.3 115.2 113.1 110.9 107.9 107 103.6 103.3 104.5 100 100.3 96.9 92.3 94 99.8 91.2 76.9 81.6 74.8 79.4 72.9 77.4 71.1 75.6 69.5 73.8 68 72.2 66.5 70.6 65 69.1 63.6 67.7 62.4 66.4 61.1 65.2 59.9 64 58.8 62.8 57.7 61.8 56.7 60.8 55.8 59.8 55 58.8 54.2 57.9 53.4 57.1 52.6 56.3 51.9 55.5 51.3 54.8 50.7 54.1 50.1 53.5 49.5 52.8 49 52.3 48.4 51.7 48 51.2 47.5 50.6 47.2 50.2 46.7 49.7 46.4 49.3 46 48.8 45.6 48.4 45.3 48 45 47.7 44.6 47.4 44.3 47 44.1 46.7 43.9 46.4 43.6 46.1 43.4 45.9 43.2 45.6 42.9 45.3 42.7 45.1 42.6 44.9 42.4 44.7 42.1 44.4 41.9 44.2 41.7 44.1 41.6 43.8 41.4 43.6 41.2 43.5 41 43.3 40.8 43.1 40.7 43 40.5 42.8 40.4 42.7 40.3 42.5 40.2 42.4 40.2 42.2 40.2 42.1 40 42.1 39.8 42 39.7 41.9 39.6 41.8 39.6 41.8 39.6 41.7 39.5 41.6 39.5 41.5 39.3 41.3 39.3 41.2 39.3 41.3 39.3 41.2 44 41.5 53.9 47.5 84.7 68 106 82.8 120.1 94.6 127.8 104 133.8 111.7 139 118.1 142.9 123.1 145.9 126.9 147.9 129.9 149.4 132.3 150.7 134.3 151.7 135.9 152.5 137.2 153.3 138.2 153.8 139.1 154.3 139.9 154.7 140.5 155.1 140.9 155.3 141.4 155.5 141.8 155.7 142 156 142.3 156 142.5 156.2 142.7 156.4 142.9 156.4 143.1 156.6 143.2 156.7 143.3 156.7 143.5 156.8 143.6 157.3 143.7 83.9 87.5 82.3 85.3 78.6 83.2 76.3 81.3 74.4 79.4 72.8 77.7 71.3 76 69.8 74.5 68.4 73 67 71.7 65.8 70.3 64.5 69.1 63.4 68 62.2 66.8 61.2 65.8 60.3 64.8 59.3 63.8 58.4 62.9 57.6 62.1 56.8 61.2 56.1 60.4 55.5 59.6 54.8 58.9 54.3 58.2 53.8 57.6 53.3 57.1 52.7 56.5 52.2 56 51.7 55.4 51.3 54.9 50.9 54.4 50.5 54 50.2 53.5 49.7 53.1 49.4 52.7 49 52.4 48.7 52 48.5 51.7 48.3 51.3 48 51 47.7 50.7 47.4 50.4 47.2 50.1 46.9 49.8 46.6 49.6 46.5 49.3 46.2 49.1 46 48.8 45.8 48.6 45.6 48.4 49.6 48.4 55.6 50.5 97.3 71.2 113.2 87.3 125.2 99.3 133.6 108.8 139.3 116.2 143.4 121.9 146.3 126.2 148.4 129.7 150.1 132.4 151.5 134.6 152.6 136.4 153.4 137.8 154.1 139 154.7 139.9 155.2 140.7 155.6 141.3 156 141.8 156.3 142.3 156.5 142.6 156.8 142.9 157 143.2 157.2 143.5 157.4 143.7 157.5 143.9 157.6 144 157.7 144.1 157.8 144.3 157.9 144.4 158 144.5 158 144.6 158 144.7 111.3 144.7 136.5 131.7 128.8 126.4 122.3 121.5 116.7 117.1 111.6 113.1 107.1 109.4 103 106 99.4 102.7 96 99.9 93 97.1 90.2 94.7 87.6 92.3 85.2 90 83.1 88 81.1 85.9 79.2 84.1 77.5 82.3 75.9 80.5 74.4 78.9 73 77.4 71.7 75.9 70.5 74.6 69.2 73.3 68 72.1 66.8 71 65.8 70 64.6 68.9 63.5 67.9 62.4 66.8 61.4 65.9 60.4 64.9 59.5 63.9 58.7 63 57.9 62.1 57.1 61.2 56.4 60.4 55.7 59.7 54.9 58.7 54.2 57.9 53.7 57.3 53.3 56.7 52.8 56.1 52.4 55.6 52 55.1 51.5 54.6 51.2 54.1 50.8 53.6 50.4 53.2 50 52.8 49.8 52.5 49.5 52.2 49.2 51.8 48.7 51.4 48.5 51.1 48.2 50.8 47.9 50.5 47.7 50.2 47.5 49.9 47.2 49.6 47 49.4 PP&PP at top side PP&Sealant at Al tab Time/s Temp/ºC Temp rise curve 34 31.5 31.8 31.6 31.9 31.7 32 31.7 32 31.7 32.1 31.8 32.1 31.8 32.1 31.7 32.1 31.7 32.2 31.8 32.3 32 32.3 38.2 33.2 44.2 35.5 62.3 47.1 85.8 61.8 110 76.3 128.1 88.7 140.4 98.7 149 107.1 154.6 114 158.3 119.7 161 124.2 162.9 128.1 164.1 131.1 165.1 133.6 165.8 135.5 166.4 137 166.8 138.1 167.1 139.1 167.4 139.9 167.7 140.6 167.9 141.2 168 141.7 168.1 142.1 165.9 140 153.5 132.7 142.6 126.2 133.4 120.5 125.5 115.5 118.7 110.9 112.7 106.7 107.4 102.9 102.6 99.3 98.4 96.1 94.5 93.1 90.9 90.4 87.6 87.8 84.7 85.4 82 83.1 79.5 81 77.3 79 75.4 77 73.6 75.2 72 73.5 70.6 71.9 69.1 70.4 67.6 69 66.1 67.7 64.7 66.4 63.2 65.2 61.9 64 60.7 63 59.6 61.9 58.5 60.9 57.4 59.9 56.4 58.9 55.5 58 54.6 57.1 53.8 56.3 53.2 55.6 52.6 54.9 51.9 54.2 51.2 53.6 50.5 52.9 49.8 52.4 49.1 51.8 48.4 51.2 47.8 50.7 47.2 50 46.7 49.5 46.2 48.9 45.7 48.4 45.3 48 44.9 47.5 44.5 47.1 44.2 46.7 43.9 46.4 43.6 46.1 43.3 45.8 43.1 45.5 42.9 45.2 42.6 45 42.5 44.7 42.2 44.5 42 44.3 41.8 44 41.6 43.9 41.4 43.7 41.3 43.4 41.1 43.3 41 43 40.8 42.9 40.6 42.8 40.5 42.6 40.4 42.4 40.3 42.2 40.2 42.1 40 42 39.8 41.9 39.7 41.7 39.6 41.7 39.5 41.5 39.5 41.5 39.5 41.4 39.6 41.4 39.5 41.3 39.3 41.2 39.2 41.2 39.2 41.1 39.1 41 38.9 40.9 38.7 40.8 38.6 40.7 38.5 40.6 38.6 40.6 38.6 40.6 38.3 40.4 38.1 40.2 38 40.2 38.1 40.2 38 40.1 38.3 40.1 38.3 40.1 38.2 40 38.2 40.1 38.1 39.9 38.3 40 38.1 39.8 38.1 39.8 38.1 39.8 38.1 39.8 38 39.7 38 39.7 39.4 39.6 47.4 40.4 57.5 47.5 88.5 63.1 118.5 78.5 134.7 91.5 145.3 102.2 152.4 110.8 156.8 117.4 160 122.7 161.9 126.7 163.5 130.2 164.6 132.8 165.4 134.8 166.1 136.4 166.5 137.7 167 138.8 167.3 139.7 167.6 140.5 167.8 141.2 168 141.7 168.1 142.3 168.3 142.7 168.3 143 162.9 138.4 151.4 131.3 141.2 125.4 132.6 120.3 125.3 115.6 118.9 111.4 113.2 107.6 108.2 104 103.8 100.8 99.7 97.9 96.1 95.1 92.7 92.5 89.6 90 86.8 87.8 84.4 85.7 82.1 83.7 79.9 81.8 78 80 76.3 78.2 74.7 76.6 73.2 75.1 71.8 73.7 70.6 72.3 69.2 71 67.9 69.8 66.6 68.6 65.4 67.5 64.2 66.4 63.1 65.4 62 64.4 61 63.4 60.1 62.5 59.3 61.6 58.4 60.8 57.6 60 56.9 59.2 56.2 58.5 55.5 57.8 54.9 57.1 54.3 56.5 53.8 55.9 53.1 55.3 52.5 54.7 52 54.2 51.6 53.8 51.1 53.3 50.7 52.8 50.2 52.4 49.8 52 49.4 51.6 49 51.2 48.7 50.9 48.3 50.5 48.1 50.2 47.8 49.9 47.5 49.6 47.2 49.3 47 49.1 46.8 48.8 46.5 48.6 46.3 48.3 46.1 48.1 46 47.9 45.9 47.7 45.7 47.5 45.4 47.3 45.2 47.1 45.1 46.9 44.9 46.8 44.7 46.6 44.6 46.5 44.4 46.3 44.2 46.2 44.1 46 44 45.9 44 45.7 43.9 45.6 43.9 45.5 43.8 45.5 43.6 45.4 43.4 45.3 43.2 45.2 43 45.1 42.8 45 42.7 44.9 42.6 44.8 42.4 44.8 42.4 44.7 42.3 44.6 42.2 44.5 42.1 44.4 42.2 44.3 42.4 44.3 42.3 44.2 42.2 44.1 42.1 44.1 42.1 44 42.1 43.9 42 43.8 41.8 43.7 41.7 43.6 41.7 43.6 41.6 43.5 47 43.8 54.9 45 70.5 57.3 107 73.1 128.7 86.9 142 99.2 150.9 109.2 156.3 116.8 159.6 122.6 161.8 127.2 163.2 130.7 164.3 133.4 165.2 135.6 165.9 137.3 166.4 138.6 166.8 139.7 167.2 140.7 167.4 141.5 167.7 142.1 167.9 142.7 168 143.2 168.2 143.6 168.3 144 168.7 143.7 158.1 136.5 147 130.3 137.8 125 129.9 120.1 123.1 115.6 117.2 111.7 112 108 107.3 104.6 103.1 101.5 99.3 98.7 95.8 96 92.7 93.5 89.8 91.2 87.1 89 84.7 87 82.5 85.1 80.5 83.3 78.7 81.5 77.2 79.8 75.7 78.3 74.4 76.8 73.2 75.4 72 74.1 70.8 72.8 69.5 71.7 68.3 70.5 67 69.5 65.9 68.5 64.6 67.4 63.4 66.5 62.2 65.5 61.1 64.5 60 63.5 59 62.5 58.1 61.6 57.2 60.9 56.4 60 55.8 59.2 55.3 58.6 54.7 57.8 54.1 57.2 53.5 56.6 53 56 52.5 55.5 52 55 51.6 54.4 51.1 54 50.7 53.5 50.4 53.2 49.9 52.7 49.6 52.3 49.1 51.8 48.9 51.6 48.4 51.1 48.2 50.9 47.9 50.5 47.6 50.2 47.3 49.9 47.1 49.6 46.8 49.3 46.5 49 46.3 48.8 PP&PP at top side PP&Sealant at Al tab Time/s Temp/ºC Temp rise curve 35 43.9 31.1 43.5 31.1 43.6 31.1 43.2 31.1 43 31.2 43 31.2 42.7 31.3 42.2 31.3 41.8 31.4 40.9 31.4 40.1 31.4 39.7 31.5 39 31.5 38.2 31.5 37.9 31.5 37.6 31.5 37.3 31.5 37.1 31.6 37.2 31.6 37.8 31.6 37.8 31.6 38.7 31.7 40.2 35.4 63.3 52.3 87.7 71.3 104.6 84.7 116 94.5 125.1 102.7 135 111.1 142 118.8 146.3 124.5 149.6 128.5 152.5 131.4 155.2 133.7 157.6 135.4 159.5 136.8 161 138 162.3 138.9 163.2 139.6 163.9 140.2 164.5 140.8 165 141.2 165.4 141.6 165.7 141.9 165.9 142.2 166 142.5 166.2 142.7 166.3 142.9 166.4 143.1 166.5 143.3 166.7 143.4 166.7 143.6 166.8 143.8 166.8 143.9 164.7 141.4 155 134 144.7 128.1 135.7 122.9 128 118.2 121.2 113.9 115.3 109.9 110 106.2 105.3 102.8 101 99.7 97 96.7 93.5 94 90.2 91.4 87.2 88.9 84.5 86.6 81.9 84.5 79.5 82.4 77.6 80.5 75.8 78.6 74.2 76.9 72.7 75.2 71.3 73.7 70 72.3 68.5 70.9 67 69.7 65.4 68.5 64 67.3 62.8 66.2 61.6 65.2 60.5 64.1 59.4 63.2 58.5 62.2 57.6 61.3 56.7 60.4 55.9 59.6 55 58.7 54.3 57.9 53.6 57.2 52.9 56.4 52.3 55.8 51.6 55.2 51.1 54.5 50.4 53.9 51 53.5 57.5 53.5 67.4 58.9 90.5 71.5 116 84.4 131.1 96.1 142.5 106.6 150.7 114.9 156 121.7 159.2 127 161.4 130.9 162.8 133.7 163.8 135.8 164.6 137.5 165.2 138.8 165.7 139.8 166.1 140.7 166.4 141.4 166.6 142 166.8 142.4 167 142.8 167.2 143.2 167.3 143.5 167.4 143.8 167.5 144 167.6 144.3 167.6 144.4 167.7 144.6 167.8 144.7 167.8 144.8 167.8 145 167.9 145.1 167.9 145.2 167.7 145.2 163.4 141 152.3 134.4 142.9 129 134.7 124.2 127.7 119.8 121.6 115.7 116.1 112 111.2 108.5 106.9 105.2 102.9 102.3 99.3 99.5 96.1 97 93.1 94.5 90.3 92.2 87.7 90 85.3 88 83.1 86.1 81.1 84.4 79.4 82.7 77.8 81.1 76.4 79.6 75.1 78.1 73.9 76.7 72.8 75.4 71.6 74.2 70.4 73 69.1 71.9 67.9 70.9 66.7 69.9 65.5 68.9 64.5 68 63.6 67.1 62.7 66.3 61.8 65.4 60.9 64.7 60 63.9 59.2 63.1 58.5 62.4 57.8 61.7 57.2 61 56.5 60.3 55.8 59.7 55.2 59 54.8 58.5 54.3 58 53.9 57.5 53.5 57 53 56.5 52.5 56 52.2 55.5 51.9 55.1 51.5 54.7 51.1 54.3 50.7 54 50.4 53.6 51.8 53.3 58.8 53.8 68.6 59.3 88 71 109.9 83.1 125 92.8 138.4 102.5 148.8 111.6 155.3 118.7 159.1 124.3 161.4 128.6 162.9 132 163.9 134.4 164.8 136.4 165.3 137.9 165.8 139.1 166.2 140.1 166.5 140.9 166.8 141.6 167 142.2 167.2 142.7 167.3 143 167.4 143.4 167.6 143.8 167.6 144.1 167.7 144.3 167.8 144.6 167.9 144.7 167.9 145 168 145.1 168 145.3 168 145.4 168.1 145.5 167.9 145.4 162.8 140.8 150.7 134.6 141.7 129.2 133.9 124.5 127.2 120.1 121.3 116.2 116.1 112.5 111.4 109.1 107.2 106.1 103.4 103.2 100 100.6 96.8 98 93.9 95.7 91.2 93.5 88.6 91.4 86.4 89.4 84.3 87.5 82.5 85.8 80.7 84.2 79.2 82.7 77.8 81.3 76.5 79.9 75.4 78.5 74.3 77.3 73.2 76.1 72 75 70.9 73.9 69.8 72.9 68.6 71.9 67.6 70.9 66.6 70 65.7 69.2 64.8 68.3 64 67.5 63.2 66.7 62.4 66 61.6 65.3 60.8 64.5 60 63.8 59.2 63 58.4 62.3 57.8 61.6 57.3 60.9 56.7 60.2 56.3 59.7 55.8 59.1 55.1 58.4 54.6 57.9 54.1 57.3 53.7 56.8 53.3 56.2 52.9 55.7 52.5 55.3 52.1 54.8 51.7 54.4 51.3 54 PP&PP at top side PP&Sealant at AL tab Time/s Temp/ºC Temp rise curve AUTO0032 0.00 43.90 31.10 0.10 43.50 31.10 0.20 43.60 31.10 0.30 43.20 31.10 0.40 43.00 31.20 0.50 43.00 31.20 0.60 42.70 31.30 0.70 42.20 31.30 0.80 41.80 31.40 0.90 40.90 31.40 1.00 40.10 31.40 1.10 39.70 31.50 1.20 39.00 31.50 1.30 38.20 31.50 1.40 37.90 31.50 1.50 37.60 31.50 1.60 37.30 31.50 1.70 37.10 31.60 1.80 37.20 31.60 1.90 37.80 31.60 2.00 37.80 31.60 2.10 38.70 31.70 2.20 40.20 35.40 2.30 63.30 52.30 2.40 87.70 71.30 2.50 104.60 84.70 2.60 116.00 94.50 2.70 125.10 102.70 2.80 135.00 111.10 2.90 142.00 118.80 3.00 146.30 124.50 3.10 149.60 128.50 3.20 152.50 131.40 3.30 155.20 133.70 3.40 157.60 135.40 3.50 159.50 136.80 3.60 161.00 138.00 3.70 162.30 138.90 3.80 163.20 139.60 3.90 163.90 140.20 4.00 164.50 140.80 4.10 165.00 141.20 4.20 165.40 141.60 4.30 165.70 141.90 4.40 165.90 142.20 4.50 166.00 142.50 4.60 166.20 142.70 4.70 166.30 142.90 4.80 166.40 143.10 4.90 166.50 143.30 5.00 166.70 143.40 5.10 166.70 143.60 5.20 166.80 143.80 5.30 166.80 143.90 5.40 164.70 141.40 5.50 155.00 134.00 5.60 144.70 128.10 5.70 135.70 122.90 5.80 128.00 118.20 5.90 121.20 113.90 6.00 115.30 109.90 6.10 110.00 106.20 6.20 105.30 102.80 6.30 101.00 99.70 6.40 97.00 96.70 6.50 93.50 94.00 6.60 90.20 91.40 6.70 87.20 88.90 6.80 84.50 86.60 6.90 81.90 84.50 7.00 79.50 82.40 7.10 77.60 80.50 7.20 75.80 78.60 7.30 74.20 76.90 7.40 72.70 75.20 7.50 71.30 73.70 7.60 70.00 72.30 7.70 68.50 70.90 7.80 67.00 69.70 7.90 65.40 68.50 8.00 64.00 67.30 8.10 62.80 66.20 8.20 61.60 65.20 8.30 60.50 64.10 8.40 59.40 63.20 8.50 58.50 62.20 8.60 57.60 61.30 8.70 56.70 60.40 8.80 55.90 59.60 8.90 55.00 58.70 9.00 54.30 57.90 9.10 53.60 57.20 9.20 52.90 56.40 9.30 52.30 55.80 9.40 51.60 55.20 9.50 51.10 54.50 9.60 50.40 53.90 9.70 51.00 53.50 9.80 57.50 53.50 9.90 67.40 58.90 10.00 90.50 71.50 10.10 116.00 84.40 10.20 131.10 96.10 10.30 142.50 106.60 10.40 150.70 114.90 10.50 156.00 121.70 10.60 159.20 127.00 10.70 161.40 130.90 10.80 162.80 133.70 10.90 163.80 135.80 11.00 164.60 137.50 11.10 165.20 138.80 11.20 165.70 139.80 11.30 166.10 140.70 11.40 166.40 141.40 11.50 166.60 142.00 11.60 166.80 142.40 11.70 167.00 142.80 11.80 167.20 143.20 11.90 167.30 143.50 12.00 167.40 143.80 12.10 167.50 144.00 12.20 167.60 144.30 12.30 167.60 144.40 12.40 167.70 144.60 12.50 167.80 144.70 12.60 167.80 144.80 12.70 167.80 145.00 12.80 167.90 145.10 12.90 167.90 145.20 13.00 167.70 145.20 13.10 163.40 141.00 13.20 152.30 134.40 13.30 142.90 129.00 13.40 134.70 124.20 13.50 127.70 119.80 13.60 121.60 115.70 13.70 116.10 112.00 13.80 111.20 108.50 13.90 106.90 105.20 14.00 102.90 102.30 14.10 99.30 99.50 14.20 96.10 97.00 14.30 93.10 94.50 14.40 90.30 92.20 14.50 87.70 90.00 14.60 85.30 88.00 14.70 83.10 86.10 14.80 81.10 84.40 14.90 79.40 82.70 15.00 77.80 81.10 15.10 76.40 79.60 15.20 75.10 78.10 15.30 73.90 76.70 15.40 72.80 75.40 15.50 71.60 74.20 15.60 70.40 73.00 15.70 69.10 71.90 15.80 67.90 70.90 15.90 66.70 69.90 16.00 65.50 68.90 16.10 64.50 68.00 16.20 63.60 67.10 16.30 62.70 66.30 16.40 61.80 65.40 16.50 60.90 64.70 16.60 60.00 63.90 16.70 59.20 63.10 16.80 58.50 62.40 16.90 57.80 61.70 17.00 57.20 61.00 17.10 56.50 60.30 17.20 55.80 59.70 17.30 55.20 59.00 17.40 54.80 58.50 17.50 54.30 58.00 17.60 53.90 57.50 17.70 53.50 57.00 17.80 53.00 56.50 17.90 52.50 56.00 18.00 52.20 55.50 18.10 51.90 55.10 18.20 51.50 54.70 18.30 51.10 54.30 18.40 50.70 54.00 18.50 50.40 53.60 18.60 51.80 53.30 18.70 58.80 53.80 18.80 68.60 59.30 18.90 88.00 71.00 19.00 109.90 83.10 19.10 125.00 92.80 19.20 138.40 102.50 19.30 148.80 111.60 19.40 155.30 118.70 19.50 159.10 124.30 19.60 161.40 128.60 19.70 162.90 132.00 19.80 163.90 134.40 19.90 164.80 136.40 20.00 165.30 137.90 20.10 165.80 139.10 20.20 166.20 140.10 20.30 166.50 140.90 20.40 166.80 141.60 20.50 167.00 142.20 20.60 167.20 142.70 20.70 167.30 143.00 20.80 167.40 143.40 20.90 167.60 143.80 21.00 167.60 144.10 21.10 167.70 144.30 21.20 167.80 144.60 21.30 167.90 144.70 21.40 167.90 145.00 21.50 168.00 145.10 21.60 168.00 145.30 21.70 168.00 145.40 21.80 168.10 145.50 21.90 167.90 145.40 22.00 162.80 140.80 22.10 150.70 134.60 22.20 141.70 129.20 22.30 133.90 124.50 22.40 127.20 120.10 22.50 121.30 116.20 22.60 116.10 112.50 22.70 111.40 109.10 22.80 107.20 106.10 22.90 103.40 103.20 23.00 100.00 100.60 23.10 96.80 98.00 23.20 93.90 95.70 23.30 91.20 93.50 23.40 88.60 91.40 23.50 86.40 89.40 23.60 84.30 87.50 23.70 82.50 85.80 23.80 80.70 84.20 23.90 79.20 82.70 24.00 77.80 81.30 24.10 76.50 79.90 24.20 75.40 78.50 24.30 74.30 77.30 24.40 73.20 76.10 24.50 72.00 75.00 24.60 70.90 73.90 24.70 69.80 72.90 24.80 68.60 71.90 24.90 67.60 70.90 25.00 66.60 70.00 25.10 65.70 69.20 25.20 64.80 68.30 25.30 64.00 67.50 25.40 63.20 66.70 25.50 62.40 66.00 25.60 61.60 65.30 25.70 60.80 64.50 25.80 60.00 63.80 25.90 59.20 63.00 26.00 58.40 62.30 26.10 57.80 61.60 26.20 57.30 60.90 26.30 56.70 60.20 26.40 56.30 59.70 26.50 55.80 59.10 26.60 55.10 58.40 26.70 54.60 57.90 26.80 54.10 57.30 26.90 53.70 56.80 27.00 53.30 56.20 27.10 52.90 55.70 27.20 52.50 55.30 27.30 52.10 54.80 27.40 51.70 54.40 27.50 51.30 54.00 AUTO0032 43.9 31.1 43.5 31.1 43.6 31.1 43.2 31.1 43 31.2 43 31.2 42.7 31.3 42.2 31.3 41.8 31.4 40.9 31.4 40.1 31.4 39.7 31.5 39 31.5 38.2 31.5 37.9 31.5 37.6 31.5 37.3 31.5 37.1 31.6 37.2 31.6 37.8 31.6 37.8 31.6 38.7 31.7 40.2 35.4 63.3 52.3 87.7 71.3 104.6 84.7 116 94.5 125.1 102.7 135 111.1 142 118.8 146.3 124.5 149.6 128.5 152.5 131.4 155.2 133.7 157.6 135.4 159.5 136.8 161 138 162.3 138.9 163.2 139.6 163.9 140.2 164.5 140.8 165 141.2 165.4 141.6 165.7 141.9 165.9 142.2 166 142.5 166.2 142.7 166.3 142.9 166.4 143.1 166.5 143.3 166.7 143.4 166.7 143.6 166.8 143.8 166.8 143.9 164.7 141.4 155 134 144.7 128.1 135.7 122.9 128 118.2 121.2 113.9 115.3 109.9 110 106.2 105.3 102.8 101 99.7 97 96.7 93.5 94 90.2 91.4 87.2 88.9 84.5 86.6 81.9 84.5 79.5 82.4 77.6 80.5 75.8 78.6 74.2 76.9 72.7 75.2 71.3 73.7 70 72.3 68.5 70.9 67 69.7 65.4 68.5 64 67.3 62.8 66.2 61.6 65.2 60.5 64.1 59.4 63.2 58.5 62.2 57.6 61.3 56.7 60.4 55.9 59.6 55 58.7 54.3 57.9 53.6 57.2 52.9 56.4 52.3 55.8 51.6 55.2 51.1 54.5 50.4 53.9 51 53.5 57.5 53.5 67.4 58.9 90.5 71.5 116 84.4 131.1 96.1 142.5 106.6 150.7 114.9 156 121.7 159.2 127 161.4 130.9 162.8 133.7 163.8 135.8 164.6 137.5 165.2 138.8 165.7 139.8 166.1 140.7 166.4 141.4 166.6 142 166.8 142.4 167 142.8 167.2 143.2 167.3 143.5 167.4 143.8 167.5 144 167.6 144.3 167.6 144.4 167.7 144.6 167.8 144.7 167.8 144.8 167.8 145 167.9 145.1 167.9 145.2 167.7 145.2 163.4 141 152.3 134.4 142.9 129 134.7 124.2 127.7 119.8 121.6 115.7 116.1 112 111.2 108.5 106.9 105.2 102.9 102.3 99.3 99.5 96.1 97 93.1 94.5 90.3 92.2 87.7 90 85.3 88 83.1 86.1 81.1 84.4 79.4 82.7 77.8 81.1 76.4 79.6 75.1 78.1 73.9 76.7 72.8 75.4 71.6 74.2 70.4 73 69.1 71.9 67.9 70.9 66.7 69.9 65.5 68.9 64.5 68 63.6 67.1 62.7 66.3 61.8 65.4 60.9 64.7 60 63.9 59.2 63.1 58.5 62.4 57.8 61.7 57.2 61 56.5 60.3 55.8 59.7 55.2 59 54.8 58.5 54.3 58 53.9 57.5 53.5 57 53 56.5 52.5 56 52.2 55.5 51.9 55.1 51.5 54.7 51.1 54.3 50.7 54 50.4 53.6 51.8 53.3 58.8 53.8 68.6 59.3 88 71 109.9 83.1 125 92.8 138.4 102.5 148.8 111.6 155.3 118.7 159.1 124.3 161.4 128.6 162.9 132 163.9 134.4 164.8 136.4 165.3 137.9 165.8 139.1 166.2 140.1 166.5 140.9 166.8 141.6 167 142.2 167.2 142.7 167.3 143 167.4 143.4 167.6 143.8 167.6 144.1 167.7 144.3 167.8 144.6 167.9 144.7 167.9 145 168 145.1 168 145.3 168 145.4 168.1 145.5 167.9 145.4 162.8 140.8 150.7 134.6 141.7 129.2 133.9 124.5 127.2 120.1 121.3 116.2 116.1 112.5 111.4 109.1 107.2 106.1 103.4 103.2 100 100.6 96.8 98 93.9 95.7 91.2 93.5 88.6 91.4 86.4 89.4 84.3 87.5 82.5 85.8 80.7 84.2 79.2 82.7 77.8 81.3 76.5 79.9 75.4 78.5 74.3 77.3 73.2 76.1 72 75 70.9 73.9 69.8 72.9 68.6 71.9 67.6 70.9 66.6 70 65.7 69.2 64.8 68.3 64 67.5 63.2 66.7 62.4 66 61.6 65.3 60.8 64.5 60 63.8 59.2 63 58.4 62.3 57.8 61.6 57.3 60.9 56.7 60.2 56.3 59.7 55.8 59.1 55.1 58.4 54.6 57.9 54.1 57.3 53.7 56.8 53.3 56.2 52.9 55.7 52.5 55.3 52.1 54.8 51.7 54.4 51.3 54 PP&PP at top side PP&Sealant at AL tab 0.00 31.50 31.80 0.10 31.60 31.90 0.20 31.70 32.00 0.30 31.70 32.00 0.40 31.70 32.10 0.50 31.80 32.10 0.60 31.80 32.10 0.70 31.70 32.10 0.80 31.70 32.20 0.90 31.80 32.30 1.00 32.00 32.30 1.10 38.20 33.20 1.20 44.20 35.50 1.30 62.30 47.10 1.40 85.80 61.80 1.50 110.00 76.30 1.60 128.10 88.70 1.70 140.40 98.70 1.80 149.00 107.10 1.90 154.60 114.00 2.00 158.30 119.70 2.10 161.00 124.20 2.20 162.90 128.10 2.30 164.10 131.10 2.40 165.10 133.60 2.50 165.80 135.50 2.60 166.40 137.00 2.70 166.80 138.10 2.80 167.10 139.10 2.90 167.40 139.90 3.00 167.70 140.60 3.10 167.90 141.20 3.20 168.00 141.70 3.30 168.10 142.10 3.40 165.90 140.00 3.50 153.50 132.70 3.60 142.60 126.20 3.70 133.40 120.50 3.80 125.50 115.50 3.90 118.70 110.90 4.00 112.70 106.70 4.10 107.40 102.90 4.20 102.60 99.30 4.30 98.40 96.10 4.40 94.50 93.10 4.50 90.90 90.40 4.60 87.60 87.80 4.70 84.70 85.40 4.80 82.00 83.10 4.90 79.50 81.00 5.00 77.30 79.00 5.10 75.40 77.00 5.20 73.60 75.20 5.30 72.00 73.50 5.40 70.60 71.90 5.50 69.10 70.40 5.60 67.60 69.00 5.70 66.10 67.70 5.80 64.70 66.40 5.90 63.20 65.20 6.00 61.90 64.00 6.10 60.70 63.00 6.20 59.60 61.90 6.30 58.50 60.90 6.40 57.40 59.90 6.50 56.40 58.90 6.60 55.50 58.00 6.70 54.60 57.10 6.80 53.80 56.30 6.90 53.20 55.60 7.00 52.60 54.90 7.10 51.90 54.20 7.20 51.20 53.60 7.30 50.50 52.90 7.40 49.80 52.40 7.50 49.10 51.80 7.60 48.40 51.20 7.70 47.80 50.70 7.80 47.20 50.00 7.90 46.70 49.50 8.00 46.20 48.90 8.10 45.70 48.40 8.20 45.30 48.00 8.30 44.90 47.50 8.40 44.50 47.10 8.50 44.20 46.70 8.60 43.90 46.40 8.70 43.60 46.10 8.80 43.30 45.80 8.90 43.10 45.50 9.00 42.90 45.20 9.10 42.60 45.00 9.20 42.50 44.70 9.30 42.20 44.50 9.40 42.00 44.30 9.50 41.80 44.00 9.60 41.60 43.90 9.70 41.40 43.70 9.80 41.30 43.40 9.90 41.10 43.30 10.00 41.00 43.00 10.10 40.80 42.90 10.20 40.60 42.80 10.30 40.50 42.60 10.40 40.40 42.40 10.50 40.30 42.20 10.60 40.20 42.10 10.70 40.00 42.00 10.80 39.80 41.90 10.90 39.70 41.70 11.00 39.60 41.70 11.10 39.50 41.50 11.20 39.50 41.50 11.30 39.50 41.40 11.40 39.60 41.40 11.50 39.50 41.30 11.60 39.30 41.20 11.70 39.20 41.20 11.80 39.20 41.10 11.90 39.10 41.00 12.00 38.90 40.90 12.10 38.70 40.80 12.20 38.60 40.70 12.30 38.50 40.60 12.40 38.60 40.60 12.50 38.60 40.60 12.60 38.30 40.40 12.70 38.10 40.20 12.80 38.00 40.20 12.90 38.10 40.20 13.00 38.00 40.10 13.10 38.30 40.10 13.20 38.30 40.10 13.30 38.20 40.00 13.40 38.20 40.10 13.50 38.10 39.90 13.60 38.30 40.00 13.70 38.10 39.80 13.80 38.10 39.80 13.90 38.10 39.80 14.00 38.10 39.80 14.10 38.00 39.70 14.20 38.00 39.70 14.30 39.40 39.60 14.40 47.40 40.40 14.50 57.50 47.50 14.60 88.50 63.10 14.70 118.50 78.50 14.80 134.70 91.50 14.90 145.30 102.20 15.00 152.40 110.80 15.10 156.80 117.40 15.20 160.00 122.70 15.30 161.90 126.70 15.40 163.50 130.20 15.50 164.60 132.80 15.60 165.40 134.80 15.70 166.10 136.40 15.80 166.50 137.70 15.90 167.00 138.80 16.00 167.30 139.70 16.10 167.60 140.50 16.20 167.80 141.20 16.30 168.00 141.70 16.40 168.10 142.30 16.50 168.30 142.70 16.60 168.30 143.00 16.70 162.90 138.40 16.80 151.40 131.30 16.90 141.20 125.40 17.00 132.60 120.30 17.10 125.30 115.60 17.20 118.90 111.40 17.30 113.20 107.60 17.40 108.20 104.00 17.50 103.80 100.80 17.60 99.70 97.90 17.70 96.10 95.10 17.80 92.70 92.50 17.90 89.60 90.00 18.00 86.80 87.80 18.10 84.40 85.70 18.20 82.10 83.70 18.30 79.90 81.80 18.40 78.00 80.00 18.50 76.30 78.20 18.60 74.70 76.60 18.70 73.20 75.10 18.80 71.80 73.70 18.90 70.60 72.30 19.00 69.20 71.00 19.10 67.90 69.80 19.20 66.60 68.60 19.30 65.40 67.50 19.40 64.20 66.40 19.50 63.10 65.40 19.60 62.00 64.40 19.70 61.00 63.40 19.80 60.10 62.50 19.90 59.30 61.60 20.00 58.40 60.80 20.10 57.60 60.00 20.20 56.90 59.20 20.30 56.20 58.50 20.40 55.50 57.80 20.50 54.90 57.10 20.60 54.30 56.50 20.70 53.80 55.90 20.80 53.10 55.30 20.90 52.50 54.70 21.00 52.00 54.20 21.10 51.60 53.80 21.20 51.10 53.30 21.30 50.70 52.80 21.40 50.20 52.40 21.50 49.80 52.00 21.60 49.40 51.60 21.70 49.00 51.20 21.80 48.70 50.90 21.90 48.30 50.50 22.00 48.10 50.20 22.10 47.80 49.90 22.20 47.50 49.60 22.30 47.20 49.30 22.40 47.00 49.10 22.50 46.80 48.80 22.60 46.50 48.60 22.70 46.30 48.30 22.80 46.10 48.10 22.90 46.00 47.90 23.00 45.90 47.70 23.10 45.70 47.50 23.20 45.40 47.30 23.30 45.20 47.10 23.40 45.10 46.90 23.50 44.90 46.80 23.60 44.70 46.60 23.70 44.60 46.50 23.80 44.40 46.30 23.90 44.20 46.20 24.00 44.10 46.00 24.10 44.00 45.90 24.20 44.00 45.70 24.30 43.90 45.60 24.40 43.90 45.50 24.50 43.80 45.50 24.60 43.60 45.40 24.70 43.40 45.30 24.80 43.20 45.20 24.90 43.00 45.10 25.00 42.80 45.00 25.10 42.70 44.90 25.20 42.60 44.80 25.30 42.40 44.80 25.40 42.40 44.70 25.50 42.30 44.60 25.60 42.20 44.50 25.70 42.10 44.40 25.80 42.20 44.30 25.90 42.40 44.30 26.00 42.30 44.20 26.10 42.20 44.10 26.20 42.10 44.10 26.30 42.10 44.00 26.40 42.10 43.90 26.50 42.00 43.80 26.60 41.80 43.70 26.70 41.70 43.60 26.80 41.70 43.60 26.90 41.60 43.50 27.00 47.00 43.80 27.10 54.90 45.00 27.20 70.50 57.30 27.30 107.00 73.10 27.40 128.70 86.90 27.50 142.00 99.20 27.60 150.90 109.20 27.70 156.30 116.80 27.80 159.60 122.60 27.90 161.80 127.20 28.00 163.20 130.70 28.10 164.30 133.40 28.20 165.20 135.60 28.30 165.90 137.30 28.40 166.40 138.60 28.50 166.80 139.70 28.60 167.20 140.70 28.70 167.40 141.50 28.80 167.70 142.10 28.90 167.90 142.70 29.00 168.00 143.20 29.10 168.20 143.60 29.20 168.30 144.00 29.30 168.70 143.70 29.40 158.10 136.50 29.50 147.00 130.30 29.60 137.80 125.00 29.70 129.90 120.10 29.80 123.10 115.60 29.90 117.20 111.70 30.00 112.00 108.00 30.10 107.30 104.60 30.20 103.10 101.50 30.30 99.30 98.70 30.40 95.80 96.00 30.50 92.70 93.50 30.60 89.80 91.20 30.70 87.10 89.00 30.80 84.70 87.00 30.90 82.50 85.10 31.00 80.50 83.30 31.10 78.70 81.50 31.20 77.20 79.80 31.30 75.70 78.30 31.40 74.40 76.80 31.50 73.20 75.40 31.60 72.00 74.10 31.70 70.80 72.80 31.80 69.50 71.70 31.90 68.30 70.50 32.00 67.00 69.50 32.10 65.90 68.50 32.20 64.60 67.40 32.30 63.40 66.50 32.40 62.20 65.50 32.50 61.10 64.50 32.60 60.00 63.50 32.70 59.00 62.50 32.80 58.10 61.60 32.90 57.20 60.90 33.00 56.40 60.00 33.10 55.80 59.20 33.20 55.30 58.60 33.30 54.70 57.80 33.40 54.10 57.20 33.50 53.50 56.60 33.60 53.00 56.00 33.70 52.50 55.50 33.80 52.00 55.00 33.90 51.60 54.40 34.00 51.10 54.00 34.10 50.70 53.50 34.20 50.40 53.20 34.30 49.90 52.70 34.40 49.60 52.30 34.50 49.10 51.80 34.60 48.90 51.60 34.70 48.40 51.10 34.80 48.20 50.90 34.90 47.90 50.50 35.00 47.60 50.20 35.10 47.30 49.90 35.20 47.10 49.60 35.30 46.80 49.30 35.40 46.50 49.00 35.50 46.30 48.80 31.5 31.8 31.6 31.9 31.7 32 31.7 32 31.7 32.1 31.8 32.1 31.8 32.1 31.7 32.1 31.7 32.2 31.8 32.3 32 32.3 38.2 33.2 44.2 35.5 62.3 47.1 85.8 61.8 110 76.3 128.1 88.7 140.4 98.7 149 107.1 154.6 114 158.3 119.7 161 124.2 162.9 128.1 164.1 131.1 165.1 133.6 165.8 135.5 166.4 137 166.8 138.1 167.1 139.1 167.4 139.9 167.7 140.6 167.9 141.2 168 141.7 168.1 142.1 165.9 140 153.5 132.7 142.6 126.2 133.4 120.5 125.5 115.5 118.7 110.9 112.7 106.7 107.4 102.9 102.6 99.3 98.4 96.1 94.5 93.1 90.9 90.4 87.6 87.8 84.7 85.4 82 83.1 79.5 81 77.3 79 75.4 77 73.6 75.2 72 73.5 70.6 71.9 69.1 70.4 67.6 69 66.1 67.7 64.7 66.4 63.2 65.2 61.9 64 60.7 63 59.6 61.9 58.5 60.9 57.4 59.9 56.4 58.9 55.5 58 54.6 57.1 53.8 56.3 53.2 55.6 52.6 54.9 51.9 54.2 51.2 53.6 50.5 52.9 49.8 52.4 49.1 51.8 48.4 51.2 47.8 50.7 47.2 50 46.7 49.5 46.2 48.9 45.7 48.4 45.3 48 44.9 47.5 44.5 47.1 44.2 46.7 43.9 46.4 43.6 46.1 43.3 45.8 43.1 45.5 42.9 45.2 42.6 45 42.5 44.7 42.2 44.5 42 44.3 41.8 44 41.6 43.9 41.4 43.7 41.3 43.4 41.1 43.3 41 43 40.8 42.9 40.6 42.8 40.5 42.6 40.4 42.4 40.3 42.2 40.2 42.1 40 42 39.8 41.9 39.7 41.7 39.6 41.7 39.5 41.5 39.5 41.5 39.5 41.4 39.6 41.4 39.5 41.3 39.3 41.2 39.2 41.2 39.2 41.1 39.1 41 38.9 40.9 38.7 40.8 38.6 40.7 38.5 40.6 38.6 40.6 38.6 40.6 38.3 40.4 38.1 40.2 38 40.2 38.1 40.2 38 40.1 38.3 40.1 38.3 40.1 38.2 40 38.2 40.1 38.1 39.9 38.3 40 38.1 39.8 38.1 39.8 38.1 39.8 38.1 39.8 38 39.7 38 39.7 39.4 39.6 47.4 40.4 57.5 47.5 88.5 63.1 118.5 78.5 134.7 91.5 145.3 102.2 152.4 110.8 156.8 117.4 160 122.7 161.9 126.7 163.5 130.2 164.6 132.8 165.4 134.8 166.1 136.4 166.5 137.7 167 138.8 167.3 139.7 167.6 140.5 167.8 141.2 168 141.7 168.1 142.3 168.3 142.7 168.3 143 162.9 138.4 151.4 131.3 141.2 125.4 132.6 120.3 125.3 115.6 118.9 111.4 113.2 107.6 108.2 104 103.8 100.8 99.7 97.9 96.1 95.1 92.7 92.5 89.6 90 86.8 87.8 84.4 85.7 82.1 83.7 79.9 81.8 78 80 76.3 78.2 74.7 76.6 73.2 75.1 71.8 73.7 70.6 72.3 69.2 71 67.9 69.8 66.6 68.6 65.4 67.5 64.2 66.4 63.1 65.4 62 64.4 61 63.4 60.1 62.5 59.3 61.6 58.4 60.8 57.6 60 56.9 59.2 56.2 58.5 55.5 57.8 54.9 57.1 54.3 56.5 53.8 55.9 53.1 55.3 52.5 54.7 52 54.2 51.6 53.8 51.1 53.3 50.7 52.8 50.2 52.4 49.8 52 49.4 51.6 49 51.2 48.7 50.9 48.3 50.5 48.1 50.2 47.8 49.9 47.5 49.6 47.2 49.3 47 49.1 46.8 48.8 46.5 48.6 46.3 48.3 46.1 48.1 46 47.9 45.9 47.7 45.7 47.5 45.4 47.3 45.2 47.1 45.1 46.9 44.9 46.8 44.7 46.6 44.6 46.5 44.4 46.3 44.2 46.2 44.1 46 44 45.9 44 45.7 43.9 45.6 43.9 45.5 43.8 45.5 43.6 45.4 43.4 45.3 43.2 45.2 43 45.1 42.8 45 42.7 44.9 42.6 44.8 42.4 44.8 42.4 44.7 42.3 44.6 42.2 44.5 42.1 44.4 42.2 44.3 42.4 44.3 42.3 44.2 42.2 44.1 42.1 44.1 42.1 44 42.1 43.9 42 43.8 41.8 43.7 41.7 43.6 41.7 43.6 41.6 43.5 47 43.8 54.9 45 70.5 57.3 107 73.1 128.7 86.9 142 99.2 150.9 109.2 156.3 116.8 159.6 122.6 161.8 127.2 163.2 130.7 164.3 133.4 165.2 135.6 165.9 137.3 166.4 138.6 166.8 139.7 167.2 140.7 167.4 141.5 167.7 142.1 167.9 142.7 168 143.2 168.2 143.6 168.3 144 168.7 143.7 158.1 136.5 147 130.3 137.8 125 129.9 120.1 123.1 115.6 117.2 111.7 112 108 107.3 104.6 103.1 101.5 99.3 98.7 95.8 96 92.7 93.5 89.8 91.2 87.1 89 84.7 87 82.5 85.1 80.5 83.3 78.7 81.5 77.2 79.8 75.7 78.3 74.4 76.8 73.2 75.4 72 74.1 70.8 72.8 69.5 71.7 68.3 70.5 67 69.5 65.9 68.5 64.6 67.4 63.4 66.5 62.2 65.5 61.1 64.5 60 63.5 59 62.5 58.1 61.6 57.2 60.9 56.4 60 55.8 59.2 55.3 58.6 54.7 57.8 54.1 57.2 53.5 56.6 53 56 52.5 55.5 52 55 51.6 54.4 51.1 54 50.7 53.5 50.4 53.2 49.9 52.7 49.6 52.3 49.1 51.8 48.9 51.6 48.4 51.1 48.2 50.9 47.9 50.5 47.6 50.2 47.3 49.9 47.1 49.6 46.8 49.3 46.5 49 46.3 48.8 PP&PP at top side PP&Sealant at Al tab 0.00 31.50 30.80 0.10 31.50 30.90 0.20 31.30 31.00 0.30 31.20 31.00 0.40 31.40 31.10 0.50 31.90 31.30 0.60 35.80 31.60 0.70 40.60 32.60 0.80 51.80 47.60 0.90 81.00 69.40 1.00 101.30 84.50 1.10 113.40 95.50 1.20 121.90 103.80 1.30 129.50 110.00 1.40 134.90 114.70 1.50 139.10 118.70 1.60 141.70 122.10 1.70 144.10 125.00 1.80 145.80 127.50 1.90 147.30 129.40 2.00 148.40 131.10 2.10 149.20 132.40 2.20 150.20 133.60 2.30 150.80 134.60 2.40 151.40 135.40 2.50 151.80 136.10 2.60 152.20 136.70 2.70 152.70 137.20 2.80 153.00 137.70 2.90 153.20 138.10 3.00 153.50 138.40 3.10 153.70 138.70 3.20 153.80 139.00 3.30 153.80 139.20 3.40 154.00 139.40 3.50 154.10 139.70 3.60 154.30 139.90 3.70 154.40 140.00 3.80 154.50 140.20 3.90 175.10 137.80 4.00 145.60 131.00 4.10 134.90 125.20 4.20 126.50 120.00 4.30 119.30 115.20 4.40 113.10 110.90 4.50 107.90 107.00 4.60 103.60 103.30 4.70 104.50 100.00 4.80 100.30 96.90 4.90 92.30 94.00 5.00 99.80 91.20 5.10 76.90 81.60 5.20 74.80 79.40 5.30 72.90 77.40 5.40 71.10 75.60 5.50 69.50 73.80 5.60 68.00 72.20 5.70 66.50 70.60 5.80 65.00 69.10 5.90 63.60 67.70 6.00 62.40 66.40 6.10 61.10 65.20 6.20 59.90 64.00 6.30 58.80 62.80 6.40 57.70 61.80 6.50 56.70 60.80 6.60 55.80 59.80 6.70 55.00 58.80 6.80 54.20 57.90 6.90 53.40 57.10 7.00 52.60 56.30 7.10 51.90 55.50 7.20 51.30 54.80 7.30 50.70 54.10 7.40 50.10 53.50 7.50 49.50 52.80 7.60 49.00 52.30 7.70 48.40 51.70 7.80 48.00 51.20 7.90 47.50 50.60 8.00 47.20 50.20 8.10 46.70 49.70 8.20 46.40 49.30 8.30 46.00 48.80 8.40 45.60 48.40 8.50 45.30 48.00 8.60 45.00 47.70 8.70 44.60 47.40 8.80 44.30 47.00 8.90 44.10 46.70 9.00 43.90 46.40 9.10 43.60 46.10 9.20 43.40 45.90 9.30 43.20 45.60 9.40 42.90 45.30 9.50 42.70 45.10 9.60 42.60 44.90 9.70 42.40 44.70 9.80 42.10 44.40 9.90 41.90 44.20 10.00 41.70 44.10 10.10 41.60 43.80 10.20 41.40 43.60 10.30 41.20 43.50 10.40 41.00 43.30 10.50 40.80 43.10 10.60 40.70 43.00 10.70 40.50 42.80 10.80 40.40 42.70 10.90 40.30 42.50 11.00 40.20 42.40 11.10 40.20 42.20 11.20 40.20 42.10 11.30 40.00 42.10 11.40 39.80 42.00 11.50 39.70 41.90 11.60 39.60 41.80 11.70 39.60 41.80 11.80 39.60 41.70 11.90 39.50 41.60 12.00 39.50 41.50 12.10 39.30 41.30 12.20 39.30 41.20 12.30 39.30 41.30 12.40 39.30 41.20 12.50 44.00 41.50 12.60 53.90 47.50 12.70 84.70 68.00 12.80 106.00 82.80 12.90 120.10 94.60 13.00 127.80 104.00 13.10 133.80 111.70 13.20 139.00 118.10 13.30 142.90 123.10 13.40 145.90 126.90 13.50 147.90 129.90 13.60 149.40 132.30 13.70 150.70 134.30 13.80 151.70 135.90 13.90 152.50 137.20 14.00 153.30 138.20 14.10 153.80 139.10 14.20 154.30 139.90 14.30 154.70 140.50 14.40 155.10 140.90 14.50 155.30 141.40 14.60 155.50 141.80 14.70 155.70 142.00 14.80 156.00 142.30 14.90 156.00 142.50 15.00 156.20 142.70 15.10 156.40 142.90 15.20 156.40 143.10 15.30 156.60 143.20 15.40 156.70 143.30 15.50 156.70 143.50 15.60 156.80 143.60 15.70 157.30 143.70 15.80 83.90 87.50 15.90 82.30 85.30 16.00 78.60 83.20 16.10 76.30 81.30 16.20 74.40 79.40 16.30 72.80 77.70 16.40 71.30 76.00 16.50 69.80 74.50 16.60 68.40 73.00 16.70 67.00 71.70 16.80 65.80 70.30 16.90 64.50 69.10 17.00 63.40 68.00 17.10 62.20 66.80 17.20 61.20 65.80 17.30 60.30 64.80 17.40 59.30 63.80 17.50 58.40 62.90 17.60 57.60 62.10 17.70 56.80 61.20 17.80 56.10 60.40 17.90 55.50 59.60 18.00 54.80 58.90 18.10 54.30 58.20 18.20 53.80 57.60 18.30 53.30 57.10 18.40 52.70 56.50 18.50 52.20 56.00 18.60 51.70 55.40 18.70 51.30 54.90 18.80 50.90 54.40 18.90 50.50 54.00 19.00 50.20 53.50 19.10 49.70 53.10 19.20 49.40 52.70 19.30 49.00 52.40 19.40 48.70 52.00 19.50 48.50 51.70 19.60 48.30 51.30 19.70 48.00 51.00 19.80 47.70 50.70 19.90 47.40 50.40 20.00 47.20 50.10 20.10 46.90 49.80 20.20 46.60 49.60 20.30 46.50 49.30 20.40 46.20 49.10 20.50 46.00 48.80 20.60 45.80 48.60 20.70 45.60 48.40 20.80 49.60 48.40 20.90 55.60 50.50 21.00 97.30 71.20 21.10 113.20 87.30 21.20 125.20 99.30 21.30 133.60 108.80 21.40 139.30 116.20 21.50 143.40 121.90 21.60 146.30 126.20 21.70 148.40 129.70 21.80 150.10 132.40 21.90 151.50 134.60 22.00 152.60 136.40 22.10 153.40 137.80 22.20 154.10 139.00 22.30 154.70 139.90 22.40 155.20 140.70 22.50 155.60 141.30 22.60 156.00 141.80 22.70 156.30 142.30 22.80 156.50 142.60 22.90 156.80 142.90 23.00 157.00 143.20 23.10 157.20 143.50 23.20 157.40 143.70 23.30 157.50 143.90 23.40 157.60 144.00 23.50 157.70 144.10 23.60 157.80 144.30 23.70 157.90 144.40 23.80 158.00 144.50 23.90 158.00 144.60 24.00 158.00 144.70 24.10 111.30 144.70 24.20 136.50 131.70 24.30 128.80 126.40 24.40 122.30 121.50 24.50 116.70 117.10 24.60 111.60 113.10 24.70 107.10 109.40 24.80 103.00 106.00 24.90 99.40 102.70 25.00 96.00 99.90 25.10 93.00 97.10 25.20 90.20 94.70 25.30 87.60 92.30 25.40 85.20 90.00 25.50 83.10 88.00 25.60 81.10 85.90 25.70 79.20 84.10 25.80 77.50 82.30 25.90 75.90 80.50 26.00 74.40 78.90 26.10 73.00 77.40 26.20 71.70 75.90 26.30 70.50 74.60 26.40 69.20 73.30 26.50 68.00 72.10 26.60 66.80 71.00 26.70 65.80 70.00 26.80 64.60 68.90 26.90 63.50 67.90 27.00 62.40 66.80 27.10 61.40 65.90 27.20 60.40 64.90 27.30 59.50 63.90 27.40 58.70 63.00 27.50 57.90 62.10 27.60 57.10 61.20 27.70 56.40 60.40 27.80 55.70 59.70 27.90 54.90 58.70 28.00 54.20 57.90 28.10 53.70 57.30 28.20 53.30 56.70 28.30 52.80 56.10 28.40 52.40 55.60 28.50 52.00 55.10 28.60 51.50 54.60 28.70 51.20 54.10 28.80 50.80 53.60 28.90 50.40 53.20 29.00 50.00 52.80 29.10 49.80 52.50 29.20 49.50 52.20 29.30 49.20 51.80 29.40 48.70 51.40 29.50 48.50 51.10 29.60 48.20 50.80 29.70 47.90 50.50 29.80 47.70 50.20 29.90 47.50 49.90 30.00 47.20 49.60 30.10 47.00 49.40 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 PP&PP at top side PP&Sealant at Al tab _1209303707.xls 图表2 43.9 31.1 43.5 31.1 43.6 31.1 43.2 31.1 43 31.2 43 31.2 42.7 31.3 42.2 31.3 41.8 31.4 40.9 31.4 40.1 31.4 39.7 31.5 39 31.5 38.2 31.5 37.9 31.5 37.6 31.5 37.3 31.5 37.1 31.6 37.2 31.6 37.8 31.6 37.8 31.6 38.7 31.7 40.2 35.4 63.3 52.3 87.7 71.3 104.6 84.7 116 94.5 125.1 102.7 135 111.1 142 118.8 146.3 124.5 149.6 128.5 152.5 131.4 155.2 133.7 157.6 135.4 159.5 136.8 161 138 162.3 138.9 163.2 139.6 163.9 140.2 164.5 140.8 165 141.2 165.4 141.6 165.7 141.9 165.9 142.2 166 142.5 166.2 142.7 166.3 142.9 166.4 143.1 166.5 143.3 166.7 143.4 166.7 143.6 166.8 143.8 166.8 143.9 164.7 141.4 155 134 144.7 128.1 135.7 122.9 128 118.2 121.2 113.9 115.3 109.9 110 106.2 105.3 102.8 101 99.7 97 96.7 93.5 94 90.2 91.4 87.2 88.9 84.5 86.6 81.9 84.5 79.5 82.4 77.6 80.5 75.8 78.6 74.2 76.9 72.7 75.2 71.3 73.7 70 72.3 68.5 70.9 67 69.7 65.4 68.5 64 67.3 62.8 66.2 61.6 65.2 60.5 64.1 59.4 63.2 58.5 62.2 57.6 61.3 56.7 60.4 55.9 59.6 55 58.7 54.3 57.9 53.6 57.2 52.9 56.4 52.3 55.8 51.6 55.2 51.1 54.5 50.4 53.9 51 53.5 57.5 53.5 67.4 58.9 90.5 71.5 116 84.4 131.1 96.1 142.5 106.6 150.7 114.9 156 121.7 159.2 127 161.4 130.9 162.8 133.7 163.8 135.8 164.6 137.5 165.2 138.8 165.7 139.8 166.1 140.7 166.4 141.4 166.6 142 166.8 142.4 167 142.8 167.2 143.2 167.3 143.5 167.4 143.8 167.5 144 167.6 144.3 167.6 144.4 167.7 144.6 167.8 144.7 167.8 144.8 167.8 145 167.9 145.1 167.9 145.2 167.7 145.2 163.4 141 152.3 134.4 142.9 129 134.7 124.2 127.7 119.8 121.6 115.7 116.1 112 111.2 108.5 106.9 105.2 102.9 102.3 99.3 99.5 96.1 97 93.1 94.5 90.3 92.2 87.7 90 85.3 88 83.1 86.1 81.1 84.4 79.4 82.7 77.8 81.1 76.4 79.6 75.1 78.1 73.9 76.7 72.8 75.4 71.6 74.2 70.4 73 69.1 71.9 67.9 70.9 66.7 69.9 65.5 68.9 64.5 68 63.6 67.1 62.7 66.3 61.8 65.4 60.9 64.7 60 63.9 59.2 63.1 58.5 62.4 57.8 61.7 57.2 61 56.5 60.3 55.8 59.7 55.2 59 54.8 58.5 54.3 58 53.9 57.5 53.5 57 53 56.5 52.5 56 52.2 55.5 51.9 55.1 51.5 54.7 51.1 54.3 50.7 54 50.4 53.6 51.8 53.3 58.8 53.8 68.6 59.3 88 71 109.9 83.1 125 92.8 138.4 102.5 148.8 111.6 155.3 118.7 159.1 124.3 161.4 128.6 162.9 132 163.9 134.4 164.8 136.4 165.3 137.9 165.8 139.1 166.2 140.1 166.5 140.9 166.8 141.6 167 142.2 167.2 142.7 167.3 143 167.4 143.4 167.6 143.8 167.6 144.1 167.7 144.3 167.8 144.6 167.9 144.7 167.9 145 168 145.1 168 145.3 168 145.4 168.1 145.5 167.9 145.4 162.8 140.8 150.7 134.6 141.7 129.2 133.9 124.5 127.2 120.1 121.3 116.2 116.1 112.5 111.4 109.1 107.2 106.1 103.4 103.2 100 100.6 96.8 98 93.9 95.7 91.2 93.5 88.6 91.4 86.4 89.4 84.3 87.5 82.5 85.8 80.7 84.2 79.2 82.7 77.8 81.3 76.5 79.9 75.4 78.5 74.3 77.3 73.2 76.1 72 75 70.9 73.9 69.8 72.9 68.6 71.9 67.6 70.9 66.6 70 65.7 69.2 64.8 68.3 64 67.5 63.2 66.7 62.4 66 61.6 65.3 60.8 64.5 60 63.8 59.2 63 58.4 62.3 57.8 61.6 57.3 60.9 56.7 60.2 56.3 59.7 55.8 59.1 55.1 58.4 54.6 57.9 54.1 57.3 53.7 56.8 53.3 56.2 52.9 55.7 52.5 55.3 52.1 54.8 51.7 54.4 51.3 54 PP&PP at top side PP&Sealant at AL tab Time/s Temp/ºC Temp rise curve Sum Top sealing temp trend for 604396 at SSL factory Top sealing time interval 2s Top sealing time interval 3s Conclusion: For PP&Sealant,the temperature reach 140ºC from RT need 1.5s,the highest is 145ºC. For PP&PP,need0.8~1.0s,the temperature over160ºC and the hightest is 168ºC. Top sealing time interval 3s Sum 31.5 30.8 31.5 30.9 31.3 31 31.2 31 31.4 31.1 31.9 31.3 35.8 31.6 40.6 32.6 51.8 47.6 81 69.4 101.3 84.5 113.4 95.5 121.9 103.8 129.5 110 134.9 114.7 139.1 118.7 141.7 122.1 144.1 125 145.8 127.5 147.3 129.4 148.4 131.1 149.2 132.4 150.2 133.6 150.8 134.6 151.4 135.4 151.8 136.1 152.2 136.7 152.7 137.2 153 137.7 153.2 138.1 153.5 138.4 153.7 138.7 153.8 139 153.8 139.2 154 139.4 154.1 139.7 154.3 139.9 154.4 140 154.5 140.2 175.1 137.8 145.6 131 134.9 125.2 126.5 120 119.3 115.2 113.1 110.9 107.9 107 103.6 103.3 104.5 100 100.3 96.9 92.3 94 99.8 91.2 76.9 81.6 74.8 79.4 72.9 77.4 71.1 75.6 69.5 73.8 68 72.2 66.5 70.6 65 69.1 63.6 67.7 62.4 66.4 61.1 65.2 59.9 64 58.8 62.8 57.7 61.8 56.7 60.8 55.8 59.8 55 58.8 54.2 57.9 53.4 57.1 52.6 56.3 51.9 55.5 51.3 54.8 50.7 54.1 50.1 53.5 49.5 52.8 49 52.3 48.4 51.7 48 51.2 47.5 50.6 47.2 50.2 46.7 49.7 46.4 49.3 46 48.8 45.6 48.4 45.3 48 45 47.7 44.6 47.4 44.3 47 44.1 46.7 43.9 46.4 43.6 46.1 43.4 45.9 43.2 45.6 42.9 45.3 42.7 45.1 42.6 44.9 42.4 44.7 42.1 44.4 41.9 44.2 41.7 44.1 41.6 43.8 41.4 43.6 41.2 43.5 41 43.3 40.8 43.1 40.7 43 40.5 42.8 40.4 42.7 40.3 42.5 40.2 42.4 40.2 42.2 40.2 42.1 40 42.1 39.8 42 39.7 41.9 39.6 41.8 39.6 41.8 39.6 41.7 39.5 41.6 39.5 41.5 39.3 41.3 39.3 41.2 39.3 41.3 39.3 41.2 44 41.5 53.9 47.5 84.7 68 106 82.8 120.1 94.6 127.8 104 133.8 111.7 139 118.1 142.9 123.1 145.9 126.9 147.9 129.9 149.4 132.3 150.7 134.3 151.7 135.9 152.5 137.2 153.3 138.2 153.8 139.1 154.3 139.9 154.7 140.5 155.1 140.9 155.3 141.4 155.5 141.8 155.7 142 156 142.3 156 142.5 156.2 142.7 156.4 142.9 156.4 143.1 156.6 143.2 156.7 143.3 156.7 143.5 156.8 143.6 157.3 143.7 83.9 87.5 82.3 85.3 78.6 83.2 76.3 81.3 74.4 79.4 72.8 77.7 71.3 76 69.8 74.5 68.4 73 67 71.7 65.8 70.3 64.5 69.1 63.4 68 62.2 66.8 61.2 65.8 60.3 64.8 59.3 63.8 58.4 62.9 57.6 62.1 56.8 61.2 56.1 60.4 55.5 59.6 54.8 58.9 54.3 58.2 53.8 57.6 53.3 57.1 52.7 56.5 52.2 56 51.7 55.4 51.3 54.9 50.9 54.4 50.5 54 50.2 53.5 49.7 53.1 49.4 52.7 49 52.4 48.7 52 48.5 51.7 48.3 51.3 48 51 47.7 50.7 47.4 50.4 47.2 50.1 46.9 49.8 46.6 49.6 46.5 49.3 46.2 49.1 46 48.8 45.8 48.6 45.6 48.4 49.6 48.4 55.6 50.5 97.3 71.2 113.2 87.3 125.2 99.3 133.6 108.8 139.3 116.2 143.4 121.9 146.3 126.2 148.4 129.7 150.1 132.4 151.5 134.6 152.6 136.4 153.4 137.8 154.1 139 154.7 139.9 155.2 140.7 155.6 141.3 156 141.8 156.3 142.3 156.5 142.6 156.8 142.9 157 143.2 157.2 143.5 157.4 143.7 157.5 143.9 157.6 144 157.7 144.1 157.8 144.3 157.9 144.4 158 144.5 158 144.6 158 144.7 111.3 144.7 136.5 131.7 128.8 126.4 122.3 121.5 116.7 117.1 111.6 113.1 107.1 109.4 103 106 99.4 102.7 96 99.9 93 97.1 90.2 94.7 87.6 92.3 85.2 90 83.1 88 81.1 85.9 79.2 84.1 77.5 82.3 75.9 80.5 74.4 78.9 73 77.4 71.7 75.9 70.5 74.6 69.2 73.3 68 72.1 66.8 71 65.8 70 64.6 68.9 63.5 67.9 62.4 66.8 61.4 65.9 60.4 64.9 59.5 63.9 58.7 63 57.9 62.1 57.1 61.2 56.4 60.4 55.7 59.7 54.9 58.7 54.2 57.9 53.7 57.3 53.3 56.7 52.8 56.1 52.4 55.6 52 55.1 51.5 54.6 51.2 54.1 50.8 53.6 50.4 53.2 50 52.8 49.8 52.5 49.5 52.2 49.2 51.8 48.7 51.4 48.5 51.1 48.2 50.8 47.9 50.5 47.7 50.2 47.5 49.9 47.2 49.6 47 49.4 PP&PP at top side PP&Sealant at Al tab Time/s Temp/ºC Temp rise curve 34 31.5 31.8 31.6 31.9 31.7 32 31.7 32 31.7 32.1 31.8 32.1 31.8 32.1 31.7 32.1 31.7 32.2 31.8 32.3 32 32.3 38.2 33.2 44.2 35.5 62.3 47.1 85.8 61.8 110 76.3 128.1 88.7 140.4 98.7 149 107.1 154.6 114 158.3 119.7 161 124.2 162.9 128.1 164.1 131.1 165.1 133.6 165.8 135.5 166.4 137 166.8 138.1 167.1 139.1 167.4 139.9 167.7 140.6 167.9 141.2 168 141.7 168.1 142.1 165.9 140 153.5 132.7 142.6 126.2 133.4 120.5 125.5 115.5 118.7 110.9 112.7 106.7 107.4 102.9 102.6 99.3 98.4 96.1 94.5 93.1 90.9 90.4 87.6 87.8 84.7 85.4 82 83.1 79.5 81 77.3 79 75.4 77 73.6 75.2 72 73.5 70.6 71.9 69.1 70.4 67.6 69 66.1 67.7 64.7 66.4 63.2 65.2 61.9 64 60.7 63 59.6 61.9 58.5 60.9 57.4 59.9 56.4 58.9 55.5 58 54.6 57.1 53.8 56.3 53.2 55.6 52.6 54.9 51.9 54.2 51.2 53.6 50.5 52.9 49.8 52.4 49.1 51.8 48.4 51.2 47.8 50.7 47.2 50 46.7 49.5 46.2 48.9 45.7 48.4 45.3 48 44.9 47.5 44.5 47.1 44.2 46.7 43.9 46.4 43.6 46.1 43.3 45.8 43.1 45.5 42.9 45.2 42.6 45 42.5 44.7 42.2 44.5 42 44.3 41.8 44 41.6 43.9 41.4 43.7 41.3 43.4 41.1 43.3 41 43 40.8 42.9 40.6 42.8 40.5 42.6 40.4 42.4 40.3 42.2 40.2 42.1 40 42 39.8 41.9 39.7 41.7 39.6 41.7 39.5 41.5 39.5 41.5 39.5 41.4 39.6 41.4 39.5 41.3 39.3 41.2 39.2 41.2 39.2 41.1 39.1 41 38.9 40.9 38.7 40.8 38.6 40.7 38.5 40.6 38.6 40.6 38.6 40.6 38.3 40.4 38.1 40.2 38 40.2 38.1 40.2 38 40.1 38.3 40.1 38.3 40.1 38.2 40 38.2 40.1 38.1 39.9 38.3 40 38.1 39.8 38.1 39.8 38.1 39.8 38.1 39.8 38 39.7 38 39.7 39.4 39.6 47.4 40.4 57.5 47.5 88.5 63.1 118.5 78.5 134.7 91.5 145.3 102.2 152.4 110.8 156.8 117.4 160 122.7 161.9 126.7 163.5 130.2 164.6 132.8 165.4 134.8 166.1 136.4 166.5 137.7 167 138.8 167.3 139.7 167.6 140.5 167.8 141.2 168 141.7 168.1 142.3 168.3 142.7 168.3 143 162.9 138.4 151.4 131.3 141.2 125.4 132.6 120.3 125.3 115.6 118.9 111.4 113.2 107.6 108.2 104 103.8 100.8 99.7 97.9 96.1 95.1 92.7 92.5 89.6 90 86.8 87.8 84.4 85.7 82.1 83.7 79.9 81.8 78 80 76.3 78.2 74.7 76.6 73.2 75.1 71.8 73.7 70.6 72.3 69.2 71 67.9 69.8 66.6 68.6 65.4 67.5 64.2 66.4 63.1 65.4 62 64.4 61 63.4 60.1 62.5 59.3 61.6 58.4 60.8 57.6 60 56.9 59.2 56.2 58.5 55.5 57.8 54.9 57.1 54.3 56.5 53.8 55.9 53.1 55.3 52.5 54.7 52 54.2 51.6 53.8 51.1 53.3 50.7 52.8 50.2 52.4 49.8 52 49.4 51.6 49 51.2 48.7 50.9 48.3 50.5 48.1 50.2 47.8 49.9 47.5 49.6 47.2 49.3 47 49.1 46.8 48.8 46.5 48.6 46.3 48.3 46.1 48.1 46 47.9 45.9 47.7 45.7 47.5 45.4 47.3 45.2 47.1 45.1 46.9 44.9 46.8 44.7 46.6 44.6 46.5 44.4 46.3 44.2 46.2 44.1 46 44 45.9 44 45.7 43.9 45.6 43.9 45.5 43.8 45.5 43.6 45.4 43.4 45.3 43.2 45.2 43 45.1 42.8 45 42.7 44.9 42.6 44.8 42.4 44.8 42.4 44.7 42.3 44.6 42.2 44.5 42.1 44.4 42.2 44.3 42.4 44.3 42.3 44.2 42.2 44.1 42.1 44.1 42.1 44 42.1 43.9 42 43.8 41.8 43.7 41.7 43.6 41.7 43.6 41.6 43.5 47 43.8 54.9 45 70.5 57.3 107 73.1 128.7 86.9 142 99.2 150.9 109.2 156.3 116.8 159.6 122.6 161.8 127.2 163.2 130.7 164.3 133.4 165.2 135.6 165.9 137.3 166.4 138.6 166.8 139.7 167.2 140.7 167.4 141.5 167.7 142.1 167.9 142.7 168 143.2 168.2 143.6 168.3 144 168.7 143.7 158.1 136.5 147 130.3 137.8 125 129.9 120.1 123.1 115.6 117.2 111.7 112 108 107.3 104.6 103.1 101.5 99.3 98.7 95.8 96 92.7 93.5 89.8 91.2 87.1 89 84.7 87 82.5 85.1 80.5 83.3 78.7 81.5 77.2 79.8 75.7 78.3 74.4 76.8 73.2 75.4 72 74.1 70.8 72.8 69.5 71.7 68.3 70.5 67 69.5 65.9 68.5 64.6 67.4 63.4 66.5 62.2 65.5 61.1 64.5 60 63.5 59 62.5 58.1 61.6 57.2 60.9 56.4 60 55.8 59.2 55.3 58.6 54.7 57.8 54.1 57.2 53.5 56.6 53 56 52.5 55.5 52 55 51.6 54.4 51.1 54 50.7 53.5 50.4 53.2 49.9 52.7 49.6 52.3 49.1 51.8 48.9 51.6 48.4 51.1 48.2 50.9 47.9 50.5 47.6 50.2 47.3 49.9 47.1 49.6 46.8 49.3 46.5 49 46.3 48.8 PP&PP at top side PP&Sealant at Al tab Time/s Temp/ºC Temp rise curve 35 43.9 31.1 43.5 31.1 43.6 31.1 43.2 31.1 43 31.2 43 31.2 42.7 31.3 42.2 31.3 41.8 31.4 40.9 31.4 40.1 31.4 39.7 31.5 39 31.5 38.2 31.5 37.9 31.5 37.6 31.5 37.3 31.5 37.1 31.6 37.2 31.6 37.8 31.6 37.8 31.6 38.7 31.7 40.2 35.4 63.3 52.3 87.7 71.3 104.6 84.7 116 94.5 125.1 102.7 135 111.1 142 118.8 146.3 124.5 149.6 128.5 152.5 131.4 155.2 133.7 157.6 135.4 159.5 136.8 161 138 162.3 138.9 163.2 139.6 163.9 140.2 164.5 140.8 165 141.2 165.4 141.6 165.7 141.9 165.9 142.2 166 142.5 166.2 142.7 166.3 142.9 166.4 143.1 166.5 143.3 166.7 143.4 166.7 143.6 166.8 143.8 166.8 143.9 164.7 141.4 155 134 144.7 128.1 135.7 122.9 128 118.2 121.2 113.9 115.3 109.9 110 106.2 105.3 102.8 101 99.7 97 96.7 93.5 94 90.2 91.4 87.2 88.9 84.5 86.6 81.9 84.5 79.5 82.4 77.6 80.5 75.8 78.6 74.2 76.9 72.7 75.2 71.3 73.7 70 72.3 68.5 70.9 67 69.7 65.4 68.5 64 67.3 62.8 66.2 61.6 65.2 60.5 64.1 59.4 63.2 58.5 62.2 57.6 61.3 56.7 60.4 55.9 59.6 55 58.7 54.3 57.9 53.6 57.2 52.9 56.4 52.3 55.8 51.6 55.2 51.1 54.5 50.4 53.9 51 53.5 57.5 53.5 67.4 58.9 90.5 71.5 116 84.4 131.1 96.1 142.5 106.6 150.7 114.9 156 121.7 159.2 127 161.4 130.9 162.8 133.7 163.8 135.8 164.6 137.5 165.2 138.8 165.7 139.8 166.1 140.7 166.4 141.4 166.6 142 166.8 142.4 167 142.8 167.2 143.2 167.3 143.5 167.4 143.8 167.5 144 167.6 144.3 167.6 144.4 167.7 144.6 167.8 144.7 167.8 144.8 167.8 145 167.9 145.1 167.9 145.2 167.7 145.2 163.4 141 152.3 134.4 142.9 129 134.7 124.2 127.7 119.8 121.6 115.7 116.1 112 111.2 108.5 106.9 105.2 102.9 102.3 99.3 99.5 96.1 97 93.1 94.5 90.3 92.2 87.7 90 85.3 88 83.1 86.1 81.1 84.4 79.4 82.7 77.8 81.1 76.4 79.6 75.1 78.1 73.9 76.7 72.8 75.4 71.6 74.2 70.4 73 69.1 71.9 67.9 70.9 66.7 69.9 65.5 68.9 64.5 68 63.6 67.1 62.7 66.3 61.8 65.4 60.9 64.7 60 63.9 59.2 63.1 58.5 62.4 57.8 61.7 57.2 61 56.5 60.3 55.8 59.7 55.2 59 54.8 58.5 54.3 58 53.9 57.5 53.5 57 53 56.5 52.5 56 52.2 55.5 51.9 55.1 51.5 54.7 51.1 54.3 50.7 54 50.4 53.6 51.8 53.3 58.8 53.8 68.6 59.3 88 71 109.9 83.1 125 92.8 138.4 102.5 148.8 111.6 155.3 118.7 159.1 124.3 161.4 128.6 162.9 132 163.9 134.4 164.8 136.4 165.3 137.9 165.8 139.1 166.2 140.1 166.5 140.9 166.8 141.6 167 142.2 167.2 142.7 167.3 143 167.4 143.4 167.6 143.8 167.6 144.1 167.7 144.3 167.8 144.6 167.9 144.7 167.9 145 168 145.1 168 145.3 168 145.4 168.1 145.5 167.9 145.4 162.8 140.8 150.7 134.6 141.7 129.2 133.9 124.5 127.2 120.1 121.3 116.2 116.1 112.5 111.4 109.1 107.2 106.1 103.4 103.2 100 100.6 96.8 98 93.9 95.7 91.2 93.5 88.6 91.4 86.4 89.4 84.3 87.5 82.5 85.8 80.7 84.2 79.2 82.7 77.8 81.3 76.5 79.9 75.4 78.5 74.3 77.3 73.2 76.1 72 75 70.9 73.9 69.8 72.9 68.6 71.9 67.6 70.9 66.6 70 65.7 69.2 64.8 68.3 64 67.5 63.2 66.7 62.4 66 61.6 65.3 60.8 64.5 60 63.8 59.2 63 58.4 62.3 57.8 61.6 57.3 60.9 56.7 60.2 56.3 59.7 55.8 59.1 55.1 58.4 54.6 57.9 54.1 57.3 53.7 56.8 53.3 56.2 52.9 55.7 52.5 55.3 52.1 54.8 51.7 54.4 51.3 54 PP&PP at top side PP&Sealant at AL tab Time/s Temp/ºC Temp rise curve AUTO0032 0.00 43.90 31.10 0.10 43.50 31.10 0.20 43.60 31.10 0.30 43.20 31.10 0.40 43.00 31.20 0.50 43.00 31.20 0.60 42.70 31.30 0.70 42.20 31.30 0.80 41.80 31.40 0.90 40.90 31.40 1.00 40.10 31.40 1.10 39.70 31.50 1.20 39.00 31.50 1.30 38.20 31.50 1.40 37.90 31.50 1.50 37.60 31.50 1.60 37.30 31.50 1.70 37.10 31.60 1.80 37.20 31.60 1.90 37.80 31.60 2.00 37.80 31.60 2.10 38.70 31.70 2.20 40.20 35.40 2.30 63.30 52.30 2.40 87.70 71.30 2.50 104.60 84.70 2.60 116.00 94.50 2.70 125.10 102.70 2.80 135.00 111.10 2.90 142.00 118.80 3.00 146.30 124.50 3.10 149.60 128.50 3.20 152.50 131.40 3.30 155.20 133.70 3.40 157.60 135.40 3.50 159.50 136.80 3.60 161.00 138.00 3.70 162.30 138.90 3.80 163.20 139.60 3.90 163.90 140.20 4.00 164.50 140.80 4.10 165.00 141.20 4.20 165.40 141.60 4.30 165.70 141.90 4.40 165.90 142.20 4.50 166.00 142.50 4.60 166.20 142.70 4.70 166.30 142.90 4.80 166.40 143.10 4.90 166.50 143.30 5.00 166.70 143.40 5.10 166.70 143.60 5.20 166.80 143.80 5.30 166.80 143.90 5.40 164.70 141.40 5.50 155.00 134.00 5.60 144.70 128.10 5.70 135.70 122.90 5.80 128.00 118.20 5.90 121.20 113.90 6.00 115.30 109.90 6.10 110.00 106.20 6.20 105.30 102.80 6.30 101.00 99.70 6.40 97.00 96.70 6.50 93.50 94.00 6.60 90.20 91.40 6.70 87.20 88.90 6.80 84.50 86.60 6.90 81.90 84.50 7.00 79.50 82.40 7.10 77.60 80.50 7.20 75.80 78.60 7.30 74.20 76.90 7.40 72.70 75.20 7.50 71.30 73.70 7.60 70.00 72.30 7.70 68.50 70.90 7.80 67.00 69.70 7.90 65.40 68.50 8.00 64.00 67.30 8.10 62.80 66.20 8.20 61.60 65.20 8.30 60.50 64.10 8.40 59.40 63.20 8.50 58.50 62.20 8.60 57.60 61.30 8.70 56.70 60.40 8.80 55.90 59.60 8.90 55.00 58.70 9.00 54.30 57.90 9.10 53.60 57.20 9.20 52.90 56.40 9.30 52.30 55.80 9.40 51.60 55.20 9.50 51.10 54.50 9.60 50.40 53.90 9.70 51.00 53.50 9.80 57.50 53.50 9.90 67.40 58.90 10.00 90.50 71.50 10.10 116.00 84.40 10.20 131.10 96.10 10.30 142.50 106.60 10.40 150.70 114.90 10.50 156.00 121.70 10.60 159.20 127.00 10.70 161.40 130.90 10.80 162.80 133.70 10.90 163.80 135.80 11.00 164.60 137.50 11.10 165.20 138.80 11.20 165.70 139.80 11.30 166.10 140.70 11.40 166.40 141.40 11.50 166.60 142.00 11.60 166.80 142.40 11.70 167.00 142.80 11.80 167.20 143.20 11.90 167.30 143.50 12.00 167.40 143.80 12.10 167.50 144.00 12.20 167.60 144.30 12.30 167.60 144.40 12.40 167.70 144.60 12.50 167.80 144.70 12.60 167.80 144.80 12.70 167.80 145.00 12.80 167.90 145.10 12.90 167.90 145.20 13.00 167.70 145.20 13.10 163.40 141.00 13.20 152.30 134.40 13.30 142.90 129.00 13.40 134.70 124.20 13.50 127.70 119.80 13.60 121.60 115.70 13.70 116.10 112.00 13.80 111.20 108.50 13.90 106.90 105.20 14.00 102.90 102.30 14.10 99.30 99.50 14.20 96.10 97.00 14.30 93.10 94.50 14.40 90.30 92.20 14.50 87.70 90.00 14.60 85.30 88.00 14.70 83.10 86.10 14.80 81.10 84.40 14.90 79.40 82.70 15.00 77.80 81.10 15.10 76.40 79.60 15.20 75.10 78.10 15.30 73.90 76.70 15.40 72.80 75.40 15.50 71.60 74.20 15.60 70.40 73.00 15.70 69.10 71.90 15.80 67.90 70.90 15.90 66.70 69.90 16.00 65.50 68.90 16.10 64.50 68.00 16.20 63.60 67.10 16.30 62.70 66.30 16.40 61.80 65.40 16.50 60.90 64.70 16.60 60.00 63.90 16.70 59.20 63.10 16.80 58.50 62.40 16.90 57.80 61.70 17.00 57.20 61.00 17.10 56.50 60.30 17.20 55.80 59.70 17.30 55.20 59.00 17.40 54.80 58.50 17.50 54.30 58.00 17.60 53.90 57.50 17.70 53.50 57.00 17.80 53.00 56.50 17.90 52.50 56.00 18.00 52.20 55.50 18.10 51.90 55.10 18.20 51.50 54.70 18.30 51.10 54.30 18.40 50.70 54.00 18.50 50.40 53.60 18.60 51.80 53.30 18.70 58.80 53.80 18.80 68.60 59.30 18.90 88.00 71.00 19.00 109.90 83.10 19.10 125.00 92.80 19.20 138.40 102.50 19.30 148.80 111.60 19.40 155.30 118.70 19.50 159.10 124.30 19.60 161.40 128.60 19.70 162.90 132.00 19.80 163.90 134.40 19.90 164.80 136.40 20.00 165.30 137.90 20.10 165.80 139.10 20.20 166.20 140.10 20.30 166.50 140.90 20.40 166.80 141.60 20.50 167.00 142.20 20.60 167.20 142.70 20.70 167.30 143.00 20.80 167.40 143.40 20.90 167.60 143.80 21.00 167.60 144.10 21.10 167.70 144.30 21.20 167.80 144.60 21.30 167.90 144.70 21.40 167.90 145.00 21.50 168.00 145.10 21.60 168.00 145.30 21.70 168.00 145.40 21.80 168.10 145.50 21.90 167.90 145.40 22.00 162.80 140.80 22.10 150.70 134.60 22.20 141.70 129.20 22.30 133.90 124.50 22.40 127.20 120.10 22.50 121.30 116.20 22.60 116.10 112.50 22.70 111.40 109.10 22.80 107.20 106.10 22.90 103.40 103.20 23.00 100.00 100.60 23.10 96.80 98.00 23.20 93.90 95.70 23.30 91.20 93.50 23.40 88.60 91.40 23.50 86.40 89.40 23.60 84.30 87.50 23.70 82.50 85.80 23.80 80.70 84.20 23.90 79.20 82.70 24.00 77.80 81.30 24.10 76.50 79.90 24.20 75.40 78.50 24.30 74.30 77.30 24.40 73.20 76.10 24.50 72.00 75.00 24.60 70.90 73.90 24.70 69.80 72.90 24.80 68.60 71.90 24.90 67.60 70.90 25.00 66.60 70.00 25.10 65.70 69.20 25.20 64.80 68.30 25.30 64.00 67.50 25.40 63.20 66.70 25.50 62.40 66.00 25.60 61.60 65.30 25.70 60.80 64.50 25.80 60.00 63.80 25.90 59.20 63.00 26.00 58.40 62.30 26.10 57.80 61.60 26.20 57.30 60.90 26.30 56.70 60.20 26.40 56.30 59.70 26.50 55.80 59.10 26.60 55.10 58.40 26.70 54.60 57.90 26.80 54.10 57.30 26.90 53.70 56.80 27.00 53.30 56.20 27.10 52.90 55.70 27.20 52.50 55.30 27.30 52.10 54.80 27.40 51.70 54.40 27.50 51.30 54.00 AUTO0032 43.9 31.1 43.5 31.1 43.6 31.1 43.2 31.1 43 31.2 43 31.2 42.7 31.3 42.2 31.3 41.8 31.4 40.9 31.4 40.1 31.4 39.7 31.5 39 31.5 38.2 31.5 37.9 31.5 37.6 31.5 37.3 31.5 37.1 31.6 37.2 31.6 37.8 31.6 37.8 31.6 38.7 31.7 40.2 35.4 63.3 52.3 87.7 71.3 104.6 84.7 116 94.5 125.1 102.7 135 111.1 142 118.8 146.3 124.5 149.6 128.5 152.5 131.4 155.2 133.7 157.6 135.4 159.5 136.8 161 138 162.3 138.9 163.2 139.6 163.9 140.2 164.5 140.8 165 141.2 165.4 141.6 165.7 141.9 165.9 142.2 166 142.5 166.2 142.7 166.3 142.9 166.4 143.1 166.5 143.3 166.7 143.4 166.7 143.6 166.8 143.8 166.8 143.9 164.7 141.4 155 134 144.7 128.1 135.7 122.9 128 118.2 121.2 113.9 115.3 109.9 110 106.2 105.3 102.8 101 99.7 97 96.7 93.5 94 90.2 91.4 87.2 88.9 84.5 86.6 81.9 84.5 79.5 82.4 77.6 80.5 75.8 78.6 74.2 76.9 72.7 75.2 71.3 73.7 70 72.3 68.5 70.9 67 69.7 65.4 68.5 64 67.3 62.8 66.2 61.6 65.2 60.5 64.1 59.4 63.2 58.5 62.2 57.6 61.3 56.7 60.4 55.9 59.6 55 58.7 54.3 57.9 53.6 57.2 52.9 56.4 52.3 55.8 51.6 55.2 51.1 54.5 50.4 53.9 51 53.5 57.5 53.5 67.4 58.9 90.5 71.5 116 84.4 131.1 96.1 142.5 106.6 150.7 114.9 156 121.7 159.2 127 161.4 130.9 162.8 133.7 163.8 135.8 164.6 137.5 165.2 138.8 165.7 139.8 166.1 140.7 166.4 141.4 166.6 142 166.8 142.4 167 142.8 167.2 143.2 167.3 143.5 167.4 143.8 167.5 144 167.6 144.3 167.6 144.4 167.7 144.6 167.8 144.7 167.8 144.8 167.8 145 167.9 145.1 167.9 145.2 167.7 145.2 163.4 141 152.3 134.4 142.9 129 134.7 124.2 127.7 119.8 121.6 115.7 116.1 112 111.2 108.5 106.9 105.2 102.9 102.3 99.3 99.5 96.1 97 93.1 94.5 90.3 92.2 87.7 90 85.3 88 83.1 86.1 81.1 84.4 79.4 82.7 77.8 81.1 76.4 79.6 75.1 78.1 73.9 76.7 72.8 75.4 71.6 74.2 70.4 73 69.1 71.9 67.9 70.9 66.7 69.9 65.5 68.9 64.5 68 63.6 67.1 62.7 66.3 61.8 65.4 60.9 64.7 60 63.9 59.2 63.1 58.5 62.4 57.8 61.7 57.2 61 56.5 60.3 55.8 59.7 55.2 59 54.8 58.5 54.3 58 53.9 57.5 53.5 57 53 56.5 52.5 56 52.2 55.5 51.9 55.1 51.5 54.7 51.1 54.3 50.7 54 50.4 53.6 51.8 53.3 58.8 53.8 68.6 59.3 88 71 109.9 83.1 125 92.8 138.4 102.5 148.8 111.6 155.3 118.7 159.1 124.3 161.4 128.6 162.9 132 163.9 134.4 164.8 136.4 165.3 137.9 165.8 139.1 166.2 140.1 166.5 140.9 166.8 141.6 167 142.2 167.2 142.7 167.3 143 167.4 143.4 167.6 143.8 167.6 144.1 167.7 144.3 167.8 144.6 167.9 144.7 167.9 145 168 145.1 168 145.3 168 145.4 168.1 145.5 167.9 145.4 162.8 140.8 150.7 134.6 141.7 129.2 133.9 124.5 127.2 120.1 121.3 116.2 116.1 112.5 111.4 109.1 107.2 106.1 103.4 103.2 100 100.6 96.8 98 93.9 95.7 91.2 93.5 88.6 91.4 86.4 89.4 84.3 87.5 82.5 85.8 80.7 84.2 79.2 82.7 77.8 81.3 76.5 79.9 75.4 78.5 74.3 77.3 73.2 76.1 72 75 70.9 73.9 69.8 72.9 68.6 71.9 67.6 70.9 66.6 70 65.7 69.2 64.8 68.3 64 67.5 63.2 66.7 62.4 66 61.6 65.3 60.8 64.5 60 63.8 59.2 63 58.4 62.3 57.8 61.6 57.3 60.9 56.7 60.2 56.3 59.7 55.8 59.1 55.1 58.4 54.6 57.9 54.1 57.3 53.7 56.8 53.3 56.2 52.9 55.7 52.5 55.3 52.1 54.8 51.7 54.4 51.3 54 PP&PP at top side PP&Sealant at AL tab 0.00 31.50 31.80 0.10 31.60 31.90 0.20 31.70 32.00 0.30 31.70 32.00 0.40 31.70 32.10 0.50 31.80 32.10 0.60 31.80 32.10 0.70 31.70 32.10 0.80 31.70 32.20 0.90 31.80 32.30 1.00 32.00 32.30 1.10 38.20 33.20 1.20 44.20 35.50 1.30 62.30 47.10 1.40 85.80 61.80 1.50 110.00 76.30 1.60 128.10 88.70 1.70 140.40 98.70 1.80 149.00 107.10 1.90 154.60 114.00 2.00 158.30 119.70 2.10 161.00 124.20 2.20 162.90 128.10 2.30 164.10 131.10 2.40 165.10 133.60 2.50 165.80 135.50 2.60 166.40 137.00 2.70 166.80 138.10 2.80 167.10 139.10 2.90 167.40 139.90 3.00 167.70 140.60 3.10 167.90 141.20 3.20 168.00 141.70 3.30 168.10 142.10 3.40 165.90 140.00 3.50 153.50 132.70 3.60 142.60 126.20 3.70 133.40 120.50 3.80 125.50 115.50 3.90 118.70 110.90 4.00 112.70 106.70 4.10 107.40 102.90 4.20 102.60 99.30 4.30 98.40 96.10 4.40 94.50 93.10 4.50 90.90 90.40 4.60 87.60 87.80 4.70 84.70 85.40 4.80 82.00 83.10 4.90 79.50 81.00 5.00 77.30 79.00 5.10 75.40 77.00 5.20 73.60 75.20 5.30 72.00 73.50 5.40 70.60 71.90 5.50 69.10 70.40 5.60 67.60 69.00 5.70 66.10 67.70 5.80 64.70 66.40 5.90 63.20 65.20 6.00 61.90 64.00 6.10 60.70 63.00 6.20 59.60 61.90 6.30 58.50 60.90 6.40 57.40 59.90 6.50 56.40 58.90 6.60 55.50 58.00 6.70 54.60 57.10 6.80 53.80 56.30 6.90 53.20 55.60 7.00 52.60 54.90 7.10 51.90 54.20 7.20 51.20 53.60 7.30 50.50 52.90 7.40 49.80 52.40 7.50 49.10 51.80 7.60 48.40 51.20 7.70 47.80 50.70 7.80 47.20 50.00 7.90 46.70 49.50 8.00 46.20 48.90 8.10 45.70 48.40 8.20 45.30 48.00 8.30 44.90 47.50 8.40 44.50 47.10 8.50 44.20 46.70 8.60 43.90 46.40 8.70 43.60 46.10 8.80 43.30 45.80 8.90 43.10 45.50 9.00 42.90 45.20 9.10 42.60 45.00 9.20 42.50 44.70 9.30 42.20 44.50 9.40 42.00 44.30 9.50 41.80 44.00 9.60 41.60 43.90 9.70 41.40 43.70 9.80 41.30 43.40 9.90 41.10 43.30 10.00 41.00 43.00 10.10 40.80 42.90 10.20 40.60 42.80 10.30 40.50 42.60 10.40 40.40 42.40 10.50 40.30 42.20 10.60 40.20 42.10 10.70 40.00 42.00 10.80 39.80 41.90 10.90 39.70 41.70 11.00 39.60 41.70 11.10 39.50 41.50 11.20 39.50 41.50 11.30 39.50 41.40 11.40 39.60 41.40 11.50 39.50 41.30 11.60 39.30 41.20 11.70 39.20 41.20 11.80 39.20 41.10 11.90 39.10 41.00 12.00 38.90 40.90 12.10 38.70 40.80 12.20 38.60 40.70 12.30 38.50 40.60 12.40 38.60 40.60 12.50 38.60 40.60 12.60 38.30 40.40 12.70 38.10 40.20 12.80 38.00 40.20 12.90 38.10 40.20 13.00 38.00 40.10 13.10 38.30 40.10 13.20 38.30 40.10 13.30 38.20 40.00 13.40 38.20 40.10 13.50 38.10 39.90 13.60 38.30 40.00 13.70 38.10 39.80 13.80 38.10 39.80 13.90 38.10 39.80 14.00 38.10 39.80 14.10 38.00 39.70 14.20 38.00 39.70 14.30 39.40 39.60 14.40 47.40 40.40 14.50 57.50 47.50 14.60 88.50 63.10 14.70 118.50 78.50 14.80 134.70 91.50 14.90 145.30 102.20 15.00 152.40 110.80 15.10 156.80 117.40 15.20 160.00 122.70 15.30 161.90 126.70 15.40 163.50 130.20 15.50 164.60 132.80 15.60 165.40 134.80 15.70 166.10 136.40 15.80 166.50 137.70 15.90 167.00 138.80 16.00 167.30 139.70 16.10 167.60 140.50 16.20 167.80 141.20 16.30 168.00 141.70 16.40 168.10 142.30 16.50 168.30 142.70 16.60 168.30 143.00 16.70 162.90 138.40 16.80 151.40 131.30 16.90 141.20 125.40 17.00 132.60 120.30 17.10 125.30 115.60 17.20 118.90 111.40 17.30 113.20 107.60 17.40 108.20 104.00 17.50 103.80 100.80 17.60 99.70 97.90 17.70 96.10 95.10 17.80 92.70 92.50 17.90 89.60 90.00 18.00 86.80 87.80 18.10 84.40 85.70 18.20 82.10 83.70 18.30 79.90 81.80 18.40 78.00 80.00 18.50 76.30 78.20 18.60 74.70 76.60 18.70 73.20 75.10 18.80 71.80 73.70 18.90 70.60 72.30 19.00 69.20 71.00 19.10 67.90 69.80 19.20 66.60 68.60 19.30 65.40 67.50 19.40 64.20 66.40 19.50 63.10 65.40 19.60 62.00 64.40 19.70 61.00 63.40 19.80 60.10 62.50 19.90 59.30 61.60 20.00 58.40 60.80 20.10 57.60 60.00 20.20 56.90 59.20 20.30 56.20 58.50 20.40 55.50 57.80 20.50 54.90 57.10 20.60 54.30 56.50 20.70 53.80 55.90 20.80 53.10 55.30 20.90 52.50 54.70 21.00 52.00 54.20 21.10 51.60 53.80 21.20 51.10 53.30 21.30 50.70 52.80 21.40 50.20 52.40 21.50 49.80 52.00 21.60 49.40 51.60 21.70 49.00 51.20 21.80 48.70 50.90 21.90 48.30 50.50 22.00 48.10 50.20 22.10 47.80 49.90 22.20 47.50 49.60 22.30 47.20 49.30 22.40 47.00 49.10 22.50 46.80 48.80 22.60 46.50 48.60 22.70 46.30 48.30 22.80 46.10 48.10 22.90 46.00 47.90 23.00 45.90 47.70 23.10 45.70 47.50 23.20 45.40 47.30 23.30 45.20 47.10 23.40 45.10 46.90 23.50 44.90 46.80 23.60 44.70 46.60 23.70 44.60 46.50 23.80 44.40 46.30 23.90 44.20 46.20 24.00 44.10 46.00 24.10 44.00 45.90 24.20 44.00 45.70 24.30 43.90 45.60 24.40 43.90 45.50 24.50 43.80 45.50 24.60 43.60 45.40 24.70 43.40 45.30 24.80 43.20 45.20 24.90 43.00 45.10 25.00 42.80 45.00 25.10 42.70 44.90 25.20 42.60 44.80 25.30 42.40 44.80 25.40 42.40 44.70 25.50 42.30 44.60 25.60 42.20 44.50 25.70 42.10 44.40 25.80 42.20 44.30 25.90 42.40 44.30 26.00 42.30 44.20 26.10 42.20 44.10 26.20 42.10 44.10 26.30 42.10 44.00 26.40 42.10 43.90 26.50 42.00 43.80 26.60 41.80 43.70 26.70 41.70 43.60 26.80 41.70 43.60 26.90 41.60 43.50 27.00 47.00 43.80 27.10 54.90 45.00 27.20 70.50 57.30 27.30 107.00 73.10 27.40 128.70 86.90 27.50 142.00 99.20 27.60 150.90 109.20 27.70 156.30 116.80 27.80 159.60 122.60 27.90 161.80 127.20 28.00 163.20 130.70 28.10 164.30 133.40 28.20 165.20 135.60 28.30 165.90 137.30 28.40 166.40 138.60 28.50 166.80 139.70 28.60 167.20 140.70 28.70 167.40 141.50 28.80 167.70 142.10 28.90 167.90 142.70 29.00 168.00 143.20 29.10 168.20 143.60 29.20 168.30 144.00 29.30 168.70 143.70 29.40 158.10 136.50 29.50 147.00 130.30 29.60 137.80 125.00 29.70 129.90 120.10 29.80 123.10 115.60 29.90 117.20 111.70 30.00 112.00 108.00 30.10 107.30 104.60 30.20 103.10 101.50 30.30 99.30 98.70 30.40 95.80 96.00 30.50 92.70 93.50 30.60 89.80 91.20 30.70 87.10 89.00 30.80 84.70 87.00 30.90 82.50 85.10 31.00 80.50 83.30 31.10 78.70 81.50 31.20 77.20 79.80 31.30 75.70 78.30 31.40 74.40 76.80 31.50 73.20 75.40 31.60 72.00 74.10 31.70 70.80 72.80 31.80 69.50 71.70 31.90 68.30 70.50 32.00 67.00 69.50 32.10 65.90 68.50 32.20 64.60 67.40 32.30 63.40 66.50 32.40 62.20 65.50 32.50 61.10 64.50 32.60 60.00 63.50 32.70 59.00 62.50 32.80 58.10 61.60 32.90 57.20 60.90 33.00 56.40 60.00 33.10 55.80 59.20 33.20 55.30 58.60 33.30 54.70 57.80 33.40 54.10 57.20 33.50 53.50 56.60 33.60 53.00 56.00 33.70 52.50 55.50 33.80 52.00 55.00 33.90 51.60 54.40 34.00 51.10 54.00 34.10 50.70 53.50 34.20 50.40 53.20 34.30 49.90 52.70 34.40 49.60 52.30 34.50 49.10 51.80 34.60 48.90 51.60 34.70 48.40 51.10 34.80 48.20 50.90 34.90 47.90 50.50 35.00 47.60 50.20 35.10 47.30 49.90 35.20 47.10 49.60 35.30 46.80 49.30 35.40 46.50 49.00 35.50 46.30 48.80 31.5 31.8 31.6 31.9 31.7 32 31.7 32 31.7 32.1 31.8 32.1 31.8 32.1 31.7 32.1 31.7 32.2 31.8 32.3 32 32.3 38.2 33.2 44.2 35.5 62.3 47.1 85.8 61.8 110 76.3 128.1 88.7 140.4 98.7 149 107.1 154.6 114 158.3 119.7 161 124.2 162.9 128.1 164.1 131.1 165.1 133.6 165.8 135.5 166.4 137 166.8 138.1 167.1 139.1 167.4 139.9 167.7 140.6 167.9 141.2 168 141.7 168.1 142.1 165.9 140 153.5 132.7 142.6 126.2 133.4 120.5 125.5 115.5 118.7 110.9 112.7 106.7 107.4 102.9 102.6 99.3 98.4 96.1 94.5 93.1 90.9 90.4 87.6 87.8 84.7 85.4 82 83.1 79.5 81 77.3 79 75.4 77 73.6 75.2 72 73.5 70.6 71.9 69.1 70.4 67.6 69 66.1 67.7 64.7 66.4 63.2 65.2 61.9 64 60.7 63 59.6 61.9 58.5 60.9 57.4 59.9 56.4 58.9 55.5 58 54.6 57.1 53.8 56.3 53.2 55.6 52.6 54.9 51.9 54.2 51.2 53.6 50.5 52.9 49.8 52.4 49.1 51.8 48.4 51.2 47.8 50.7 47.2 50 46.7 49.5 46.2 48.9 45.7 48.4 45.3 48 44.9 47.5 44.5 47.1 44.2 46.7 43.9 46.4 43.6 46.1 43.3 45.8 43.1 45.5 42.9 45.2 42.6 45 42.5 44.7 42.2 44.5 42 44.3 41.8 44 41.6 43.9 41.4 43.7 41.3 43.4 41.1 43.3 41 43 40.8 42.9 40.6 42.8 40.5 42.6 40.4 42.4 40.3 42.2 40.2 42.1 40 42 39.8 41.9 39.7 41.7 39.6 41.7 39.5 41.5 39.5 41.5 39.5 41.4 39.6 41.4 39.5 41.3 39.3 41.2 39.2 41.2 39.2 41.1 39.1 41 38.9 40.9 38.7 40.8 38.6 40.7 38.5 40.6 38.6 40.6 38.6 40.6 38.3 40.4 38.1 40.2 38 40.2 38.1 40.2 38 40.1 38.3 40.1 38.3 40.1 38.2 40 38.2 40.1 38.1 39.9 38.3 40 38.1 39.8 38.1 39.8 38.1 39.8 38.1 39.8 38 39.7 38 39.7 39.4 39.6 47.4 40.4 57.5 47.5 88.5 63.1 118.5 78.5 134.7 91.5 145.3 102.2 152.4 110.8 156.8 117.4 160 122.7 161.9 126.7 163.5 130.2 164.6 132.8 165.4 134.8 166.1 136.4 166.5 137.7 167 138.8 167.3 139.7 167.6 140.5 167.8 141.2 168 141.7 168.1 142.3 168.3 142.7 168.3 143 162.9 138.4 151.4 131.3 141.2 125.4 132.6 120.3 125.3 115.6 118.9 111.4 113.2 107.6 108.2 104 103.8 100.8 99.7 97.9 96.1 95.1 92.7 92.5 89.6 90 86.8 87.8 84.4 85.7 82.1 83.7 79.9 81.8 78 80 76.3 78.2 74.7 76.6 73.2 75.1 71.8 73.7 70.6 72.3 69.2 71 67.9 69.8 66.6 68.6 65.4 67.5 64.2 66.4 63.1 65.4 62 64.4 61 63.4 60.1 62.5 59.3 61.6 58.4 60.8 57.6 60 56.9 59.2 56.2 58.5 55.5 57.8 54.9 57.1 54.3 56.5 53.8 55.9 53.1 55.3 52.5 54.7 52 54.2 51.6 53.8 51.1 53.3 50.7 52.8 50.2 52.4 49.8 52 49.4 51.6 49 51.2 48.7 50.9 48.3 50.5 48.1 50.2 47.8 49.9 47.5 49.6 47.2 49.3 47 49.1 46.8 48.8 46.5 48.6 46.3 48.3 46.1 48.1 46 47.9 45.9 47.7 45.7 47.5 45.4 47.3 45.2 47.1 45.1 46.9 44.9 46.8 44.7 46.6 44.6 46.5 44.4 46.3 44.2 46.2 44.1 46 44 45.9 44 45.7 43.9 45.6 43.9 45.5 43.8 45.5 43.6 45.4 43.4 45.3 43.2 45.2 43 45.1 42.8 45 42.7 44.9 42.6 44.8 42.4 44.8 42.4 44.7 42.3 44.6 42.2 44.5 42.1 44.4 42.2 44.3 42.4 44.3 42.3 44.2 42.2 44.1 42.1 44.1 42.1 44 42.1 43.9 42 43.8 41.8 43.7 41.7 43.6 41.7 43.6 41.6 43.5 47 43.8 54.9 45 70.5 57.3 107 73.1 128.7 86.9 142 99.2 150.9 109.2 156.3 116.8 159.6 122.6 161.8 127.2 163.2 130.7 164.3 133.4 165.2 135.6 165.9 137.3 166.4 138.6 166.8 139.7 167.2 140.7 167.4 141.5 167.7 142.1 167.9 142.7 168 143.2 168.2 143.6 168.3 144 168.7 143.7 158.1 136.5 147 130.3 137.8 125 129.9 120.1 123.1 115.6 117.2 111.7 112 108 107.3 104.6 103.1 101.5 99.3 98.7 95.8 96 92.7 93.5 89.8 91.2 87.1 89 84.7 87 82.5 85.1 80.5 83.3 78.7 81.5 77.2 79.8 75.7 78.3 74.4 76.8 73.2 75.4 72 74.1 70.8 72.8 69.5 71.7 68.3 70.5 67 69.5 65.9 68.5 64.6 67.4 63.4 66.5 62.2 65.5 61.1 64.5 60 63.5 59 62.5 58.1 61.6 57.2 60.9 56.4 60 55.8 59.2 55.3 58.6 54.7 57.8 54.1 57.2 53.5 56.6 53 56 52.5 55.5 52 55 51.6 54.4 51.1 54 50.7 53.5 50.4 53.2 49.9 52.7 49.6 52.3 49.1 51.8 48.9 51.6 48.4 51.1 48.2 50.9 47.9 50.5 47.6 50.2 47.3 49.9 47.1 49.6 46.8 49.3 46.5 49 46.3 48.8 PP&PP at top side PP&Sealant at Al tab 0.00 31.50 30.80 0.10 31.50 30.90 0.20 31.30 31.00 0.30 31.20 31.00 0.40 31.40 31.10 0.50 31.90 31.30 0.60 35.80 31.60 0.70 40.60 32.60 0.80 51.80 47.60 0.90 81.00 69.40 1.00 101.30 84.50 1.10 113.40 95.50 1.20 121.90 103.80 1.30 129.50 110.00 1.40 134.90 114.70 1.50 139.10 118.70 1.60 141.70 122.10 1.70 144.10 125.00 1.80 145.80 127.50 1.90 147.30 129.40 2.00 148.40 131.10 2.10 149.20 132.40 2.20 150.20 133.60 2.30 150.80 134.60 2.40 151.40 135.40 2.50 151.80 136.10 2.60 152.20 136.70 2.70 152.70 137.20 2.80 153.00 137.70 2.90 153.20 138.10 3.00 153.50 138.40 3.10 153.70 138.70 3.20 153.80 139.00 3.30 153.80 139.20 3.40 154.00 139.40 3.50 154.10 139.70 3.60 154.30 139.90 3.70 154.40 140.00 3.80 154.50 140.20 3.90 175.10 137.80 4.00 145.60 131.00 4.10 134.90 125.20 4.20 126.50 120.00 4.30 119.30 115.20 4.40 113.10 110.90 4.50 107.90 107.00 4.60 103.60 103.30 4.70 104.50 100.00 4.80 100.30 96.90 4.90 92.30 94.00 5.00 99.80 91.20 5.10 76.90 81.60 5.20 74.80 79.40 5.30 72.90 77.40 5.40 71.10 75.60 5.50 69.50 73.80 5.60 68.00 72.20 5.70 66.50 70.60 5.80 65.00 69.10 5.90 63.60 67.70 6.00 62.40 66.40 6.10 61.10 65.20 6.20 59.90 64.00 6.30 58.80 62.80 6.40 57.70 61.80 6.50 56.70 60.80 6.60 55.80 59.80 6.70 55.00 58.80 6.80 54.20 57.90 6.90 53.40 57.10 7.00 52.60 56.30 7.10 51.90 55.50 7.20 51.30 54.80 7.30 50.70 54.10 7.40 50.10 53.50 7.50 49.50 52.80 7.60 49.00 52.30 7.70 48.40 51.70 7.80 48.00 51.20 7.90 47.50 50.60 8.00 47.20 50.20 8.10 46.70 49.70 8.20 46.40 49.30 8.30 46.00 48.80 8.40 45.60 48.40 8.50 45.30 48.00 8.60 45.00 47.70 8.70 44.60 47.40 8.80 44.30 47.00 8.90 44.10 46.70 9.00 43.90 46.40 9.10 43.60 46.10 9.20 43.40 45.90 9.30 43.20 45.60 9.40 42.90 45.30 9.50 42.70 45.10 9.60 42.60 44.90 9.70 42.40 44.70 9.80 42.10 44.40 9.90 41.90 44.20 10.00 41.70 44.10 10.10 41.60 43.80 10.20 41.40 43.60 10.30 41.20 43.50 10.40 41.00 43.30 10.50 40.80 43.10 10.60 40.70 43.00 10.70 40.50 42.80 10.80 40.40 42.70 10.90 40.30 42.50 11.00 40.20 42.40 11.10 40.20 42.20 11.20 40.20 42.10 11.30 40.00 42.10 11.40 39.80 42.00 11.50 39.70 41.90 11.60 39.60 41.80 11.70 39.60 41.80 11.80 39.60 41.70 11.90 39.50 41.60 12.00 39.50 41.50 12.10 39.30 41.30 12.20 39.30 41.20 12.30 39.30 41.30 12.40 39.30 41.20 12.50 44.00 41.50 12.60 53.90 47.50 12.70 84.70 68.00 12.80 106.00 82.80 12.90 120.10 94.60 13.00 127.80 104.00 13.10 133.80 111.70 13.20 139.00 118.10 13.30 142.90 123.10 13.40 145.90 126.90 13.50 147.90 129.90 13.60 149.40 132.30 13.70 150.70 134.30 13.80 151.70 135.90 13.90 152.50 137.20 14.00 153.30 138.20 14.10 153.80 139.10 14.20 154.30 139.90 14.30 154.70 140.50 14.40 155.10 140.90 14.50 155.30 141.40 14.60 155.50 141.80 14.70 155.70 142.00 14.80 156.00 142.30 14.90 156.00 142.50 15.00 156.20 142.70 15.10 156.40 142.90 15.20 156.40 143.10 15.30 156.60 143.20 15.40 156.70 143.30 15.50 156.70 143.50 15.60 156.80 143.60 15.70 157.30 143.70 15.80 83.90 87.50 15.90 82.30 85.30 16.00 78.60 83.20 16.10 76.30 81.30 16.20 74.40 79.40 16.30 72.80 77.70 16.40 71.30 76.00 16.50 69.80 74.50 16.60 68.40 73.00 16.70 67.00 71.70 16.80 65.80 70.30 16.90 64.50 69.10 17.00 63.40 68.00 17.10 62.20 66.80 17.20 61.20 65.80 17.30 60.30 64.80 17.40 59.30 63.80 17.50 58.40 62.90 17.60 57.60 62.10 17.70 56.80 61.20 17.80 56.10 60.40 17.90 55.50 59.60 18.00 54.80 58.90 18.10 54.30 58.20 18.20 53.80 57.60 18.30 53.30 57.10 18.40 52.70 56.50 18.50 52.20 56.00 18.60 51.70 55.40 18.70 51.30 54.90 18.80 50.90 54.40 18.90 50.50 54.00 19.00 50.20 53.50 19.10 49.70 53.10 19.20 49.40 52.70 19.30 49.00 52.40 19.40 48.70 52.00 19.50 48.50 51.70 19.60 48.30 51.30 19.70 48.00 51.00 19.80 47.70 50.70 19.90 47.40 50.40 20.00 47.20 50.10 20.10 46.90 49.80 20.20 46.60 49.60 20.30 46.50 49.30 20.40 46.20 49.10 20.50 46.00 48.80 20.60 45.80 48.60 20.70 45.60 48.40 20.80 49.60 48.40 20.90 55.60 50.50 21.00 97.30 71.20 21.10 113.20 87.30 21.20 125.20 99.30 21.30 133.60 108.80 21.40 139.30 116.20 21.50 143.40 121.90 21.60 146.30 126.20 21.70 148.40 129.70 21.80 150.10 132.40 21.90 151.50 134.60 22.00 152.60 136.40 22.10 153.40 137.80 22.20 154.10 139.00 22.30 154.70 139.90 22.40 155.20 140.70 22.50 155.60 141.30 22.60 156.00 141.80 22.70 156.30 142.30 22.80 156.50 142.60 22.90 156.80 142.90 23.00 157.00 143.20 23.10 157.20 143.50 23.20 157.40 143.70 23.30 157.50 143.90 23.40 157.60 144.00 23.50 157.70 144.10 23.60 157.80 144.30 23.70 157.90 144.40 23.80 158.00 144.50 23.90 158.00 144.60 24.00 158.00 144.70 24.10 111.30 144.70 24.20 136.50 131.70 24.30 128.80 126.40 24.40 122.30 121.50 24.50 116.70 117.10 24.60 111.60 113.10 24.70 107.10 109.40 24.80 103.00 106.00 24.90 99.40 102.70 25.00 96.00 99.90 25.10 93.00 97.10 25.20 90.20 94.70 25.30 87.60 92.30 25.40 85.20 90.00 25.50 83.10 88.00 25.60 81.10 85.90 25.70 79.20 84.10 25.80 77.50 82.30 25.90 75.90 80.50 26.00 74.40 78.90 26.10 73.00 77.40 26.20 71.70 75.90 26.30 70.50 74.60 26.40 69.20 73.30 26.50 68.00 72.10 26.60 66.80 71.00 26.70 65.80 70.00 26.80 64.60 68.90 26.90 63.50 67.90 27.00 62.40 66.80 27.10 61.40 65.90 27.20 60.40 64.90 27.30 59.50 63.90 27.40 58.70 63.00 27.50 57.90 62.10 27.60 57.10 61.20 27.70 56.40 60.40 27.80 55.70 59.70 27.90 54.90 58.70 28.00 54.20 57.90 28.10 53.70 57.30 28.20 53.30 56.70 28.30 52.80 56.10 28.40 52.40 55.60 28.50 52.00 55.10 28.60 51.50 54.60 28.70 51.20 54.10 28.80 50.80 53.60 28.90 50.40 53.20 29.00 50.00 52.80 29.10 49.80 52.50 29.20 49.50 52.20 29.30 49.20 51.80 29.40 48.70 51.40 29.50 48.50 51.10 29.60 48.20 50.80 29.70 47.90 50.50 29.80 47.70 50.20 29.90 47.50 49.90 30.00 47.20 49.60 30.10 47.00 49.40 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 PP&PP at top side PP&Sealant at Al tab _1209303674.xls 图表1 31.5 31.8 31.6 31.9 31.7 32 31.7 32 31.7 32.1 31.8 32.1 31.8 32.1 31.7 32.1 31.7 32.2 31.8 32.3 32 32.3 38.2 33.2 44.2 35.5 62.3 47.1 85.8 61.8 110 76.3 128.1 88.7 140.4 98.7 149 107.1 154.6 114 158.3 119.7 161 124.2 162.9 128.1 164.1 131.1 165.1 133.6 165.8 135.5 166.4 137 166.8 138.1 167.1 139.1 167.4 139.9 167.7 140.6 167.9 141.2 168 141.7 168.1 142.1 165.9 140 153.5 132.7 142.6 126.2 133.4 120.5 125.5 115.5 118.7 110.9 112.7 106.7 107.4 102.9 102.6 99.3 98.4 96.1 94.5 93.1 90.9 90.4 87.6 87.8 84.7 85.4 82 83.1 79.5 81 77.3 79 75.4 77 73.6 75.2 72 73.5 70.6 71.9 69.1 70.4 67.6 69 66.1 67.7 64.7 66.4 63.2 65.2 61.9 64 60.7 63 59.6 61.9 58.5 60.9 57.4 59.9 56.4 58.9 55.5 58 54.6 57.1 53.8 56.3 53.2 55.6 52.6 54.9 51.9 54.2 51.2 53.6 50.5 52.9 49.8 52.4 49.1 51.8 48.4 51.2 47.8 50.7 47.2 50 46.7 49.5 46.2 48.9 45.7 48.4 45.3 48 44.9 47.5 44.5 47.1 44.2 46.7 43.9 46.4 43.6 46.1 43.3 45.8 43.1 45.5 42.9 45.2 42.6 45 42.5 44.7 42.2 44.5 42 44.3 41.8 44 41.6 43.9 41.4 43.7 41.3 43.4 41.1 43.3 41 43 40.8 42.9 40.6 42.8 40.5 42.6 40.4 42.4 40.3 42.2 40.2 42.1 40 42 39.8 41.9 39.7 41.7 39.6 41.7 39.5 41.5 39.5 41.5 39.5 41.4 39.6 41.4 39.5 41.3 39.3 41.2 39.2 41.2 39.2 41.1 39.1 41 38.9 40.9 38.7 40.8 38.6 40.7 38.5 40.6 38.6 40.6 38.6 40.6 38.3 40.4 38.1 40.2 38 40.2 38.1 40.2 38 40.1 38.3 40.1 38.3 40.1 38.2 40 38.2 40.1 38.1 39.9 38.3 40 38.1 39.8 38.1 39.8 38.1 39.8 38.1 39.8 38 39.7 38 39.7 39.4 39.6 47.4 40.4 57.5 47.5 88.5 63.1 118.5 78.5 134.7 91.5 145.3 102.2 152.4 110.8 156.8 117.4 160 122.7 161.9 126.7 163.5 130.2 164.6 132.8 165.4 134.8 166.1 136.4 166.5 137.7 167 138.8 167.3 139.7 167.6 140.5 167.8 141.2 168 141.7 168.1 142.3 168.3 142.7 168.3 143 162.9 138.4 151.4 131.3 141.2 125.4 132.6 120.3 125.3 115.6 118.9 111.4 113.2 107.6 108.2 104 103.8 100.8 99.7 97.9 96.1 95.1 92.7 92.5 89.6 90 86.8 87.8 84.4 85.7 82.1 83.7 79.9 81.8 78 80 76.3 78.2 74.7 76.6 73.2 75.1 71.8 73.7 70.6 72.3 69.2 71 67.9 69.8 66.6 68.6 65.4 67.5 64.2 66.4 63.1 65.4 62 64.4 61 63.4 60.1 62.5 59.3 61.6 58.4 60.8 57.6 60 56.9 59.2 56.2 58.5 55.5 57.8 54.9 57.1 54.3 56.5 53.8 55.9 53.1 55.3 52.5 54.7 52 54.2 51.6 53.8 51.1 53.3 50.7 52.8 50.2 52.4 49.8 52 49.4 51.6 49 51.2 48.7 50.9 48.3 50.5 48.1 50.2 47.8 49.9 47.5 49.6 47.2 49.3 47 49.1 46.8 48.8 46.5 48.6 46.3 48.3 46.1 48.1 46 47.9 45.9 47.7 45.7 47.5 45.4 47.3 45.2 47.1 45.1 46.9 44.9 46.8 44.7 46.6 44.6 46.5 44.4 46.3 44.2 46.2 44.1 46 44 45.9 44 45.7 43.9 45.6 43.9 45.5 43.8 45.5 43.6 45.4 43.4 45.3 43.2 45.2 43 45.1 42.8 45 42.7 44.9 42.6 44.8 42.4 44.8 42.4 44.7 42.3 44.6 42.2 44.5 42.1 44.4 42.2 44.3 42.4 44.3 42.3 44.2 42.2 44.1 42.1 44.1 42.1 44 42.1 43.9 42 43.8 41.8 43.7 41.7 43.6 41.7 43.6 41.6 43.5 47 43.8 54.9 45 70.5 57.3 107 73.1 128.7 86.9 142 99.2 150.9 109.2 156.3 116.8 159.6 122.6 161.8 127.2 163.2 130.7 164.3 133.4 165.2 135.6 165.9 137.3 166.4 138.6 166.8 139.7 167.2 140.7 167.4 141.5 167.7 142.1 167.9 142.7 168 143.2 168.2 143.6 168.3 144 168.7 143.7 158.1 136.5 147 130.3 137.8 125 129.9 120.1 123.1 115.6 117.2 111.7 112 108 107.3 104.6 103.1 101.5 99.3 98.7 95.8 96 92.7 93.5 89.8 91.2 87.1 89 84.7 87 82.5 85.1 80.5 83.3 78.7 81.5 77.2 79.8 75.7 78.3 74.4 76.8 73.2 75.4 72 74.1 70.8 72.8 69.5 71.7 68.3 70.5 67 69.5 65.9 68.5 64.6 67.4 63.4 66.5 62.2 65.5 61.1 64.5 60 63.5 59 62.5 58.1 61.6 57.2 60.9 56.4 60 55.8 59.2 55.3 58.6 54.7 57.8 54.1 57.2 53.5 56.6 53 56 52.5 55.5 52 55 51.6 54.4 51.1 54 50.7 53.5 50.4 53.2 49.9 52.7 49.6 52.3 49.1 51.8 48.9 51.6 48.4 51.1 48.2 50.9 47.9 50.5 47.6 50.2 47.3 49.9 47.1 49.6 46.8 49.3 46.5 49 46.3 48.8 PP&PP at top side PP&Sealant at Al tab Time/s Temp/ºC Temp rise curve Sum Top sealing temp trend for 604396 at SSL factory Top sealing time interval 2s Top sealing time interval 3s Conclusion: For PP&Sealant,the temperature reach 140ºC from RT need 1.5s,the highest is 145ºC. For PP&PP,need0.8~1.0s,the temperature over160ºC and the hightest is 168ºC. Top sealing time interval 3s Sum 31.5 30.8 31.5 30.9 31.3 31 31.2 31 31.4 31.1 31.9 31.3 35.8 31.6 40.6 32.6 51.8 47.6 81 69.4 101.3 84.5 113.4 95.5 121.9 103.8 129.5 110 134.9 114.7 139.1 118.7 141.7 122.1 144.1 125 145.8 127.5 147.3 129.4 148.4 131.1 149.2 132.4 150.2 133.6 150.8 134.6 151.4 135.4 151.8 136.1 152.2 136.7 152.7 137.2 153 137.7 153.2 138.1 153.5 138.4 153.7 138.7 153.8 139 153.8 139.2 154 139.4 154.1 139.7 154.3 139.9 154.4 140 154.5 140.2 175.1 137.8 145.6 131 134.9 125.2 126.5 120 119.3 115.2 113.1 110.9 107.9 107 103.6 103.3 104.5 100 100.3 96.9 92.3 94 99.8 91.2 76.9 81.6 74.8 79.4 72.9 77.4 71.1 75.6 69.5 73.8 68 72.2 66.5 70.6 65 69.1 63.6 67.7 62.4 66.4 61.1 65.2 59.9 64 58.8 62.8 57.7 61.8 56.7 60.8 55.8 59.8 55 58.8 54.2 57.9 53.4 57.1 52.6 56.3 51.9 55.5 51.3 54.8 50.7 54.1 50.1 53.5 49.5 52.8 49 52.3 48.4 51.7 48 51.2 47.5 50.6 47.2 50.2 46.7 49.7 46.4 49.3 46 48.8 45.6 48.4 45.3 48 45 47.7 44.6 47.4 44.3 47 44.1 46.7 43.9 46.4 43.6 46.1 43.4 45.9 43.2 45.6 42.9 45.3 42.7 45.1 42.6 44.9 42.4 44.7 42.1 44.4 41.9 44.2 41.7 44.1 41.6 43.8 41.4 43.6 41.2 43.5 41 43.3 40.8 43.1 40.7 43 40.5 42.8 40.4 42.7 40.3 42.5 40.2 42.4 40.2 42.2 40.2 42.1 40 42.1 39.8 42 39.7 41.9 39.6 41.8 39.6 41.8 39.6 41.7 39.5 41.6 39.5 41.5 39.3 41.3 39.3 41.2 39.3 41.3 39.3 41.2 44 41.5 53.9 47.5 84.7 68 106 82.8 120.1 94.6 127.8 104 133.8 111.7 139 118.1 142.9 123.1 145.9 126.9 147.9 129.9 149.4 132.3 150.7 134.3 151.7 135.9 152.5 137.2 153.3 138.2 153.8 139.1 154.3 139.9 154.7 140.5 155.1 140.9 155.3 141.4 155.5 141.8 155.7 142 156 142.3 156 142.5 156.2 142.7 156.4 142.9 156.4 143.1 156.6 143.2 156.7 143.3 156.7 143.5 156.8 143.6 157.3 143.7 83.9 87.5 82.3 85.3 78.6 83.2 76.3 81.3 74.4 79.4 72.8 77.7 71.3 76 69.8 74.5 68.4 73 67 71.7 65.8 70.3 64.5 69.1 63.4 68 62.2 66.8 61.2 65.8 60.3 64.8 59.3 63.8 58.4 62.9 57.6 62.1 56.8 61.2 56.1 60.4 55.5 59.6 54.8 58.9 54.3 58.2 53.8 57.6 53.3 57.1 52.7 56.5 52.2 56 51.7 55.4 51.3 54.9 50.9 54.4 50.5 54 50.2 53.5 49.7 53.1 49.4 52.7 49 52.4 48.7 52 48.5 51.7 48.3 51.3 48 51 47.7 50.7 47.4 50.4 47.2 50.1 46.9 49.8 46.6 49.6 46.5 49.3 46.2 49.1 46 48.8 45.8 48.6 45.6 48.4 49.6 48.4 55.6 50.5 97.3 71.2 113.2 87.3 125.2 99.3 133.6 108.8 139.3 116.2 143.4 121.9 146.3 126.2 148.4 129.7 150.1 132.4 151.5 134.6 152.6 136.4 153.4 137.8 154.1 139 154.7 139.9 155.2 140.7 155.6 141.3 156 141.8 156.3 142.3 156.5 142.6 156.8 142.9 157 143.2 157.2 143.5 157.4 143.7 157.5 143.9 157.6 144 157.7 144.1 157.8 144.3 157.9 144.4 158 144.5 158 144.6 158 144.7 111.3 144.7 136.5 131.7 128.8 126.4 122.3 121.5 116.7 117.1 111.6 113.1 107.1 109.4 103 106 99.4 102.7 96 99.9 93 97.1 90.2 94.7 87.6 92.3 85.2 90 83.1 88 81.1 85.9 79.2 84.1 77.5 82.3 75.9 80.5 74.4 78.9 73 77.4 71.7 75.9 70.5 74.6 69.2 73.3 68 72.1 66.8 71 65.8 70 64.6 68.9 63.5 67.9 62.4 66.8 61.4 65.9 60.4 64.9 59.5 63.9 58.7 63 57.9 62.1 57.1 61.2 56.4 60.4 55.7 59.7 54.9 58.7 54.2 57.9 53.7 57.3 53.3 56.7 52.8 56.1 52.4 55.6 52 55.1 51.5 54.6 51.2 54.1 50.8 53.6 50.4 53.2 50 52.8 49.8 52.5 49.5 52.2 49.2 51.8 48.7 51.4 48.5 51.1 48.2 50.8 47.9 50.5 47.7 50.2 47.5 49.9 47.2 49.6 47 49.4 PP&PP at top side PP&Sealant at Al tab Time/s Temp/ºC Temp rise curve 34 31.5 31.8 31.6 31.9 31.7 32 31.7 32 31.7 32.1 31.8 32.1 31.8 32.1 31.7 32.1 31.7 32.2 31.8 32.3 32 32.3 38.2 33.2 44.2 35.5 62.3 47.1 85.8 61.8 110 76.3 128.1 88.7 140.4 98.7 149 107.1 154.6 114 158.3 119.7 161 124.2 162.9 128.1 164.1 131.1 165.1 133.6 165.8 135.5 166.4 137 166.8 138.1 167.1 139.1 167.4 139.9 167.7 140.6 167.9 141.2 168 141.7 168.1 142.1 165.9 140 153.5 132.7 142.6 126.2 133.4 120.5 125.5 115.5 118.7 110.9 112.7 106.7 107.4 102.9 102.6 99.3 98.4 96.1 94.5 93.1 90.9 90.4 87.6 87.8 84.7 85.4 82 83.1 79.5 81 77.3 79 75.4 77 73.6 75.2 72 73.5 70.6 71.9 69.1 70.4 67.6 69 66.1 67.7 64.7 66.4 63.2 65.2 61.9 64 60.7 63 59.6 61.9 58.5 60.9 57.4 59.9 56.4 58.9 55.5 58 54.6 57.1 53.8 56.3 53.2 55.6 52.6 54.9 51.9 54.2 51.2 53.6 50.5 52.9 49.8 52.4 49.1 51.8 48.4 51.2 47.8 50.7 47.2 50 46.7 49.5 46.2 48.9 45.7 48.4 45.3 48 44.9 47.5 44.5 47.1 44.2 46.7 43.9 46.4 43.6 46.1 43.3 45.8 43.1 45.5 42.9 45.2 42.6 45 42.5 44.7 42.2 44.5 42 44.3 41.8 44 41.6 43.9 41.4 43.7 41.3 43.4 41.1 43.3 41 43 40.8 42.9 40.6 42.8 40.5 42.6 40.4 42.4 40.3 42.2 40.2 42.1 40 42 39.8 41.9 39.7 41.7 39.6 41.7 39.5 41.5 39.5 41.5 39.5 41.4 39.6 41.4 39.5 41.3 39.3 41.2 39.2 41.2 39.2 41.1 39.1 41 38.9 40.9 38.7 40.8 38.6 40.7 38.5 40.6 38.6 40.6 38.6 40.6 38.3 40.4 38.1 40.2 38 40.2 38.1 40.2 38 40.1 38.3 40.1 38.3 40.1 38.2 40 38.2 40.1 38.1 39.9 38.3 40 38.1 39.8 38.1 39.8 38.1 39.8 38.1 39.8 38 39.7 38 39.7 39.4 39.6 47.4 40.4 57.5 47.5 88.5 63.1 118.5 78.5 134.7 91.5 145.3 102.2 152.4 110.8 156.8 117.4 160 122.7 161.9 126.7 163.5 130.2 164.6 132.8 165.4 134.8 166.1 136.4 166.5 137.7 167 138.8 167.3 139.7 167.6 140.5 167.8 141.2 168 141.7 168.1 142.3 168.3 142.7 168.3 143 162.9 138.4 151.4 131.3 141.2 125.4 132.6 120.3 125.3 115.6 118.9 111.4 113.2 107.6 108.2 104 103.8 100.8 99.7 97.9 96.1 95.1 92.7 92.5 89.6 90 86.8 87.8 84.4 85.7 82.1 83.7 79.9 81.8 78 80 76.3 78.2 74.7 76.6 73.2 75.1 71.8 73.7 70.6 72.3 69.2 71 67.9 69.8 66.6 68.6 65.4 67.5 64.2 66.4 63.1 65.4 62 64.4 61 63.4 60.1 62.5 59.3 61.6 58.4 60.8 57.6 60 56.9 59.2 56.2 58.5 55.5 57.8 54.9 57.1 54.3 56.5 53.8 55.9 53.1 55.3 52.5 54.7 52 54.2 51.6 53.8 51.1 53.3 50.7 52.8 50.2 52.4 49.8 52 49.4 51.6 49 51.2 48.7 50.9 48.3 50.5 48.1 50.2 47.8 49.9 47.5 49.6 47.2 49.3 47 49.1 46.8 48.8 46.5 48.6 46.3 48.3 46.1 48.1 46 47.9 45.9 47.7 45.7 47.5 45.4 47.3 45.2 47.1 45.1 46.9 44.9 46.8 44.7 46.6 44.6 46.5 44.4 46.3 44.2 46.2 44.1 46 44 45.9 44 45.7 43.9 45.6 43.9 45.5 43.8 45.5 43.6 45.4 43.4 45.3 43.2 45.2 43 45.1 42.8 45 42.7 44.9 42.6 44.8 42.4 44.8 42.4 44.7 42.3 44.6 42.2 44.5 42.1 44.4 42.2 44.3 42.4 44.3 42.3 44.2 42.2 44.1 42.1 44.1 42.1 44 42.1 43.9 42 43.8 41.8 43.7 41.7 43.6 41.7 43.6 41.6 43.5 47 43.8 54.9 45 70.5 57.3 107 73.1 128.7 86.9 142 99.2 150.9 109.2 156.3 116.8 159.6 122.6 161.8 127.2 163.2 130.7 164.3 133.4 165.2 135.6 165.9 137.3 166.4 138.6 166.8 139.7 167.2 140.7 167.4 141.5 167.7 142.1 167.9 142.7 168 143.2 168.2 143.6 168.3 144 168.7 143.7 158.1 136.5 147 130.3 137.8 125 129.9 120.1 123.1 115.6 117.2 111.7 112 108 107.3 104.6 103.1 101.5 99.3 98.7 95.8 96 92.7 93.5 89.8 91.2 87.1 89 84.7 87 82.5 85.1 80.5 83.3 78.7 81.5 77.2 79.8 75.7 78.3 74.4 76.8 73.2 75.4 72 74.1 70.8 72.8 69.5 71.7 68.3 70.5 67 69.5 65.9 68.5 64.6 67.4 63.4 66.5 62.2 65.5 61.1 64.5 60 63.5 59 62.5 58.1 61.6 57.2 60.9 56.4 60 55.8 59.2 55.3 58.6 54.7 57.8 54.1 57.2 53.5 56.6 53 56 52.5 55.5 52 55 51.6 54.4 51.1 54 50.7 53.5 50.4 53.2 49.9 52.7 49.6 52.3 49.1 51.8 48.9 51.6 48.4 51.1 48.2 50.9 47.9 50.5 47.6 50.2 47.3 49.9 47.1 49.6 46.8 49.3 46.5 49 46.3 48.8 PP&PP at top side PP&Sealant at Al tab Time/s Temp/ºC Temp rise curve 35 43.9 31.1 43.5 31.1 43.6 31.1 43.2 31.1 43 31.2 43 31.2 42.7 31.3 42.2 31.3 41.8 31.4 40.9 31.4 40.1 31.4 39.7 31.5 39 31.5 38.2 31.5 37.9 31.5 37.6 31.5 37.3 31.5 37.1 31.6 37.2 31.6 37.8 31.6 37.8 31.6 38.7 31.7 40.2 35.4 63.3 52.3 87.7 71.3 104.6 84.7 116 94.5 125.1 102.7 135 111.1 142 118.8 146.3 124.5 149.6 128.5 152.5 131.4 155.2 133.7 157.6 135.4 159.5 136.8 161 138 162.3 138.9 163.2 139.6 163.9 140.2 164.5 140.8 165 141.2 165.4 141.6 165.7 141.9 165.9 142.2 166 142.5 166.2 142.7 166.3 142.9 166.4 143.1 166.5 143.3 166.7 143.4 166.7 143.6 166.8 143.8 166.8 143.9 164.7 141.4 155 134 144.7 128.1 135.7 122.9 128 118.2 121.2 113.9 115.3 109.9 110 106.2 105.3 102.8 101 99.7 97 96.7 93.5 94 90.2 91.4 87.2 88.9 84.5 86.6 81.9 84.5 79.5 82.4 77.6 80.5 75.8 78.6 74.2 76.9 72.7 75.2 71.3 73.7 70 72.3 68.5 70.9 67 69.7 65.4 68.5 64 67.3 62.8 66.2 61.6 65.2 60.5 64.1 59.4 63.2 58.5 62.2 57.6 61.3 56.7 60.4 55.9 59.6 55 58.7 54.3 57.9 53.6 57.2 52.9 56.4 52.3 55.8 51.6 55.2 51.1 54.5 50.4 53.9 51 53.5 57.5 53.5 67.4 58.9 90.5 71.5 116 84.4 131.1 96.1 142.5 106.6 150.7 114.9 156 121.7 159.2 127 161.4 130.9 162.8 133.7 163.8 135.8 164.6 137.5 165.2 138.8 165.7 139.8 166.1 140.7 166.4 141.4 166.6 142 166.8 142.4 167 142.8 167.2 143.2 167.3 143.5 167.4 143.8 167.5 144 167.6 144.3 167.6 144.4 167.7 144.6 167.8 144.7 167.8 144.8 167.8 145 167.9 145.1 167.9 145.2 167.7 145.2 163.4 141 152.3 134.4 142.9 129 134.7 124.2 127.7 119.8 121.6 115.7 116.1 112 111.2 108.5 106.9 105.2 102.9 102.3 99.3 99.5 96.1 97 93.1 94.5 90.3 92.2 87.7 90 85.3 88 83.1 86.1 81.1 84.4 79.4 82.7 77.8 81.1 76.4 79.6 75.1 78.1 73.9 76.7 72.8 75.4 71.6 74.2 70.4 73 69.1 71.9 67.9 70.9 66.7 69.9 65.5 68.9 64.5 68 63.6 67.1 62.7 66.3 61.8 65.4 60.9 64.7 60 63.9 59.2 63.1 58.5 62.4 57.8 61.7 57.2 61 56.5 60.3 55.8 59.7 55.2 59 54.8 58.5 54.3 58 53.9 57.5 53.5 57 53 56.5 52.5 56 52.2 55.5 51.9 55.1 51.5 54.7 51.1 54.3 50.7 54 50.4 53.6 51.8 53.3 58.8 53.8 68.6 59.3 88 71 109.9 83.1 125 92.8 138.4 102.5 148.8 111.6 155.3 118.7 159.1 124.3 161.4 128.6 162.9 132 163.9 134.4 164.8 136.4 165.3 137.9 165.8 139.1 166.2 140.1 166.5 140.9 166.8 141.6 167 142.2 167.2 142.7 167.3 143 167.4 143.4 167.6 143.8 167.6 144.1 167.7 144.3 167.8 144.6 167.9 144.7 167.9 145 168 145.1 168 145.3 168 145.4 168.1 145.5 167.9 145.4 162.8 140.8 150.7 134.6 141.7 129.2 133.9 124.5 127.2 120.1 121.3 116.2 116.1 112.5 111.4 109.1 107.2 106.1 103.4 103.2 100 100.6 96.8 98 93.9 95.7 91.2 93.5 88.6 91.4 86.4 89.4 84.3 87.5 82.5 85.8 80.7 84.2 79.2 82.7 77.8 81.3 76.5 79.9 75.4 78.5 74.3 77.3 73.2 76.1 72 75 70.9 73.9 69.8 72.9 68.6 71.9 67.6 70.9 66.6 70 65.7 69.2 64.8 68.3 64 67.5 63.2 66.7 62.4 66 61.6 65.3 60.8 64.5 60 63.8 59.2 63 58.4 62.3 57.8 61.6 57.3 60.9 56.7 60.2 56.3 59.7 55.8 59.1 55.1 58.4 54.6 57.9 54.1 57.3 53.7 56.8 53.3 56.2 52.9 55.7 52.5 55.3 52.1 54.8 51.7 54.4 51.3 54 PP&PP at top side PP&Sealant at AL tab Time/s Temp/ºC Temp rise curve AUTO0032 0.00 43.90 31.10 0.10 43.50 31.10 0.20 43.60 31.10 0.30 43.20 31.10 0.40 43.00 31.20 0.50 43.00 31.20 0.60 42.70 31.30 0.70 42.20 31.30 0.80 41.80 31.40 0.90 40.90 31.40 1.00 40.10 31.40 1.10 39.70 31.50 1.20 39.00 31.50 1.30 38.20 31.50 1.40 37.90 31.50 1.50 37.60 31.50 1.60 37.30 31.50 1.70 37.10 31.60 1.80 37.20 31.60 1.90 37.80 31.60 2.00 37.80 31.60 2.10 38.70 31.70 2.20 40.20 35.40 2.30 63.30 52.30 2.40 87.70 71.30 2.50 104.60 84.70 2.60 116.00 94.50 2.70 125.10 102.70 2.80 135.00 111.10 2.90 142.00 118.80 3.00 146.30 124.50 3.10 149.60 128.50 3.20 152.50 131.40 3.30 155.20 133.70 3.40 157.60 135.40 3.50 159.50 136.80 3.60 161.00 138.00 3.70 162.30 138.90 3.80 163.20 139.60 3.90 163.90 140.20 4.00 164.50 140.80 4.10 165.00 141.20 4.20 165.40 141.60 4.30 165.70 141.90 4.40 165.90 142.20 4.50 166.00 142.50 4.60 166.20 142.70 4.70 166.30 142.90 4.80 166.40 143.10 4.90 166.50 143.30 5.00 166.70 143.40 5.10 166.70 143.60 5.20 166.80 143.80 5.30 166.80 143.90 5.40 164.70 141.40 5.50 155.00 134.00 5.60 144.70 128.10 5.70 135.70 122.90 5.80 128.00 118.20 5.90 121.20 113.90 6.00 115.30 109.90 6.10 110.00 106.20 6.20 105.30 102.80 6.30 101.00 99.70 6.40 97.00 96.70 6.50 93.50 94.00 6.60 90.20 91.40 6.70 87.20 88.90 6.80 84.50 86.60 6.90 81.90 84.50 7.00 79.50 82.40 7.10 77.60 80.50 7.20 75.80 78.60 7.30 74.20 76.90 7.40 72.70 75.20 7.50 71.30 73.70 7.60 70.00 72.30 7.70 68.50 70.90 7.80 67.00 69.70 7.90 65.40 68.50 8.00 64.00 67.30 8.10 62.80 66.20 8.20 61.60 65.20 8.30 60.50 64.10 8.40 59.40 63.20 8.50 58.50 62.20 8.60 57.60 61.30 8.70 56.70 60.40 8.80 55.90 59.60 8.90 55.00 58.70 9.00 54.30 57.90 9.10 53.60 57.20 9.20 52.90 56.40 9.30 52.30 55.80 9.40 51.60 55.20 9.50 51.10 54.50 9.60 50.40 53.90 9.70 51.00 53.50 9.80 57.50 53.50 9.90 67.40 58.90 10.00 90.50 71.50 10.10 116.00 84.40 10.20 131.10 96.10 10.30 142.50 106.60 10.40 150.70 114.90 10.50 156.00 121.70 10.60 159.20 127.00 10.70 161.40 130.90 10.80 162.80 133.70 10.90 163.80 135.80 11.00 164.60 137.50 11.10 165.20 138.80 11.20 165.70 139.80 11.30 166.10 140.70 11.40 166.40 141.40 11.50 166.60 142.00 11.60 166.80 142.40 11.70 167.00 142.80 11.80 167.20 143.20 11.90 167.30 143.50 12.00 167.40 143.80 12.10 167.50 144.00 12.20 167.60 144.30 12.30 167.60 144.40 12.40 167.70 144.60 12.50 167.80 144.70 12.60 167.80 144.80 12.70 167.80 145.00 12.80 167.90 145.10 12.90 167.90 145.20 13.00 167.70 145.20 13.10 163.40 141.00 13.20 152.30 134.40 13.30 142.90 129.00 13.40 134.70 124.20 13.50 127.70 119.80 13.60 121.60 115.70 13.70 116.10 112.00 13.80 111.20 108.50 13.90 106.90 105.20 14.00 102.90 102.30 14.10 99.30 99.50 14.20 96.10 97.00 14.30 93.10 94.50 14.40 90.30 92.20 14.50 87.70 90.00 14.60 85.30 88.00 14.70 83.10 86.10 14.80 81.10 84.40 14.90 79.40 82.70 15.00 77.80 81.10 15.10 76.40 79.60 15.20 75.10 78.10 15.30 73.90 76.70 15.40 72.80 75.40 15.50 71.60 74.20 15.60 70.40 73.00 15.70 69.10 71.90 15.80 67.90 70.90 15.90 66.70 69.90 16.00 65.50 68.90 16.10 64.50 68.00 16.20 63.60 67.10 16.30 62.70 66.30 16.40 61.80 65.40 16.50 60.90 64.70 16.60 60.00 63.90 16.70 59.20 63.10 16.80 58.50 62.40 16.90 57.80 61.70 17.00 57.20 61.00 17.10 56.50 60.30 17.20 55.80 59.70 17.30 55.20 59.00 17.40 54.80 58.50 17.50 54.30 58.00 17.60 53.90 57.50 17.70 53.50 57.00 17.80 53.00 56.50 17.90 52.50 56.00 18.00 52.20 55.50 18.10 51.90 55.10 18.20 51.50 54.70 18.30 51.10 54.30 18.40 50.70 54.00 18.50 50.40 53.60 18.60 51.80 53.30 18.70 58.80 53.80 18.80 68.60 59.30 18.90 88.00 71.00 19.00 109.90 83.10 19.10 125.00 92.80 19.20 138.40 102.50 19.30 148.80 111.60 19.40 155.30 118.70 19.50 159.10 124.30 19.60 161.40 128.60 19.70 162.90 132.00 19.80 163.90 134.40 19.90 164.80 136.40 20.00 165.30 137.90 20.10 165.80 139.10 20.20 166.20 140.10 20.30 166.50 140.90 20.40 166.80 141.60 20.50 167.00 142.20 20.60 167.20 142.70 20.70 167.30 143.00 20.80 167.40 143.40 20.90 167.60 143.80 21.00 167.60 144.10 21.10 167.70 144.30 21.20 167.80 144.60 21.30 167.90 144.70 21.40 167.90 145.00 21.50 168.00 145.10 21.60 168.00 145.30 21.70 168.00 145.40 21.80 168.10 145.50 21.90 167.90 145.40 22.00 162.80 140.80 22.10 150.70 134.60 22.20 141.70 129.20 22.30 133.90 124.50 22.40 127.20 120.10 22.50 121.30 116.20 22.60 116.10 112.50 22.70 111.40 109.10 22.80 107.20 106.10 22.90 103.40 103.20 23.00 100.00 100.60 23.10 96.80 98.00 23.20 93.90 95.70 23.30 91.20 93.50 23.40 88.60 91.40 23.50 86.40 89.40 23.60 84.30 87.50 23.70 82.50 85.80 23.80 80.70 84.20 23.90 79.20 82.70 24.00 77.80 81.30 24.10 76.50 79.90 24.20 75.40 78.50 24.30 74.30 77.30 24.40 73.20 76.10 24.50 72.00 75.00 24.60 70.90 73.90 24.70 69.80 72.90 24.80 68.60 71.90 24.90 67.60 70.90 25.00 66.60 70.00 25.10 65.70 69.20 25.20 64.80 68.30 25.30 64.00 67.50 25.40 63.20 66.70 25.50 62.40 66.00 25.60 61.60 65.30 25.70 60.80 64.50 25.80 60.00 63.80 25.90 59.20 63.00 26.00 58.40 62.30 26.10 57.80 61.60 26.20 57.30 60.90 26.30 56.70 60.20 26.40 56.30 59.70 26.50 55.80 59.10 26.60 55.10 58.40 26.70 54.60 57.90 26.80 54.10 57.30 26.90 53.70 56.80 27.00 53.30 56.20 27.10 52.90 55.70 27.20 52.50 55.30 27.30 52.10 54.80 27.40 51.70 54.40 27.50 51.30 54.00 AUTO0032 43.9 31.1 43.5 31.1 43.6 31.1 43.2 31.1 43 31.2 43 31.2 42.7 31.3 42.2 31.3 41.8 31.4 40.9 31.4 40.1 31.4 39.7 31.5 39 31.5 38.2 31.5 37.9 31.5 37.6 31.5 37.3 31.5 37.1 31.6 37.2 31.6 37.8 31.6 37.8 31.6 38.7 31.7 40.2 35.4 63.3 52.3 87.7 71.3 104.6 84.7 116 94.5 125.1 102.7 135 111.1 142 118.8 146.3 124.5 149.6 128.5 152.5 131.4 155.2 133.7 157.6 135.4 159.5 136.8 161 138 162.3 138.9 163.2 139.6 163.9 140.2 164.5 140.8 165 141.2 165.4 141.6 165.7 141.9 165.9 142.2 166 142.5 166.2 142.7 166.3 142.9 166.4 143.1 166.5 143.3 166.7 143.4 166.7 143.6 166.8 143.8 166.8 143.9 164.7 141.4 155 134 144.7 128.1 135.7 122.9 128 118.2 121.2 113.9 115.3 109.9 110 106.2 105.3 102.8 101 99.7 97 96.7 93.5 94 90.2 91.4 87.2 88.9 84.5 86.6 81.9 84.5 79.5 82.4 77.6 80.5 75.8 78.6 74.2 76.9 72.7 75.2 71.3 73.7 70 72.3 68.5 70.9 67 69.7 65.4 68.5 64 67.3 62.8 66.2 61.6 65.2 60.5 64.1 59.4 63.2 58.5 62.2 57.6 61.3 56.7 60.4 55.9 59.6 55 58.7 54.3 57.9 53.6 57.2 52.9 56.4 52.3 55.8 51.6 55.2 51.1 54.5 50.4 53.9 51 53.5 57.5 53.5 67.4 58.9 90.5 71.5 116 84.4 131.1 96.1 142.5 106.6 150.7 114.9 156 121.7 159.2 127 161.4 130.9 162.8 133.7 163.8 135.8 164.6 137.5 165.2 138.8 165.7 139.8 166.1 140.7 166.4 141.4 166.6 142 166.8 142.4 167 142.8 167.2 143.2 167.3 143.5 167.4 143.8 167.5 144 167.6 144.3 167.6 144.4 167.7 144.6 167.8 144.7 167.8 144.8 167.8 145 167.9 145.1 167.9 145.2 167.7 145.2 163.4 141 152.3 134.4 142.9 129 134.7 124.2 127.7 119.8 121.6 115.7 116.1 112 111.2 108.5 106.9 105.2 102.9 102.3 99.3 99.5 96.1 97 93.1 94.5 90.3 92.2 87.7 90 85.3 88 83.1 86.1 81.1 84.4 79.4 82.7 77.8 81.1 76.4 79.6 75.1 78.1 73.9 76.7 72.8 75.4 71.6 74.2 70.4 73 69.1 71.9 67.9 70.9 66.7 69.9 65.5 68.9 64.5 68 63.6 67.1 62.7 66.3 61.8 65.4 60.9 64.7 60 63.9 59.2 63.1 58.5 62.4 57.8 61.7 57.2 61 56.5 60.3 55.8 59.7 55.2 59 54.8 58.5 54.3 58 53.9 57.5 53.5 57 53 56.5 52.5 56 52.2 55.5 51.9 55.1 51.5 54.7 51.1 54.3 50.7 54 50.4 53.6 51.8 53.3 58.8 53.8 68.6 59.3 88 71 109.9 83.1 125 92.8 138.4 102.5 148.8 111.6 155.3 118.7 159.1 124.3 161.4 128.6 162.9 132 163.9 134.4 164.8 136.4 165.3 137.9 165.8 139.1 166.2 140.1 166.5 140.9 166.8 141.6 167 142.2 167.2 142.7 167.3 143 167.4 143.4 167.6 143.8 167.6 144.1 167.7 144.3 167.8 144.6 167.9 144.7 167.9 145 168 145.1 168 145.3 168 145.4 168.1 145.5 167.9 145.4 162.8 140.8 150.7 134.6 141.7 129.2 133.9 124.5 127.2 120.1 121.3 116.2 116.1 112.5 111.4 109.1 107.2 106.1 103.4 103.2 100 100.6 96.8 98 93.9 95.7 91.2 93.5 88.6 91.4 86.4 89.4 84.3 87.5 82.5 85.8 80.7 84.2 79.2 82.7 77.8 81.3 76.5 79.9 75.4 78.5 74.3 77.3 73.2 76.1 72 75 70.9 73.9 69.8 72.9 68.6 71.9 67.6 70.9 66.6 70 65.7 69.2 64.8 68.3 64 67.5 63.2 66.7 62.4 66 61.6 65.3 60.8 64.5 60 63.8 59.2 63 58.4 62.3 57.8 61.6 57.3 60.9 56.7 60.2 56.3 59.7 55.8 59.1 55.1 58.4 54.6 57.9 54.1 57.3 53.7 56.8 53.3 56.2 52.9 55.7 52.5 55.3 52.1 54.8 51.7 54.4 51.3 54 PP&PP at top side PP&Sealant at AL tab 0.00 31.50 31.80 0.10 31.60 31.90 0.20 31.70 32.00 0.30 31.70 32.00 0.40 31.70 32.10 0.50 31.80 32.10 0.60 31.80 32.10 0.70 31.70 32.10 0.80 31.70 32.20 0.90 31.80 32.30 1.00 32.00 32.30 1.10 38.20 33.20 1.20 44.20 35.50 1.30 62.30 47.10 1.40 85.80 61.80 1.50 110.00 76.30 1.60 128.10 88.70 1.70 140.40 98.70 1.80 149.00 107.10 1.90 154.60 114.00 2.00 158.30 119.70 2.10 161.00 124.20 2.20 162.90 128.10 2.30 164.10 131.10 2.40 165.10 133.60 2.50 165.80 135.50 2.60 166.40 137.00 2.70 166.80 138.10 2.80 167.10 139.10 2.90 167.40 139.90 3.00 167.70 140.60 3.10 167.90 141.20 3.20 168.00 141.70 3.30 168.10 142.10 3.40 165.90 140.00 3.50 153.50 132.70 3.60 142.60 126.20 3.70 133.40 120.50 3.80 125.50 115.50 3.90 118.70 110.90 4.00 112.70 106.70 4.10 107.40 102.90 4.20 102.60 99.30 4.30 98.40 96.10 4.40 94.50 93.10 4.50 90.90 90.40 4.60 87.60 87.80 4.70 84.70 85.40 4.80 82.00 83.10 4.90 79.50 81.00 5.00 77.30 79.00 5.10 75.40 77.00 5.20 73.60 75.20 5.30 72.00 73.50 5.40 70.60 71.90 5.50 69.10 70.40 5.60 67.60 69.00 5.70 66.10 67.70 5.80 64.70 66.40 5.90 63.20 65.20 6.00 61.90 64.00 6.10 60.70 63.00 6.20 59.60 61.90 6.30 58.50 60.90 6.40 57.40 59.90 6.50 56.40 58.90 6.60 55.50 58.00 6.70 54.60 57.10 6.80 53.80 56.30 6.90 53.20 55.60 7.00 52.60 54.90 7.10 51.90 54.20 7.20 51.20 53.60 7.30 50.50 52.90 7.40 49.80 52.40 7.50 49.10 51.80 7.60 48.40 51.20 7.70 47.80 50.70 7.80 47.20 50.00 7.90 46.70 49.50 8.00 46.20 48.90 8.10 45.70 48.40 8.20 45.30 48.00 8.30 44.90 47.50 8.40 44.50 47.10 8.50 44.20 46.70 8.60 43.90 46.40 8.70 43.60 46.10 8.80 43.30 45.80 8.90 43.10 45.50 9.00 42.90 45.20 9.10 42.60 45.00 9.20 42.50 44.70 9.30 42.20 44.50 9.40 42.00 44.30 9.50 41.80 44.00 9.60 41.60 43.90 9.70 41.40 43.70 9.80 41.30 43.40 9.90 41.10 43.30 10.00 41.00 43.00 10.10 40.80 42.90 10.20 40.60 42.80 10.30 40.50 42.60 10.40 40.40 42.40 10.50 40.30 42.20 10.60 40.20 42.10 10.70 40.00 42.00 10.80 39.80 41.90 10.90 39.70 41.70 11.00 39.60 41.70 11.10 39.50 41.50 11.20 39.50 41.50 11.30 39.50 41.40 11.40 39.60 41.40 11.50 39.50 41.30 11.60 39.30 41.20 11.70 39.20 41.20 11.80 39.20 41.10 11.90 39.10 41.00 12.00 38.90 40.90 12.10 38.70 40.80 12.20 38.60 40.70 12.30 38.50 40.60 12.40 38.60 40.60 12.50 38.60 40.60 12.60 38.30 40.40 12.70 38.10 40.20 12.80 38.00 40.20 12.90 38.10 40.20 13.00 38.00 40.10 13.10 38.30 40.10 13.20 38.30 40.10 13.30 38.20 40.00 13.40 38.20 40.10 13.50 38.10 39.90 13.60 38.30 40.00 13.70 38.10 39.80 13.80 38.10 39.80 13.90 38.10 39.80 14.00 38.10 39.80 14.10 38.00 39.70 14.20 38.00 39.70 14.30 39.40 39.60 14.40 47.40 40.40 14.50 57.50 47.50 14.60 88.50 63.10 14.70 118.50 78.50 14.80 134.70 91.50 14.90 145.30 102.20 15.00 152.40 110.80 15.10 156.80 117.40 15.20 160.00 122.70 15.30 161.90 126.70 15.40 163.50 130.20 15.50 164.60 132.80 15.60 165.40 134.80 15.70 166.10 136.40 15.80 166.50 137.70 15.90 167.00 138.80 16.00 167.30 139.70 16.10 167.60 140.50 16.20 167.80 141.20 16.30 168.00 141.70 16.40 168.10 142.30 16.50 168.30 142.70 16.60 168.30 143.00 16.70 162.90 138.40 16.80 151.40 131.30 16.90 141.20 125.40 17.00 132.60 120.30 17.10 125.30 115.60 17.20 118.90 111.40 17.30 113.20 107.60 17.40 108.20 104.00 17.50 103.80 100.80 17.60 99.70 97.90 17.70 96.10 95.10 17.80 92.70 92.50 17.90 89.60 90.00 18.00 86.80 87.80 18.10 84.40 85.70 18.20 82.10 83.70 18.30 79.90 81.80 18.40 78.00 80.00 18.50 76.30 78.20 18.60 74.70 76.60 18.70 73.20 75.10 18.80 71.80 73.70 18.90 70.60 72.30 19.00 69.20 71.00 19.10 67.90 69.80 19.20 66.60 68.60 19.30 65.40 67.50 19.40 64.20 66.40 19.50 63.10 65.40 19.60 62.00 64.40 19.70 61.00 63.40 19.80 60.10 62.50 19.90 59.30 61.60 20.00 58.40 60.80 20.10 57.60 60.00 20.20 56.90 59.20 20.30 56.20 58.50 20.40 55.50 57.80 20.50 54.90 57.10 20.60 54.30 56.50 20.70 53.80 55.90 20.80 53.10 55.30 20.90 52.50 54.70 21.00 52.00 54.20 21.10 51.60 53.80 21.20 51.10 53.30 21.30 50.70 52.80 21.40 50.20 52.40 21.50 49.80 52.00 21.60 49.40 51.60 21.70 49.00 51.20 21.80 48.70 50.90 21.90 48.30 50.50 22.00 48.10 50.20 22.10 47.80 49.90 22.20 47.50 49.60 22.30 47.20 49.30 22.40 47.00 49.10 22.50 46.80 48.80 22.60 46.50 48.60 22.70 46.30 48.30 22.80 46.10 48.10 22.90 46.00 47.90 23.00 45.90 47.70 23.10 45.70 47.50 23.20 45.40 47.30 23.30 45.20 47.10 23.40 45.10 46.90 23.50 44.90 46.80 23.60 44.70 46.60 23.70 44.60 46.50 23.80 44.40 46.30 23.90 44.20 46.20 24.00 44.10 46.00 24.10 44.00 45.90 24.20 44.00 45.70 24.30 43.90 45.60 24.40 43.90 45.50 24.50 43.80 45.50 24.60 43.60 45.40 24.70 43.40 45.30 24.80 43.20 45.20 24.90 43.00 45.10 25.00 42.80 45.00 25.10 42.70 44.90 25.20 42.60 44.80 25.30 42.40 44.80 25.40 42.40 44.70 25.50 42.30 44.60 25.60 42.20 44.50 25.70 42.10 44.40 25.80 42.20 44.30 25.90 42.40 44.30 26.00 42.30 44.20 26.10 42.20 44.10 26.20 42.10 44.10 26.30 42.10 44.00 26.40 42.10 43.90 26.50 42.00 43.80 26.60 41.80 43.70 26.70 41.70 43.60 26.80 41.70 43.60 26.90 41.60 43.50 27.00 47.00 43.80 27.10 54.90 45.00 27.20 70.50 57.30 27.30 107.00 73.10 27.40 128.70 86.90 27.50 142.00 99.20 27.60 150.90 109.20 27.70 156.30 116.80 27.80 159.60 122.60 27.90 161.80 127.20 28.00 163.20 130.70 28.10 164.30 133.40 28.20 165.20 135.60 28.30 165.90 137.30 28.40 166.40 138.60 28.50 166.80 139.70 28.60 167.20 140.70 28.70 167.40 141.50 28.80 167.70 142.10 28.90 167.90 142.70 29.00 168.00 143.20 29.10 168.20 143.60 29.20 168.30 144.00 29.30 168.70 143.70 29.40 158.10 136.50 29.50 147.00 130.30 29.60 137.80 125.00 29.70 129.90 120.10 29.80 123.10 115.60 29.90 117.20 111.70 30.00 112.00 108.00 30.10 107.30 104.60 30.20 103.10 101.50 30.30 99.30 98.70 30.40 95.80 96.00 30.50 92.70 93.50 30.60 89.80 91.20 30.70 87.10 89.00 30.80 84.70 87.00 30.90 82.50 85.10 31.00 80.50 83.30 31.10 78.70 81.50 31.20 77.20 79.80 31.30 75.70 78.30 31.40 74.40 76.80 31.50 73.20 75.40 31.60 72.00 74.10 31.70 70.80 72.80 31.80 69.50 71.70 31.90 68.30 70.50 32.00 67.00 69.50 32.10 65.90 68.50 32.20 64.60 67.40 32.30 63.40 66.50 32.40 62.20 65.50 32.50 61.10 64.50 32.60 60.00 63.50 32.70 59.00 62.50 32.80 58.10 61.60 32.90 57.20 60.90 33.00 56.40 60.00 33.10 55.80 59.20 33.20 55.30 58.60 33.30 54.70 57.80 33.40 54.10 57.20 33.50 53.50 56.60 33.60 53.00 56.00 33.70 52.50 55.50 33.80 52.00 55.00 33.90 51.60 54.40 34.00 51.10 54.00 34.10 50.70 53.50 34.20 50.40 53.20 34.30 49.90 52.70 34.40 49.60 52.30 34.50 49.10 51.80 34.60 48.90 51.60 34.70 48.40 51.10 34.80 48.20 50.90 34.90 47.90 50.50 35.00 47.60 50.20 35.10 47.30 49.90 35.20 47.10 49.60 35.30 46.80 49.30 35.40 46.50 49.00 35.50 46.30 48.80 31.5 31.8 31.6 31.9 31.7 32 31.7 32 31.7 32.1 31.8 32.1 31.8 32.1 31.7 32.1 31.7 32.2 31.8 32.3 32 32.3 38.2 33.2 44.2 35.5 62.3 47.1 85.8 61.8 110 76.3 128.1 88.7 140.4 98.7 149 107.1 154.6 114 158.3 119.7 161 124.2 162.9 128.1 164.1 131.1 165.1 133.6 165.8 135.5 166.4 137 166.8 138.1 167.1 139.1 167.4 139.9 167.7 140.6 167.9 141.2 168 141.7 168.1 142.1 165.9 140 153.5 132.7 142.6 126.2 133.4 120.5 125.5 115.5 118.7 110.9 112.7 106.7 107.4 102.9 102.6 99.3 98.4 96.1 94.5 93.1 90.9 90.4 87.6 87.8 84.7 85.4 82 83.1 79.5 81 77.3 79 75.4 77 73.6 75.2 72 73.5 70.6 71.9 69.1 70.4 67.6 69 66.1 67.7 64.7 66.4 63.2 65.2 61.9 64 60.7 63 59.6 61.9 58.5 60.9 57.4 59.9 56.4 58.9 55.5 58 54.6 57.1 53.8 56.3 53.2 55.6 52.6 54.9 51.9 54.2 51.2 53.6 50.5 52.9 49.8 52.4 49.1 51.8 48.4 51.2 47.8 50.7 47.2 50 46.7 49.5 46.2 48.9 45.7 48.4 45.3 48 44.9 47.5 44.5 47.1 44.2 46.7 43.9 46.4 43.6 46.1 43.3 45.8 43.1 45.5 42.9 45.2 42.6 45 42.5 44.7 42.2 44.5 42 44.3 41.8 44 41.6 43.9 41.4 43.7 41.3 43.4 41.1 43.3 41 43 40.8 42.9 40.6 42.8 40.5 42.6 40.4 42.4 40.3 42.2 40.2 42.1 40 42 39.8 41.9 39.7 41.7 39.6 41.7 39.5 41.5 39.5 41.5 39.5 41.4 39.6 41.4 39.5 41.3 39.3 41.2 39.2 41.2 39.2 41.1 39.1 41 38.9 40.9 38.7 40.8 38.6 40.7 38.5 40.6 38.6 40.6 38.6 40.6 38.3 40.4 38.1 40.2 38 40.2 38.1 40.2 38 40.1 38.3 40.1 38.3 40.1 38.2 40 38.2 40.1 38.1 39.9 38.3 40 38.1 39.8 38.1 39.8 38.1 39.8 38.1 39.8 38 39.7 38 39.7 39.4 39.6 47.4 40.4 57.5 47.5 88.5 63.1 118.5 78.5 134.7 91.5 145.3 102.2 152.4 110.8 156.8 117.4 160 122.7 161.9 126.7 163.5 130.2 164.6 132.8 165.4 134.8 166.1 136.4 166.5 137.7 167 138.8 167.3 139.7 167.6 140.5 167.8 141.2 168 141.7 168.1 142.3 168.3 142.7 168.3 143 162.9 138.4 151.4 131.3 141.2 125.4 132.6 120.3 125.3 115.6 118.9 111.4 113.2 107.6 108.2 104 103.8 100.8 99.7 97.9 96.1 95.1 92.7 92.5 89.6 90 86.8 87.8 84.4 85.7 82.1 83.7 79.9 81.8 78 80 76.3 78.2 74.7 76.6 73.2 75.1 71.8 73.7 70.6 72.3 69.2 71 67.9 69.8 66.6 68.6 65.4 67.5 64.2 66.4 63.1 65.4 62 64.4 61 63.4 60.1 62.5 59.3 61.6 58.4 60.8 57.6 60 56.9 59.2 56.2 58.5 55.5 57.8 54.9 57.1 54.3 56.5 53.8 55.9 53.1 55.3 52.5 54.7 52 54.2 51.6 53.8 51.1 53.3 50.7 52.8 50.2 52.4 49.8 52 49.4 51.6 49 51.2 48.7 50.9 48.3 50.5 48.1 50.2 47.8 49.9 47.5 49.6 47.2 49.3 47 49.1 46.8 48.8 46.5 48.6 46.3 48.3 46.1 48.1 46 47.9 45.9 47.7 45.7 47.5 45.4 47.3 45.2 47.1 45.1 46.9 44.9 46.8 44.7 46.6 44.6 46.5 44.4 46.3 44.2 46.2 44.1 46 44 45.9 44 45.7 43.9 45.6 43.9 45.5 43.8 45.5 43.6 45.4 43.4 45.3 43.2 45.2 43 45.1 42.8 45 42.7 44.9 42.6 44.8 42.4 44.8 42.4 44.7 42.3 44.6 42.2 44.5 42.1 44.4 42.2 44.3 42.4 44.3 42.3 44.2 42.2 44.1 42.1 44.1 42.1 44 42.1 43.9 42 43.8 41.8 43.7 41.7 43.6 41.7 43.6 41.6 43.5 47 43.8 54.9 45 70.5 57.3 107 73.1 128.7 86.9 142 99.2 150.9 109.2 156.3 116.8 159.6 122.6 161.8 127.2 163.2 130.7 164.3 133.4 165.2 135.6 165.9 137.3 166.4 138.6 166.8 139.7 167.2 140.7 167.4 141.5 167.7 142.1 167.9 142.7 168 143.2 168.2 143.6 168.3 144 168.7 143.7 158.1 136.5 147 130.3 137.8 125 129.9 120.1 123.1 115.6 117.2 111.7 112 108 107.3 104.6 103.1 101.5 99.3 98.7 95.8 96 92.7 93.5 89.8 91.2 87.1 89 84.7 87 82.5 85.1 80.5 83.3 78.7 81.5 77.2 79.8 75.7 78.3 74.4 76.8 73.2 75.4 72 74.1 70.8 72.8 69.5 71.7 68.3 70.5 67 69.5 65.9 68.5 64.6 67.4 63.4 66.5 62.2 65.5 61.1 64.5 60 63.5 59 62.5 58.1 61.6 57.2 60.9 56.4 60 55.8 59.2 55.3 58.6 54.7 57.8 54.1 57.2 53.5 56.6 53 56 52.5 55.5 52 55 51.6 54.4 51.1 54 50.7 53.5 50.4 53.2 49.9 52.7 49.6 52.3 49.1 51.8 48.9 51.6 48.4 51.1 48.2 50.9 47.9 50.5 47.6 50.2 47.3 49.9 47.1 49.6 46.8 49.3 46.5 49 46.3 48.8 PP&PP at top side PP&Sealant at Al tab 0.00 31.50 30.80 0.10 31.50 30.90 0.20 31.30 31.00 0.30 31.20 31.00 0.40 31.40 31.10 0.50 31.90 31.30 0.60 35.80 31.60 0.70 40.60 32.60 0.80 51.80 47.60 0.90 81.00 69.40 1.00 101.30 84.50 1.10 113.40 95.50 1.20 121.90 103.80 1.30 129.50 110.00 1.40 134.90 114.70 1.50 139.10 118.70 1.60 141.70 122.10 1.70 144.10 125.00 1.80 145.80 127.50 1.90 147.30 129.40 2.00 148.40 131.10 2.10 149.20 132.40 2.20 150.20 133.60 2.30 150.80 134.60 2.40 151.40 135.40 2.50 151.80 136.10 2.60 152.20 136.70 2.70 152.70 137.20 2.80 153.00 137.70 2.90 153.20 138.10 3.00 153.50 138.40 3.10 153.70 138.70 3.20 153.80 139.00 3.30 153.80 139.20 3.40 154.00 139.40 3.50 154.10 139.70 3.60 154.30 139.90 3.70 154.40 140.00 3.80 154.50 140.20 3.90 175.10 137.80 4.00 145.60 131.00 4.10 134.90 125.20 4.20 126.50 120.00 4.30 119.30 115.20 4.40 113.10 110.90 4.50 107.90 107.00 4.60 103.60 103.30 4.70 104.50 100.00 4.80 100.30 96.90 4.90 92.30 94.00 5.00 99.80 91.20 5.10 76.90 81.60 5.20 74.80 79.40 5.30 72.90 77.40 5.40 71.10 75.60 5.50 69.50 73.80 5.60 68.00 72.20 5.70 66.50 70.60 5.80 65.00 69.10 5.90 63.60 67.70 6.00 62.40 66.40 6.10 61.10 65.20 6.20 59.90 64.00 6.30 58.80 62.80 6.40 57.70 61.80 6.50 56.70 60.80 6.60 55.80 59.80 6.70 55.00 58.80 6.80 54.20 57.90 6.90 53.40 57.10 7.00 52.60 56.30 7.10 51.90 55.50 7.20 51.30 54.80 7.30 50.70 54.10 7.40 50.10 53.50 7.50 49.50 52.80 7.60 49.00 52.30 7.70 48.40 51.70 7.80 48.00 51.20 7.90 47.50 50.60 8.00 47.20 50.20 8.10 46.70 49.70 8.20 46.40 49.30 8.30 46.00 48.80 8.40 45.60 48.40 8.50 45.30 48.00 8.60 45.00 47.70 8.70 44.60 47.40 8.80 44.30 47.00 8.90 44.10 46.70 9.00 43.90 46.40 9.10 43.60 46.10 9.20 43.40 45.90 9.30 43.20 45.60 9.40 42.90 45.30 9.50 42.70 45.10 9.60 42.60 44.90 9.70 42.40 44.70 9.80 42.10 44.40 9.90 41.90 44.20 10.00 41.70 44.10 10.10 41.60 43.80 10.20 41.40 43.60 10.30 41.20 43.50 10.40 41.00 43.30 10.50 40.80 43.10 10.60 40.70 43.00 10.70 40.50 42.80 10.80 40.40 42.70 10.90 40.30 42.50 11.00 40.20 42.40 11.10 40.20 42.20 11.20 40.20 42.10 11.30 40.00 42.10 11.40 39.80 42.00 11.50 39.70 41.90 11.60 39.60 41.80 11.70 39.60 41.80 11.80 39.60 41.70 11.90 39.50 41.60 12.00 39.50 41.50 12.10 39.30 41.30 12.20 39.30 41.20 12.30 39.30 41.30 12.40 39.30 41.20 12.50 44.00 41.50 12.60 53.90 47.50 12.70 84.70 68.00 12.80 106.00 82.80 12.90 120.10 94.60 13.00 127.80 104.00 13.10 133.80 111.70 13.20 139.00 118.10 13.30 142.90 123.10 13.40 145.90 126.90 13.50 147.90 129.90 13.60 149.40 132.30 13.70 150.70 134.30 13.80 151.70 135.90 13.90 152.50 137.20 14.00 153.30 138.20 14.10 153.80 139.10 14.20 154.30 139.90 14.30 154.70 140.50 14.40 155.10 140.90 14.50 155.30 141.40 14.60 155.50 141.80 14.70 155.70 142.00 14.80 156.00 142.30 14.90 156.00 142.50 15.00 156.20 142.70 15.10 156.40 142.90 15.20 156.40 143.10 15.30 156.60 143.20 15.40 156.70 143.30 15.50 156.70 143.50 15.60 156.80 143.60 15.70 157.30 143.70 15.80 83.90 87.50 15.90 82.30 85.30 16.00 78.60 83.20 16.10 76.30 81.30 16.20 74.40 79.40 16.30 72.80 77.70 16.40 71.30 76.00 16.50 69.80 74.50 16.60 68.40 73.00 16.70 67.00 71.70 16.80 65.80 70.30 16.90 64.50 69.10 17.00 63.40 68.00 17.10 62.20 66.80 17.20 61.20 65.80 17.30 60.30 64.80 17.40 59.30 63.80 17.50 58.40 62.90 17.60 57.60 62.10 17.70 56.80 61.20 17.80 56.10 60.40 17.90 55.50 59.60 18.00 54.80 58.90 18.10 54.30 58.20 18.20 53.80 57.60 18.30 53.30 57.10 18.40 52.70 56.50 18.50 52.20 56.00 18.60 51.70 55.40 18.70 51.30 54.90 18.80 50.90 54.40 18.90 50.50 54.00 19.00 50.20 53.50 19.10 49.70 53.10 19.20 49.40 52.70 19.30 49.00 52.40 19.40 48.70 52.00 19.50 48.50 51.70 19.60 48.30 51.30 19.70 48.00 51.00 19.80 47.70 50.70 19.90 47.40 50.40 20.00 47.20 50.10 20.10 46.90 49.80 20.20 46.60 49.60 20.30 46.50 49.30 20.40 46.20 49.10 20.50 46.00 48.80 20.60 45.80 48.60 20.70 45.60 48.40 20.80 49.60 48.40 20.90 55.60 50.50 21.00 97.30 71.20 21.10 113.20 87.30 21.20 125.20 99.30 21.30 133.60 108.80 21.40 139.30 116.20 21.50 143.40 121.90 21.60 146.30 126.20 21.70 148.40 129.70 21.80 150.10 132.40 21.90 151.50 134.60 22.00 152.60 136.40 22.10 153.40 137.80 22.20 154.10 139.00 22.30 154.70 139.90 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0 0 PP&PP at top side PP&Sealant at Al tab _1208779482.bin _1208779649.bin _1208780110.bin _1208779588.bin _1208779065.bin _1208779388.bin
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